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81.
Vijay S. Reddy 《Crystallography Reviews》2016,22(2):128-140
The procedure for phase extension (PX) involves gradually extending the initial phases from low resolution (e.g. ~8?Å) to the high-resolution limit of a diffraction data set. Structural redundancy present in the viral capsids that display icosahedral symmetry results in a high degree of non-crystallographic symmetry (NCS), which in turn translates into higher phasing power and is critical for improving and extending phases to higher resolution. Greater completeness of the diffraction data and determination of a molecular replacement solution, which entails accurately identifying the virus particle orientation(s) and position(s), are important for the smooth progression of the PX procedure. In addition, proper definition of a molecular mask (envelope) around the NCS-asymmetric unit has been found to be important for the success of density modification procedures, such as density averaging and solvent flattening. Regardless of the degree of NCS, the PX method appears to work well in all space groups, provided an accurate molecular mask is used along with reasonable initial phases. However, in the cases with space group P1, in addition to requiring a molecular mask, starting the PX at a higher resolution (e.g. 6?Å) overcame the previously reported problems due to Babinet phases and phase flipping errors. 相似文献
82.
R. Vijay M. Nagini S. S. Sarma M. Ramakrishna A. V. Reddy G. Sundararajan 《Metallurgical and Materials Transactions A》2014,45(2):777-784
Bulk samples of pure iron and yttria dispersed iron with and without titanium (i.e., Fe, Fe-Y2O3, and Fe-Y2O3-Ti) were prepared by hot extrusion of high-energy ball-milled powders. An examination of the microstructure using TEM revealed that the addition of titanium resulted in the reduction of the dispersoid size with a concomitant increase in the volume fraction of the dispersoids. As a result, Fe-Y2O3-Ti exhibited a substantial increase in hardness and tensile properties as compared to Fe and Fe-Y2O3. The higher hardness and strength of Fe-Y2O3-Ti is shown to be due to the presence of finer and higher number density of Y-Ti-O complex oxides. Dynamic strain aging in the temperature range of 423 K to 573 K (150 °C to 300 °C) was observed in all the compositions studied. 相似文献
83.
84.
Ghosh Mritunjoy Prasad Muley Trupti Vijay Roy Shradha Mohanty Sipun Mukherjee Samrat 《Journal of Superconductivity and Novel Magnetism》2021,34(10):2643-2650
Journal of Superconductivity and Novel Magnetism - This paper reports the effects of rare-earth Sm3+ ion substitution on structural, optical, electronic, and magnetic responses of maghemite... 相似文献
85.
Shambhu Prasad Suraj Nayak Vamshi Vijay Rajib Mall 《Innovations in Systems and Software Engineering》2016,12(4):263-278
Simulink and Stateflow (SL/SF) models are being widely used to design and develop embedded systems. Often the SL/SF models of embedded controllers turn out to be large and consist of many subsystems and hierarchies. When such a system is maintained, it becomes difficult to manually analyse the model to identify the impacted elements due to the existence of several explicit and implicit dependencies among the model elements. To automate the analysis of an SL/SF model, we propose a metamodel to capture various types of dependencies existing across the basic blocks. We have named this metamodel Simulink dependency graph (SLDG). We investigate the use of SLDG in change impact visualization and regression test selection. We have developed a prototype tool by implementing our approach for the aforementioned applications. 相似文献
86.
Nair do Amaral Sampaio Neta José Cleiton Sousa dos Santos Soraya de Oliveira Sancho Sueli Rodrigues Luciana Rocha Barros Gonçalves Ligia R. Rodrigues José A. Teixeira 《Food Hydrocolloids》2012
Sugar esters are compounds with surfactant properties (biosurfactants), i.e., capable of reducing the surface tension and promote the emulsification of immiscible liquids. On the other hand, as with all emulsions, coconut milk is not physically stable and is prone to phase separation. Therefore, the aim of this work was to evaluate the synthesis of fructose, sucrose and lactose esters from the corresponding sugars using Candida antarctica type B lipase immobilized in two different supports, namely acrylic resin and chitosan, and evaluate its application in the stabilization of coconut milk emulsions. The enzyme immobilized on chitosan showed the highest yield of lactose ester production (84.1%). Additionally, the production of fructose ester was found to be higher for the enzyme immobilized on the acrylic resin support (74.3%) as compared with the one immobilized on chitosan (70.1%). The same trend was observed for the sucrose ester, although with lower percentage yields. Sugar esters were then added to samples of fresh coconut milk and characterized according to their surface tension, emulsification index and particle size distribution. Although the microscopic analysis showed similar results for all sugar esters, results indicated lactose ester as the best biosurfactant, with a surface tension of 38.0 N/m and an emulsification index of 54.1%, when used in a ratio of 1:10 (biosurfactant:coconut milk, v/v) for 48 h experiments. 相似文献
87.
