Method, algorithm and device for estimation of components above the harmonic frequency range up to 9 kHz

The paper presents a method of estimation of frequency groups with 200 Hz bandwidth in the frequency range from the 50th harmonic up to 9 kHz. The method consists of the application of a fast Fourier transform (FFT) for wavelet coefficients after input signal decomposition and partial synthesis for chosen frequency bands. It enables the computational complexity of the algorithm to be reduced and also attenuates influence of the fundamental component and low-frequency harmonics, as required by IEC Standard 61000-4-7. The particulars of this method are shown and analysis for a chosen wavelet family is provided. Further, the algorithm and its implementation in real device for power quality monitoring is presented. Finally, the results of measurements of two testing signals are shown. The required attenuation of fundamental component and required accuracy was obtained.     

Thermal and structural effects of poly(vinyl chloride)/(wood flour) compound gelation in the Brabender mixer

The processing of two unplasticized compounds of poly(vinyl chloride) (PVC) with and without wood flour (WF) was performed in a Brabender mixing chamber, at various chamber temperatures between 130 and 200°C and at a shear rate of 12.61 s^?1. The test was carried out up to the time corresponding to the equilibrium state of the torque, and the variations of torque and real melt temperature as functions of time were analyzed. It was found that the addition of WF led to fusion at lower chamber temperature and that during gelation, stronger self‐heating effects occurred in the WF‐filled PVC compound. Various characteristics of the real temperature gelation curves of PVC with and without the WF filler were observed and are discussed. J. VINYL ADDIT. TECHNOL., 2011. © 2011 Society of Plastics Engineers     

Active control of boundary conditions for dynamic thermal characterization of electronic components

This paper presents a practical realization of the system for the active control of boundary conditions during the dynamic thermal characterization of electronic components. The control of boundary conditions is exercised by the dual cold plate cooling assembly equipped with Peltier thermo-electric modules and an appropriate control circuit. Additionally, a tensometer bridge is used to assure the parallel alignment of surfaces and to adjust the contact thermal resistance between particular layers. The operation of the entire control system is illustrated based on a practical example where Peltier module currents are adjusted in real time so as to impose isothermal or constant heat flux boundary conditions on a power diode package surface during measurements performed with time varying power dissipation in the device.     

4,10-Dinitro-2,6,8,12-tetraoxa-4,10-diazatetracyclo[5.5.0.05,903,11]dodecane Synthesis

4,10-Dinitro-2,6,8,12-tetraoxa-4,10-diazatetracyclo[5.5.0.0^5,90^3,11]dodecane (TEX) was obtained by nitrolysis of 1,4-diformyl-2,3,5,6-tetrahydroxypiperazine reaction using a mixture of fuming nitric acid and concentrated sulfuric acid. The optimal process temperature was 54–56°C. The yield of the synthesis depends inter alia on the rate the reactants are introduced into the reaction medium and on the time of conditioning of the reaction mixture. A maximal yield of ca. 40% was achieved at the reactant addition time of 2 h and conditioning time of 2 h. None of the other nitrating mixtures examined proved superior to the conventional nitrating mixture. The product was examined by high-performance liquid chromatography (HPLC), nuclear magnetic resonance (NMR), Fourier transform infrared (FTIR), and differential scanning calorimetry (DSC) techniques and the results are reported.     

Time–frequency approach to extraction of selected second-order cyclostationary vibration components for varying operational conditions

In this paper, the authors propose a method for extracting second-order cyclostationary components from a vibration signal. For a known cyclic frequency, the proposed algorithm allows to estimate the amount of energy of each cyclic component of interest in the time–frequency domain. In this way, the resulting representation contains only the chosen second-order cyclostationary component that manifests itself as a number of carrier frequencies modulated by the harmonic signal of selected frequency.     

Ant colony optimization for job shop scheduling using multi-attribute dispatching rules

This paper proposes a heuristic method based on ant colony optimization to determine the suboptimal allocation of dynamic multi-attribute dispatching rules to maximize job shop system performance (four measures were analyzed: mean flow time, max flow time, mean tardiness, and max tardiness). In order to assure high adequacy of the job shop system representation, modeling is carried out using discrete-event simulation. The proposed methodology constitutes a framework of integration of simulation and heuristic optimization. Simulation is used for evaluation of the local fitness function for ants. A case study is used in this paper to illustrate how performance of a job shop production system could be affected by dynamic multi-attribute dispatching rule assignment.     

Influence of Potassium and NO Addition on Catalytic Activity in Soot Combustion and Surface Properties of Iron and Manganese Spinels

Two series of (0–4 wt%) potassium doped oxide catalysts based on iron and manganese spinel were prepared. The synthesized materials were characterized in terms of their structure (XRD, Raman spectroscopy) and surface electronic properties (work function measurements). The catalytic activity towards soot combustion was determined by temperature programmed oxidation of a physical mixture of soot and catalyst in tight contact in gas oxygen mixtures with and without NO addition. For iron spinel based materials, where potassium is localized at the surface, the catalytic activity correlates with the work function lowering upon K doping, while for manganese spinel based materials, where potassium is incorporated into the bulk (formation of KMn₄O₈ or KMn₈O₁₆), the correlation was not found. The presence of NO in the gas mixture leads to a systematic decrease of soot ignition temperature for all samples.     

High‐Mobility and Low Turn‐On Voltage n‐Channel OTFTs Based on a Solution‐Processable Derivative of Naphthalene Bisimide

In organic electronics solution‐processable n‐channel field‐effect transistors (FETs) matching the parameters of the best p‐channel FETs are needed. Progress toward the fabrication of such devices is strongly impeded by a limited number of suitable organic semiconductors as well as by the lack of processing techniques that enable strict control of the supramolecular organization in the deposited layer. Here, the use of N,N′‐bis(4‐n‐butylphenyl)‐1,4,5,8‐naphthalenetetracarboxylic‐1,4:5,8‐bisimide (NBI‐4‐n‐BuPh) for fabrication of n‐channel FETs is described. The unidirectionally oriented crystalline layers of NBI‐4‐n‐BuPh are obtained by the zone‐casting method under ambient conditions. Due to the bottom‐contact, top‐gate configuration used, the gate dielectric, Parylene C, also acts as a protective layer. This, together with a sufficiently low LUMO level of NBI‐4‐n‐BuPh allows the fabrication and operation of these novel n‐channel transistors under ambient conditions. The high order of the NBI‐4‐n‐BuPh molecules in the zone‐cast layer and high purity of the gate dielectric yield good performance of the transistors.