High-efficiency ammonium polyphosphate intumescent encapsulated polypropylene flame retardant

The flame retardant polypropylene containing the micro-envelope core-shell structure flame retardant, which encapsulated ammonium polyphosphate into melamine-formaldehyde resin and sodium silicate through in situ polymerization was prepared with polyamide 6, added as a carbon-forming agent. The composition of ammonium polyphosphate, encapsulated ammonium polyphosphate with melamine-formaldehyde resin and the micro-envelope core-shell structure flame retardant were characterized. The fire safety and thermal stability were investigated and showed an improvement including limiting oxygen index, thermogravimetric analysis, vertical burning tests, and microscale combustion calorimeter. The burned compounds were also studied to confirm the burning mechanism. The results showed the flame retardant performance had been greatly improved, while polyamide 6 had better char-forming effect. Besides, the water solubility of flame retardants and their influence on the mechanical properties of polypropylene were also investigated. The results on the effects of additives demonstrated a high efficiency flame retardant to polypropylene. A core-shell flame retardant that sodium silicate and melamine-formaldehyde resin-coated ammonium polyphosphate had been constructed. The effect of the built flame retardant system on the combustion performance of polypropylene was studied from the mechanism and performance. The LOI of the most flame retardant polypropylene reached 28.6%, and UL-94 reached the V-0 level.     

反向工程中测量点云配准的新方法

在光学非接触三维测量中，复杂对象的重构需要多组测量数据的配准。为了获得好的配准结果，提出一种新的配准方法——直接误差分析配准方法。该方法基于一种新型的双目CCD光栅投影测量系统进行测量和分析。实验结果表明该测量方法的配准误差大约0．2mm左右．从而证实该方法的可行性。     

新型节能防触电交流弧焊机

提出一种用可控硅代替节能开关中的接触器的节能防触电交流弧焊机。该机引弧动作快,有较好的焊接适应性,为造船、建筑、桥梁和矿山等工业部门提供了较理想的交流弧焊机。     

自动金刚石刀头磨弧机

针对采用激光焊接工艺的金刚石锯片上，其金刚石刀头内弧面需要磨抛的工艺要求，研发了一种自动金刚石刀头磨弧机。该设备将金刚石刀头放置在作间歇回转的工作转盘上，工作转盘由槽轮机构驱动；磨削砂轮安装在拖板系统上，拖板的间歇往复运动由一种在滑块上开有长槽的曲柄滑块机构实现，可满足工作转盘转位时，拖板停歇；工作转盘停歇时，拖板运动的工作要求。用靠模控制砂轮磨削的进给量。通过靠模的更换及设计能快速装卡的刀头夹具，可实现对不同弧度刀头的磨弧。本文介绍了该设备的结构组成、设计参数的选择及相关的设计方案，并对在滑块上开有长槽的曲柄滑块机构的设计方法进行了详细地讨论。     

放电等离子烧结法制备二硼化钛多孔陶瓷

以二硼化钛微粉为原料，采用放电等离子烧结技术，通过控制烧结温度、保温时间、施加压力等工艺参数，成功的制备出具有高强度和高气孔率的二硼化钛多孔陶瓷。采用浸泡介质法，三点弯曲法测试了材料的气孔率，开口气孔率及强度；用扫描电镜对材料断口进行了观察。实验结果表明：在1300-1500℃的烧结温度下，获得了气孔率33％～45％，最大抗弯强度〉60MPa的二硼化钛多孔陶瓷。扫描电镜结果显示，二硼化钛颗粒间有明显的颈部烧结。     

MODELLING OF P/M FORMING PROCESSES BY FEM

ＭＯＤＥＬＬＩＮＧＯＦＰ／ＭＦＯＲＭＩＮＧＰＲＯＣＥＳＳＥＳＢＹＦＥＭ￥Ｗｅｉ，Ｙｕａｎｐｉｎｇ；Ｒｕａｎ，Ｘｕｅｙｕ（ＤｅｐａｒｔｍｅｎｔｏｆＰｌａｓｔｉｃｉｔｙＴｅｃｈｎｏｌｏｇｙ，ＳｈａｎｇｈａｉＪｉａｏＴｏｎｇＵｎｉｖｅｒｓｉｔｙ，Ｓｈａｎｇ...     

RH—KIP双重精炼工艺对钢中夹杂物的影响

本文讨论了RH-KIP双重精炼工艺对钢中夹杂物的影响。结果表明,无论采用RH→KIP还是KIP-RH处理工艺均能使钢液净化和夹杂物良好球化,但前一种工艺易使钢中产生较大颗粒夹杂物。     

基于特征模板的分组编程法

介绍了国内数控加工中存在的问题，结合广东省科委项目，提出了基于平面、曲面特征模板的分组加工编程法，并用实例验证了这种方法的正确性，极大地提高UG软件的加工编程效率，也解决了加工编程难以掌握的问题。     

正向充液变薄拉深工艺的研究

提出了一种称为正向充液变薄拉深的工艺方法。从理论上推导出变薄成形传力区拉应力计算式，并采用软铝车削毛坯进行了正向充液变薄拉深试验。当液压达到了１２０ＭＰａ时，车削铝毛坯的极限变薄拉深系数由０．５减小到０．３，说明正向充液变薄拉深工艺能有效地提高一次变薄拉深成形极限。     

Microstructures of mechanically activated Ti-46at.% Al powders and spark plasma sintered ultrafine TiAl alloy

Powder of Ti-46at.%Al was synthesized through mechanical activation (MA) for different milling times, and the 16 h MAed powder was sintered by using a spark plasma sintering (SPS) process at different sintering temperatures. The XRD profiles showed that the MAed Ti-46at%Al powder for 12,16, and 20 h contained initial α-Ti and Al phases, and that the SPSed TiAl alloys contained the gamma TiAl and α2-Ti3Al phases. The TEM showed two different types of regions in the 16 h MAed Ti-46at.%Al powder. One type consisted of only Al with a grain size about 80 nm, and the other type a mixture of Al and Ti with a grain size of 30 nm. According to the optical micrographs of MA-SPSed samples, the alloys sintered at higher temperatures showed a coarser microstructure. In the case of the 1473 K sintering, typical duplex structures ((α2 + γ) lamella and γ phases) with interlamellar spacings of 50-400 nm and the grain size either less man 100 nm, or 1000 nm were observed.