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61.
Stress analysis of spontaneous Sn whisker growth 总被引:5,自引:0,他引:5
K. N. Tu Chih Chen Albert T. Wu 《Journal of Materials Science: Materials in Electronics》2007,18(1-3):269-281
Spontaneous Sn whisker growth is a surface relief phenomenon of creep, driven by a compressive stress gradient. No externally
applied stress is required for the growth, and the compressive stress is generated within, from the chemical reaction between
Sn and Cu to form the intermetallic compound Cu6Sn5 at room temperature. To obtain the compressive stress gradient, a break of the protective oxide on the Sn surface is required
because the free surface of the break is stress-free. Thus, spontaneous Sn whisker growth is unique that stress relaxation
accompanies stress generation. One of the whisker challenging issues in understanding and in finding effective methods to
prevent spontaneous Sn whisker growth is to develop accelerated tests of whisker growth. Use of electromigration on short
Sn stripes can facilitate this. The stress distribution around the vicinity and the root of a whisker can be obtained by using
the micro-beam X-ray diffraction utilizing synchrotron radiation. A discussion of how to prevent spontaneous Sn whisker growth
by blocking both stress generation and stress relaxation is given. 相似文献
62.
Skim and whole milk powders were manufactured at lab scale by spray freeze drying (SFD), using liquid nitrogen as the cryogen. The polydispersity of droplet/particle sizes was limited using an encapsulator nozzle to atomize the feed. Particle morphology was examined using a scanning electron microscope. Samples were compared with equivalent spray-dried powders in tests of wettability and dissolution in water. The spray freeze-dried powders were found to be highly porous, with a uniform structure of pores throughout the entire particles. When tested in water, SFD skim milk powders wetted roughly three times as fast as industrially spray-dried agglomerated skim milk powders and were observed to dissolve rapidly by breaking down into smaller particles. 相似文献
63.
Tian Xiao Qing Huo Liu 《Antennas and Propagation, IEEE Transactions on》2008,56(3):765-773
In this paper, we present an enlarged cell technique (ECT) to avoid the time step reduction encountered in the conformal finite-difference time-domain (CFDTD) method due to small irregular cells truncated by metallic boundaries. We focus our efforts on the discussion of the accuracy and stability of the ECT and its comparison with other conformal methods, especially the one called the uniformly stable conformal (USC) method. We also provide a simplified ECT, which is much easier to implement. In the ECT, a stability criterion is first constructed to identify instable irregular cells, i.e., those having so small an area to cause instability. Those instable cells are then enlarged into their adjacent cells to obtain a large, stable area. Careful treatment is performed on the communication between the intruding and intruded cells in terms of electromotive force by keeping the total electromotive force conservative. This technique is verified by several 3-D numerical experiments. Results show that the ECT is second-order accurate and numerically stable at the regular Courant time step limit. 相似文献
64.
65.
MIP-CGP工艺专用催化剂CGP-1的开发与应用 总被引:11,自引:3,他引:8
阐述了生产汽油组分满足欧Ⅲ排放标准并多产丙烯的催化裂化工艺(简称MIP-CGP)专用催化剂(简称CGP-1)的研究开发与工业应用结果。CGP-1催化剂的基质具有良好的容炭性能,使活性组元受到良好保护,其优势作用在第二反应区得以充分发挥,具有更高的氢转移活性和强的汽油小分子烯烃裂化活性。中国石化九江分公司和镇海炼化公司的MIP-CGP工业试验标定结果表明,与常规FCC相比,采用CGP-1催化剂的MIP-CGP技术在生产烯烃体积分数小于18%的汽油组分的同时,丙烯产率达到8%以上。此外,汽油诱导期大幅提高,抗爆指数增加;总液体收率有所提高,干气产率下降,焦炭选择性良好。 相似文献
66.
镁钴铝类水滑石催化合成安息香甲醚 总被引:1,自引:0,他引:1
采用共沉淀法制备了镁钴铝类水滑石化合物(MgCoAl-HTLcs),并用 X 射线衍射、扫描电子显微镜、NH_3程序升温脱附等方法对 MgCoAl-HTLcs 进行了表征,并以 MgCoAl-HTLcs 为催化剂催化苯甲醛与甲醇反应合成安息香甲醚,研究了n(Mg):n(Co):n(Al)、催化剂用量、原料配比、反应温度、反应时间对合成反应的影响。表征结果显示,MgCoAl-HTLcs 的晶相完整,表面主要为弱酸、弱碱性。催化合成安息香甲醚的适宜条件为:MgCoAl-HTLcs 催化剂用量0.10 g(约为原料总质量的0.23%),n(Mg):n(Co):n(Al)=0.4:1.6:1.0,V(苯甲醛):V(甲醇)=3:50,反应温度50℃,反应时间150 min。在此条件下,苯甲醛的平衡转化率达77.49%,安息香甲醚选择性接近100%。为洁净合成安息香甲醚开辟了一条新的途径。 相似文献
67.
镍氢电池负极用低成本储氢合金的研究 总被引:1,自引:0,他引:1
研究了ABS型储氢合金在低Co含量条件下,随B组元替代元素Co,Al,Si等含量的变化对合金电化学性能的影响规律,同时研究了A组元中不同La/Ce比对合金电化学性能的影响情况。结果表明,随合金中Co含量的降低,合金的活化性能和放电容量得以改善,但合金的循环寿命下降也比较明显;在试验范围内,随Al元素的加入,合金的循环寿命得以改善,但材料的放电容量和活化性能均有所下降;随合金La/Ce比的降低,合金的放电容量略有下降,但其循环寿命和放电电压平台有较大提高。 相似文献
68.
Bingyong Yan Zuohua Tian Songjiao Shi 《International Journal of Electrical Power & Energy Systems》2008,30(5):343-360
In this paper, we propose a novel distributed robust fault detection and identification (RFDI) scheme for a class of nonlinear systems. Firstly, a detection and identification estimator—robust fault tracking approximator (RFTA) is designed for online health monitoring. A novel feature of the RFTA is that it can simultaneously detect and accurately identify the shape and magnitude of the fault and disturbance. Moreover, it takes less online training time compared with the traditional neural network based fault diagnosis schemes. For some distributed systems, a network of distributed estimators is constructed where the RFTA is embedded into each estimator. Then we use consensus filter to filter the outputs of each estimator. One of the most important merits of the consensus filter is that its outputs can dramatically improve the accuracy of fault detection and identification. Next, the stability of the distributed RFDI scheme is rigorously investigated. Finally, two numerical examples are given to illustrate the feasibility and effectiveness of the proposed approach. 相似文献
69.
70.
Mixtures of Cr and Mo elemental powders, with the nominal compositions Cr25Mo75, Cr50Mo50, and Cr75Mo25, are processed by high-energy ball milling at ambient temperature. Milling is observed to force the mixing of the immiscible
bcc elements Cr and Mo into solid solutions. The lattice parameter of these solid solutions, measured by X-ray diffraction
(XRD), displays the expected positive deviation from Vegard’s law. These deviations are compared to the ones predicted by
Eshelby’s inclusion model for dilute alloys. The conventional Williamson-Hall approach is shown to fail to determine the grain
size in as-milled samples, probably due to the high density of dislocations. Annealing at 700 °C for 10 hours under argon
leads to a large reduction in structural defect density, without inducing any significant decomposition. The mixing measured
in Cr-Mo is discussed in the broader context of the mechanical mixing forced by ball milling in moderately immiscible systems. 相似文献