大孔强酸树脂吸附硫脲金

研究了D072大孔强酸性阳离子交换树脂从硫脲[Tu=CS(NH2)2]浸金液中吸附Au(Tu)2+的性能和机理. 结果表明，pH=2.0时，树脂对Au(Tu)2+有优良的吸附性能，金的交换容量为78.95 mg/g (Au/干树脂)，吸附的硫脲金可用乙醇-硫酸水溶液洗脱，洗脱率可达96.5%. D072树脂对Au(Tu)2+的吸附符合Langmuir吸附模型.     

<Emphasis Type="Italic">Penicillium</Emphasis> sp. ZD-Z1 chitosanase immobilized on DEAE cellulose by cross-linking reaction

Chitosanase obtained fromPenicillium sp.ZD-Z1 was immobilized on DEAE cellulose with glutaraldehyde by cross-linking reaction. The optimal conditions of immobilization were as follows: 0.1 g DEAE cellulose was treated with 5 ml 5% glutaraldehyde solution; then 2.3 mg chitosanase was immobilized on the carrier. The optimal temperature and pH was 60 °C and 4.0, and the K _m value was 18.87 g/L. Under optimal conditions, the activity of immobilized enzyme is 1.5 U/g, and the recovery of enzyme activity is 81.3%. After immobilization, the optimal temperature and K _m value increased (from 50 °C to 60 °C, from 2.49 g/L to 18.87 g/L), whereas the optimal pH was reduced (from 5.0 to 4.0). The enzyme activity loss was less than 20% after 10 times batch reaction; the immobilized enzyme showed good operation stability.     

Polyurethane–urea anionomer dispersions. I

Polyurethane–urea anionomer dispersions with different stoichiometric DMPA/polyol and NCO/OH ratios were preapred from poly(oxypropylene)glycol, toluene diisocyanate (TDI), dimethylolpropionic acid (DMPA), and ethylenediamine (EDA). The dispersion-cast films were prepared and characterized by mechanical properties, dynamic mechanical analysis (DMA), and differential scanning calorimetry (DSC). Increasing the hard-segment content by either increasing the DMPA/polyol or the NCO/OH ratios affects the glass transition temperature (T_g) of the soft segments. © 1994 John Wiley & Sons, Inc.     

三维编织复合材料编织工艺过程仿真研究

总结了四步编织工艺的运动规律。对纱线的空间坐标进行三次B样条曲线拟合得到拟合坐标;设计实现了纱线实体的静态模型算法,根据拟合坐标得到纱线空间网格坐标并建立了纱线实体的静态模型;实现了纱线轨迹的动态展示以及实体生成过程的动态展示;构建了GUI界面并编译成了可脱离Matlab环境的独立运行程序。     

基于HLA的分布式仿真框架自动生成技术

针对基于HLA仿真应用系统开发中存在的计算模型程序与RTI服务程序的耦合问题,研究了基于共享内存和中断回调技术的解耦方法,进一步采用HLA仿真适配器对RTI服务程序进行封装,从而实现了计算模型程序与RTI底层服务程序的有效隔离。为提高仿真应用程序开发效率,分析了联邦成员中RTI服务程序功能需求,研究实现了仿真适配器自动生成软件。该软件可快速生成基于HLA的联邦成员适配器代码和执行程序,从而构建仿真应用系统分布式仿真框架。     

基于ASL的模型驱动架构测试方法

针对模型驱动架构（MDA）下的软件开发方法中测试启动比较晚、难以发现隐藏在模型中的缺陷及UML模型描述缺乏精确语义等问题,提出了基于ASL的模型测试方法：从UML模型出发,将动作规约语言（ASL）运用于平台无关模型（PIM）上建立测试模型。给出了ASL语句在MDA过程中的工作原理、平台无关模型的建立过程、测试用例建立的步骤、测试执行的实施过程,最后结合实例,在UML图的基础上运用ASL对测试环境进行构建,并创建了系统的测试用例,对模型及业务逻辑进行了测试。实验结果表明,提出的基于ASL的模型测试方法既能利用模型驱动对复杂的测试用例进行简化和抽象,又能在软件生存期早期揭示软件的缺陷,防止缺陷随着软件开发过程的进行而被放大。     

创新型嵌入式实验教学模式研究

结合军校计算机专业人才培养的具体需求,深入阐述了嵌入式计算机实验教学模式面临的问题,分析了当前军队院校实验教学现状及存在的不足,提出了嵌入式计算机实验教学的改革措施和原则,最后给出了发展创新型实验教学模式的思路。     

基于改进型批决策与调度建模的生产计划调度系统的研究

热轧型钢生产工艺复杂,其生产中极易出现由于计划调度安排不当而产生的交货期延误、库存超负荷等问题。针对以上问题研究设计了MES生产计划调度系统,改进了批决策调度策略用于数学建模,利用自适应遗传算法求解生产调度计划。以此为基础,为某热轧企业设计实现了生产计划调度系统,并通过真实的热轧型钢订单、原料、设备等数据,对模型改进前后的计划编制方法进行模拟与比较,验证了利用该改进型批决策与调度模型编制的热轧型钢生产调度计划可节省生产时间、降低设备调度时间,以此来指导热轧型钢的生产可切实减少交货延误和减少库存占用率,并提高企业利润率。     

Preparation and characterization of carboxymethyl konjac glucomannan/sodium montmorillonite hybrid films

Carboxymethyl konjac glucomannan (CKGM)/ sodium montmorillonite (MMT) hybrid films of various compositions were prepared by casting from a polymer/silicate water suspension. The structure and properties of the hybrid films were investigated by wide angle X‐ray diffraction (WAXD), transmission electron microscopy (TEM), attenuated total reflection infrared spectroscopy (ATR‐IR), differential scanning calorimetry (DSC), and tensile tests. The results from WXRD and TEM indicated that an intercalated CKGM/MMT nanocomposite film was obtained by polymer solution intercalation. WXRD and DSC showed that the high‐T_m crystal phase was induced by the presence of lower MMT loading, but the T_m of the hybrid films became weak with the increase of MMT content due to the polymer confinement. The hybrid films showed higher thermal stability and mechanical properties than that of the neat polysaccharide due to the strong interaction between hydroxyl and carbonyl group of CKGM and the silicate layer of MMT. Furthermore, the degree of swelling of the hybrid films was investigated in acidic buffer solutions. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 103: 2954–2961, 2007     

Adhesion properties of UV crosslinked polystyrene-block-polybutadiene-block-polystyrene copolymer and tackifier mixture

The peel and tack properties of mixtures of polystyrene-block-polybutadiene-block-polystyrene (SBS) and a tackifier were investigated after these were crosslinked by ultraviolet (UV) irradiation at various amounts of benzophenone (BP) as a photoinitiator and trimethylolpropane mercaptopropionate (TRIS) as a crosslinking agent.The degree of crosslinking of polybutadiene (PB) block in the SBS mixture was qualitatively estimated from the amount of gel fraction as well as the change in the glass transition temperature of the PB block. The crosslinking of the PB block was done within 3 min after UV irradiation and the peel strength of crosslinked specimens was as low as 45[percnt] of specimens without crosslinking. Nano-tack and bulk tack properties as well as the surface tension of mixtures were measured depending upon amounts of BP and TRIS.