Enrichment of ω‐3 fatty acids in flax seed oil by alkaline lipase of Aspergillus fumigatus MTCC 9657
Akhila Rajan Dasiah R. Sobankumar Ananthakrishnan J. Nair 《International Journal of Food Science & Technology》2014,49(5):1337-1343
Flax seed oil obtained from the seeds of flax plant (Linum usitatissimum, L.) is an unexploited source which contains ω‐3 and ω‐6 fatty acids. Flax seed oil is hydrolysed with a novel alkaline lipase from Aspergillus fumigatus MTCC 9657 for the removal of unwanted fatty acids and enrichment of ω‐3 fatty acids. An appropriate balance of ω‐3 and ω‐6 polyunsaturated fatty acids and enzymatic enrichment of polyunsaturated fatty acids in diet promote nutrition and health. Fatty acid composition shows that flax seed oil contains about 26.80%, 13.5% and 25.45% of ω‐3 and ω‐6 fatty acids in triglyceride (TG), diglyceride (DG) and monoglyceride (MG), respectively. After 8 h of hydrolysis, ω‐3 content was increased to 39% in TG, showing that unwanted saturated fatty acids are removed. ω‐6 content of triglycerides in flax seed oil also showed 54.76% increase after 8 h of hydrolysis. An enzymatic method of hydrolysis by fungal lipase was developed by this study and achieved to concentrate the essential fatty acids linoleic acid (LA) and α‐linoleic acids (ALA). 相似文献
88.
The interaction between molten gallium and the hydrocarbon medium induced by ultrasonic energy—can gallium carbide be formed?
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Vijay Bhooshan Kumar Manuel Monte Olivier Mathon Sakura Pascarelli Ze'ev Porat Aharon Gedanken 《Journal of the American Ceramic Society》2017,100(7):3305-3315
Ultrasonic irradiation of molten gallium in organic liquids (decane, dodecane, etc.) results in dispersion of the gallium into nanometric spheres. These were examined by several analytical methods XRD, DSC, Raman and IR spectroscopy) as well as electron microscopy (SEM, TEM) and found to be composed of Ga and C. The DSC analysis indicates that the Ga has possibly reacted with carbon, while the Raman spectrum of the product demonstrates a strong additional peak that could not be identified. This work explores the possibility that the product is gallium carbide or another gallium‐carbon complex. To investigate the nature of the product, we performed detailed extended X‐ray absorption fine structure (EXAFS) and X‐ray absorption near‐edge structure (XANES) analyses. On the basis of DSC, IR, and Raman it appear to be formation of GaC, whereas the analysis by EXAFS and XANES demonstrated that the gallium is found to be in a higher reduced state (almost metallic), supported by carbon. The question that remains open in addition to the one related to the formation of galium carbide is whether a complex structure, including oxygen contamination is involved in the layers surrounding the Ga as indicated by the EXAFS results. 相似文献
89.
Kayanne P. McCook-Russell Muraleedharan G. Nair Petrea C. Facey Camille S. Bowen-Forbes 《Food chemistry》2012
Psidium cattleianum (strawberry guava) is one of many underutilised edible fruits that grow wild in Jamaica, and could potentially be commercially exploited to yield health and economic benefits. In this study, the total phenolics, proximate contents, and antioxidant, anti-inflammatory, and antimicrobial activities of P. cattleianum and P. guajava (common guava), a well-known species, were compared. Strawberry guavas were found to be superior to common guavas in antioxidant and antimicrobial activities, total phenolics and vitamin C content. They also possessed relatively high fibre content (24.9%). The hexane and ethyl acetate extracts of strawberry guavas showed cyclooxygenase-2 enzyme inhibitory activities of 18.3% and 26.5%, respectively (250 μg/mL), indicating anti-inflammatory activity. The EtOAc and MeOH extracts of P. guajava showed 56.4% (COX-2) and 44.1% (COX-1) inhibitory activity, respectively. Additionally, nine compounds were isolated from strawberry guava fruits, some of which demonstrated anti-inflammatory activity. These results indicate that strawberry guavas are beneficial for health. 相似文献
90.
Microsystem Technologies - In the current paper, a new temperature sensor with improved temperature inaccuracy and with very low power consumption has been designed for avionic industry. The... 相似文献