对气体分析仪现状与发展的初步探讨

本文较详细地介绍了氩、氧、水分等几种分析仪器 ,阐述了它们的工作原理、优点、缺点及使用中应注意的问题     

改善GH99合金板材力学性能的研究

GH99合金是时效强化型高温合金，其γ′相的含量决定了力学性能的水平，而合金的Al、Ti含量和板材固溶后的冷却速度是决定γ′相的含量的主要因素。另外，板材晶粒度的大小在一定程度上也会影响其力学性能。本文作者通过对这些原理的研究，摸索出了改善GH99舍金板材力学性能的措施：控制Al=2．0～2．1％、Ti=1．2～1．3％，晶粒度为5～6级；若Al、Ti含量超过这个范围，调整板材的固溶冷却速度和晶粒度可以改善合金的力学性能。     

Derivation of applied stress-crack opening displacement relationships for the evaluation of effective stress intensity factor range

Linear elastic fracture mechanics (LEFM) integrated with the interference of fracture surface asperities has been formulated. The asperities are considered to simulate the influence of the microstructures and possibly oxide debris. The applied stress/load-crack opening displacement (COD) relationships in several cases have been derived. In the original LEFM, the stress-COD relationship is represented by a straight line passing through the origin of the stress-COD plot. The insert of one asperity results in a deviation of the stress-COD response from the LEFM relationship, leading to the exhibition of an inflection point (first contact point, σ_op), a larger slope, and a residual COD. In the case of two asperities, the slope and the residual COD of the stress-COD relationship become further larger, and two inflection points emerge. A general stress-COD expression in the case of multiple asperities has been derived. The slope of the stress-COD equation, the residual COD, and the minimum COD all increase with increasing number of asperities for a given loading condition, resulting in a smaller ΔCOD and Δσ_eff. The number of the inflection points is the same as that of the asperities. To the authors' knowledge, this paper is the first to derive analytically an applied stress-COD curve with a gradual variation below σ_op, caused by the asperity-/roughness-, or oxide-induced crack closure.     

Structure, Phonon Vibration, and Spin Correlation of LaBa2Cu3−x Co x O y

Polycrystalline samples LaBa₂Cu_3?xCo _x O _y (0 ≤ x ≤ 1.0) were synthesized by solid state reaction method. The structure, phonon vibration, conduction, and spin correlation were investigated by means of X-ray diffraction, infrared spectra, resistivity, and electron spin resonance. It is found that there are orthorhombic–tetragonal and tetragonal–orthorhombic structural transitions with Co doping, and the conduction behavior changes from metallic to semiconducting. With the increase of Co content, the Cu(1)—O(1) phonon mode around 531 cm^?1 softens, the Cu(2)—O(2) phonon mode around 657 cm^?1 hardens, and the Cu(1)—O(4) mode around 583 cm^?1 is nearly unchanged. The Cu²⁺ spins tend to localize with Co doping. The changes in structure, phonon vibration, and spin correlation with Co doping are analyzed and discussed.     

Growth and optical properties of Er,Yb:YAl3(BO3)4 crystal

Single crystal of erbium, ytterbium-codoped yttrium aluminum tetraborate Er,Yb:YAl₃(BO₃)₄(Er,Yb:YAB) has been grown by the flux method. The absorption spectrum in the visible and NIR regions of Er,Yb:YAl₃(BO₃)₄ crystal are measured at room temperature and fluorescence spectrum of Er,Yb:YAl₃(BO₃)₄ crystal are also measured at room temperature, excited by 976 nm laser. Not only the strong NIR emission peaks located at 1548 nm was observed, but also the visible up-conversion luminescence has been found. The specific heat of the Er/Yb:YAB crystal at room temperature is 0.81 J/g °C.     

265m2烧结主传动柔性减速机受力分析及改造

针对天钢集团公司炼铁厂烧结车间265m^2烧结机主传动柔性减速机出现的吊挂滚动轴承损坏和传动异响问题，分析了烧结机传动装置定位轴承受力情况，找出产生故障的原因，提出具体的改进措施和改造方案。经实践表明，效果良好。     

V-Nb微合金高强度热轧H型钢桩BS 55C的开发

马钢用60 t顶底复吹转炉冶炼,钢包炉吹氩、喂线和成分微调,异型坯(mm750×450×120)弧形连铸和H型钢万能轧机轧制工艺研制了碳当量Ceq≤0.42%的V-Nb微合金高强度热轧H型钢(%)0.14～0.17C,0.43～0.55Si,1.28～1.45Mn,0.010～0.028S,0.010～0.027P,0.03～0.05Nb,0.08～0.12V.检验统计数据表明,BS 55C热轧H型钢组织为铁素体+珠光体,实际晶粒度9级,屈服强度均在420 MPa以上.