Effect of Post-weld Heat Treatment on Microstructure and Mechanical Properties of Laser Beam Welded TiAl-based Alloy

Post-weld heat treatment is carried out on the laser beam welded γ-TiAl-based alloy Ti-48Al-1Cr-1.5Nb-1Mn-0.2Si-0.5B (at. pct). The macro/microstructure and mechanical properties of both as-welded and heat-treated specimens are investigated by radiography, SEM, and tensile tests. Moreover, high energy synchrotron X-ray diffraction is performed to measure the residual stresses and evaluate the microstructure evolution. It is found that the residual stresses are distributed in a three-peak shape in the region of the weld zone and heat-affected zone of the as-welded specimen due to the microstructural transformation and heat softening. The residual stresses are largely relieved after the heat treatment. The heat-treated specimens have a near fully lamellar microstructure and show balanced mechanical properties of strength and ductility. The diffraction shows that the phase transformation from α ₂ to γ takes place under tensile load at 1023 K (750 °C), and the grain size and lamellar spacing are refined in the weld zone. Finally, the fracture mechanisms are found to be controlled by the local stress concentration-induced strain misfit between α ₂ and γ phases in the near γ grains and delamination and debonding in the lamellae. Boride ribbons of 5 μm in the near fully lamellar microstructure are found not to be detrimental to the tensile properties.     

Surge arresters for insulation coordination in UHV power systems—related problems and solutions

Surge arresters play an important role in the insulation coordination of ultra high-voltage (UHV) electric power systems. In this contribution the requirements on the surge arresters are discussed in comparison with those in conventional applications, and how surge arrester standards are being changed to cover these special requirements.     

An analysis of the transition proportion for binarization in handwritten historical documents

In this paper, we will present a mathematical analysis of the transition proportion for the normal threshold (NorT) based on the transition method. The transition proportion is a parameter of NorT which plays an important role in the theoretical development of NorT. We will study the mathematical forms of the quadratic equation from which NorT is computed. Through this analysis, we will describe how the transition proportion affects NorT. Then, we will prove that NorT is robust to inaccurate estimations of the transition proportion. Furthermore, our analysis extends to thresholding methods that rely on Bayes rule, and it also gives the mathematical bases for potential applications of the transition proportion as a feature to estimate stroke width and detect regions of interest. In the majority of our experiments, we used a database composed of small images that were extracted from DIBCO 2009 and H-DIBCO 2010 benchmarks. However, we also report evaluations using the original (H-)DIBCO?s benchmarks.     

On the kinetics of AlH3 decomposition and the subsequent Al oxidation

Metal hydrides are used for hydrogen storage. AlH₃ shows a capacity to store about 10 wt% hydrogen. Its hydrogen is split-off in the temperature interval of 400–500 K. On dehydrogenation a nano-structured Al material emerges with specific surfaces up to 15–20 m²/g. The surface areas depend on the heating rate because of a temperature dependent crystallite growth. The resulting Al oxidizes up to 20–25% weight on air access forming an alumina passivation layer of 3–4 nm thickness on all exposed surfaces. The heat released from this Al oxidation induces a high risk to this type of hydrogen storage if the containment might be destroyed, accidentally. The kinetics of the dehydrogenation and the subsequent oxidation is investigated by methods of thermal analysis. A reaction scheme is confirmed which consists of a starting Avrami-Erofeev mechanism followed by formal 1st order oxidation on unlimited air access. The kinetic parameters, activation energies and pre-exponentials are evaluated and can be used to calculate the reaction progress. Together with the heat of the Al oxidation the overall heat release and the related rate can be estimated.     

In-house and interlaboratory validation of a method for the extraction of DNA from maize starch

Here, we describe the procedure of a DNA extraction method from maize starch including the method??s validation by in-house and interlaboratory tests. The amplifiable amount of maize DNA tested by real-time PCR was used as parameter for evaluating our method. The practical (i.e. relative) limit of detection (LOD) was used as key criterion for assessing the suitability of the extraction method with respect to genetically modified organism analysis. In a round-robin test with ten participating laboratories, satisfactory results were achieved with practical LODs in the range of 0.1?% with three native maize starch materials. In-house tests showed that this protocol??with an additional purification step??can also be applied for extracting DNA from chemically or enzymatically modified starch.     

Taking on a wider view: public value interests of construction clients in a changing construction industry

For financial and strategic reasons, public and semi-public construction clients increasingly depend on private parties to carry out public service delivery. They subcontract operational responsibilities to private parties while remaining socio-politically responsible for ensuring public values. Public administration literature mainly addresses the importance of procedural and performance values in safeguarding public values. However, safeguarding the quality of the built environment also requires a focus on product values. In this study, we aim to increase the understanding of the meaning and significance of public values in the daily practice of public construction clients and identify the challenges they face in commissioning these seemingly opposing values. A set of semi-structured interviews with the public administrators of a variety of public and semi-public construction client organizations in the Netherlands shows that both internal and external factors influence the collaborative practices between clients and contractors. This causes a value shift from an emphasis on procedural values to managing performance and product values, indicating that clients need to take on a wider view on public values. Six main public value dilemmas were found that complicate the task of developing an open, transparent and sustainable long-term client–contractor relationship. The current contractual system, however, lacks the flexibility to facilitate this product-based value view in construction.     

Design methodology for barrier‐based two phase flow distributor

The barrier‐based distributor is a multiphase flow distributor for a multichannel microreactor which assures flow uniformity and prevents channeling between the two phases. For N number of reaction channels, the barrier‐based distributor consists of a gas manifold, a liquid manifold, N barrier channels for the gas, N barrier channels for the liquid, and N mixers for mixing the phases before the reaction channels. The flow distribution is studied numerically using a method based on the hydraulic resistive networks (RN). The single phase hydraulic RN model (Commenge et al., 2002;48:345–358) is extended for two phases gas‐liquid Taylor flow. For Re_GL <30, the accuracy for the model was above 90%. The developed‐model was used to study the effects of fabrication tolerance and barrier channel dimensions. A design methodology has been proposed as an algorithm to determine the required hydraulic resistance in the barrier channels and their dimensions. This methodology is demonstrated using a numerical example. © 2012 American Institute of Chemical Engineers AIChE J, 2012