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51.
Biodegradable multiblock poloxamers (BMPs) with gel duration of 8 h to several weeks were prepared by varying their molecular weights from 4000 to 40 000 g mol?1. The molecular weight of the BMP was controlled by changing the poloxamer to coupling agent ratio. Assuming a micelle packing model of the BMP gel, as in the case of a poloxamer gel, the micelle properties and critical gel concentration of BMPs were investigated on the basis of the scaling concept. The findings suggest that the control of molecular weight by hydrolyzable groups can be a facile approach to optimize the gel properties for biomedical applications. Copyright © 2005 Society of Chemical Industry 相似文献
52.
A set of six coals ranging in rank from lignite to hvA bituminous was swollen with a series of alkyl-substituted pyridines and a smaller set of 4-alkylanilines. The size and branching of the alkyl groups was varied and the effect of this variation on the dissolution of the amines in the coal and the resulting coal swelling was measured volumetrically. In a few cases, substituents which hindered the amine nitrogen were studied. The lignite and subbituminous coal have a much higher tolerance to branched, bulky groups than do the bituminous coals. The presence of tertiary groups in a solute strongly inhibits their dissolution in bituminous coals. Bituminous coals behave as if extensive parallel packing of structures occurs. Often, they can accept very large planar groups but have a low capacity for branched groups. 相似文献
53.
A multi-channel continuous toxicity monitoring system developed in our laboratory, based on two-stage mini-bioreactors, was successfully implemented in the form of computer-based data acquisition. The multi-channel system consists of a series of a two-stage minibioreactor systems connected by a fiber optic probe to a luminometer, and uses genetically engineered bioluminescent bacteria for the detection of the potential toxicity from the soluble chemicals. This system can be stably and continuously operated due to the separation of the culture reactor from the test reactor and accomplish easy and long-term monitoring without system shut down by abrupt inflows of severe polluting chemicals. Four different recombinant bioluminescent bacteria were used in different channels so that the modes of the samples toxicities can be reasonably identified and evaluated based upon the response signature of each channel. The bioluminescent signatures were delivered from four channels by switching one at once, while the data is automatically logged to an IBM compatible computer. We also achieved the enhancement of the system through the manipulation of the dilution rate and the use of thermo-lux fusion strains. Finally, this system is now being implemented to a drinking water reservoir and river for remote sensing as an early warning system. 相似文献
54.
The influence of liquid penetration at grain boundary regions on the rate of advance of the solid-liquid interface during
isothermal solidification of transient liquid phase (TLP) brazed nickel joints has been examined. The test samples used in
this study were Ohno-cast nickel with a grain size of >4 mm and a fine-grained nickel with a grain size of around 40 μm. Both
Ni-base materials had the same chemical composition. The rate of isothermal solidification was greater when fine-grained nickel
was employed during TLP brazing using Ni-11 wt pct P filler metal at 1200 °C. Liquid penetration at grain boundaries accelerates
the isothermal solidification process by increasing the effective solid-liquid interfacial area and increasing the rate of
solute diffusion into the base material. An analysis of electron channeling patterns has confirmed that random high-angle
boundaries have a greater influence on the rate of isothermal solidification than ordered boundaries including small-angle
or twin boundaries.
Formerly Visiting Scientist, Department of Metallurgy and Materials Science, University of Toronto.
Formerly Postdoctoral Fellow, Department of Metallurgy and Materials Science, University of Toronto 相似文献
55.
Trieu-Kien Truong Yaotsu Chang Yan-Haw Chen Lee C.D. 《Communications, IEEE Transactions on》2005,53(5):749-754
In this paper, two algebraic decoders for the (103, 52, 19) and (113, 57, 15) quadratic residue codes, which have lengths greater than 100, are presented. The results have been verified by software simulation that programs in C++ language have been executed to check possible error patterns of both quadratic residue codes. 相似文献
56.
Jong-Hwan Kim Yeon-Chan Hong Sung-Jun Lee Keh-Kun Choi 《Industrial Electronics, IEEE Transactions on》1989,36(3):361-364
A direct adaptive control scheme is proposed for nonminimum-phase systems in which controller parameters are estimated from the recursive least-squares algorithm and additional auxiliary parameters are obtained from the proposed polynomial identity. A local convergence is guaranteed without any extra condition. Integral action is incorporated into the adaptive controller to eliminate the steady-state error and to satisfy a condition of the unique solution for the polynomial identity. The control law used in this scheme is based on the set-point-on-I-only proportional-integral-derivative (PID) structure 相似文献
57.
Zirconium(IV) tungstoiodophosphate has been synthesized under a variety of conditions. The most chemically and thermally stable
sample is prepared by adding a mixture of aqueous solutions of 0·5 mol L−1 sodium tungstate, potassium iodate and 1 mol L−1 orthophosphoric acid to aqueous solution of 0·1 mol L−1 zirconium(IV) oxychloride. Its ion exchange capacity for Na+ and K+ was found to be 2·20 and 2·35 meq g−1 dry exchanger, respectively. The material has been characterized on the basis of chemical composition, pH titration, Fourier
transform infrared spectroscopy (FTIR) and thermogravimetric analysis. The effect on the exchange capacity of drying the exchanger
at different temperatures has been studied. The analytical importance of the material has been established by quantitative
separation of Pb2+ from other metal ions. 相似文献
58.
Jonathan P. Belnoue Giang D. Nguyen Alexander M. Korsunsky 《International Journal of Fracture》2007,144(1):53-60
This paper presents a new 1-D non-local damage-plasticity deformation model for ductile materials. It uses the thermodynamic
framework described in Houlsby and Puzrin (2000) and holds, nevertheless, some similarities with Lemaitre’s (1971) approach.
A 1D finite element (FE) model of a bar fixed at one end and loaded in tension at the other end is introduced. This simple
model demonstrates how the approach can be implemented within the finite element framework, and that it is capable of capturing
both the pre-peak hardening and post-peak softening (generally responsible for models instability) due to damage-induced stiffness
and strength reduction characteristic of ductile materials. It is also shown that the approach has further advantages of achieving
some degree of mesh independence, and of being able to capture deformation size effects. Finally, it is illustrated how the
model permits the calculation of essential work of rupture (EWR), i.e. the specific energy per unit cross-sectional area that
is needed to cause tensile failure of a specimen. 相似文献
59.
Yewang Su Baohua Ji Yonggang Huang Kehchih Hwang 《Journal of Materials Science》2007,42(21):8885-8893
Wet adhesion is widely adopted in biological adhesion systems in nature. Wet adhesion is studied in this paper with the focus
on the effect of different contact shapes (flat, concave, convex, and ring-like) on the adhesion force. The evolution of the
liquid bridge between a fiber tip and substrate during the detaching process shows two transition points. The first transition
from the radius-controlled to the contact-angle controlled process is critical to influence the strength and robustness of
adhesion. We show that a concave shape is more effective than a flat one, while a convex shape has no advantage. A ring-like
contact shape has advantages in a hydrophobic environment and on a rough surface. 相似文献
60.
Irine Banu Lucy 《Journal of Materials Science》2007,42(14):5875-5879
Capacitance and dielectric loss measurements were carried out using an Al/Cu–GeO2/Al sandwich structure for 0 to 10 vol% Cu films, 120–400 nm thick, deposited at 0.4–1.5 nm/s in the frequency and temperature
range 1–106 Hz and 90–573 K, respectively. The variation of capacitance and dielectric loss with frequency and temperature follows the
Goswami and Goswami model. Capacitance decreases slowly with increasing thickness and also varies with the change in deposition
rate of the cermet film. 相似文献