高岭土在碳热还原氮化过程中的相变

系统研究了苏州高岭土碳热还原氮化合成SiAlON过程在不同温度下的相变。对试样的XRD、SEM以及EDXA分析结果表明 ,1 30 0℃之前 ,试样中没有氮化物生成 ,物相为莫来石、石英和方石英 ;1 30 0℃时 ,高岭土开始发生氮化反应 ,生成过渡型SiAlON和β SiAlON。此时 ,石英和方石英相基本消失 ;1 4 0 0℃时 ,过渡型SiAlON、β SiAlON和X SiAlON三相共存 ,β SiAlON有所增多并有少量刚玉相生成 ;从 1 4 50℃到 1 550℃ ,Z值为 3的β SiAlON成为惟一的氮化产物 ,与少量SiC和刚玉相并存。莫来石在 1 50 0℃时完全消失     

Increased α-linolenic acid intake increases tissue α-linolenic acid content and apparent oxidation with little effect on tissue docosahexaenoic acid in the guinea pig

The essential fatty acids do not have identical roles in nutrition. Linoleic acid (LA) accumulates throughout the body of most mammals, whereas α-linolenic acid (ALA) is rarely found in tissue lipids to the same extent as LA. It has been argued that this is the result of metabolism of ALA to docosahexaenoic acid (DHA) or that ALA is rapidly β-oxidized to acetyl CoA and CO₂. In this study, we consider the effect of high and low ALA levels on the tissue distribution of ALA and other n-3 polyunsaturated fatty acids (PUFA) in all tissues. Guinea pigs were fed one of two defined diets for 3 wk from wearning with both diets containing 1.8% (by weight) of LA and either 1.7% ALA or 0.03% ALA. The high ALA diet was associated with significantly increased ALA levels in all tissues except the brain and significantly increased levels of long-chain n-3 PUFA in all tissues except intestines, brain, carcass, and skin. The long-chain n-3 PUFA content of the whole body was less than 5% of that of the ALA content in both diet groups, and the major long-chain n-3 PUFA (>66% of total) in the body was 22∶5n−3. The brain was the only tissue where the DHA content exceeded that of 22∶5n−3. On the low ALA diet, there appeared to be conservation of ALA based on a comparison of the ratio of LA to ALA in the tissues compared with that in the diet. On the high ALA diet there was a loss of ALA relative to LA in the tissues compared with the diet. These studies suggest that the low levels of tissue ALA in the guinea pig are likely the result of β-oxidation or excretion via the skin and fur rather than metabolism to DHA.     

填充母料及其他常用塑料母料

塑料母料对推动塑料工业的迅猛发展起了很大作用，其主要特点是：可以简化生产工艺过程：原料混合方便，混炼质量均匀，提高生产效率及制品性能指标；减少粉尘飞扬及对设备的磨损；降低制品在换色时清洗螺杆的用料量；延长原料储存的保质期等。     

锆莫来石材料的反应烧结机制和显微结构特征

研究了用锆英石和工业氧化铝合成锆莫来石材料的反应烧结过程和显微结构。结果表明，添加适量ＭｇＣｌ２·６Ｈ２Ｏ可以促进反应烧结进程。锆英石大颗粒完全分解以后形成ＺｒＯ２聚集体，结构中出现封闭气孔可能与ＺｒＯ２聚集体有密切关系。加入ＭｇＣｌ２·６Ｈ２Ｏ后锆莫来石材料显微结构的主要特征：ＺｒＯ２有聚集体和均匀分布两种赋存形式；封闭气孔一般与ＺｒＯ２聚集体相邻。     

基于大数据背景下的企业生态系统架构研究

随着全球网络技术与移动通信设备的融合发展,“大数据”时代已经引起社会各界的重点关注。苹果、三星、华为、IBM、微软、腾讯等国际知名企业都开始建构出“大数据”时代的企业生态系统。本文将对“大数据”时代的企业生态系统的演化和建构进行深入分析。     

悬浮液进样-火焰原子吸收光谱法测定茶叶中的微量铬

将茶叶悬浮于琼脂胶体中制成悬浮液 ,直接喷入空气 -乙炔火焰 ,用火焰原子吸收光谱法测定茶叶中的微量铬 ,方法简便、快速、灵敏度和精密度高、测定结果与用灰化法处理样品一致 ,检验表明 ,两种样品前处理方法之间无显著性差异。相对标准偏差为 3.4 %～ 6 .1% ,加标回收率为 95 .7%～ 10 3.8 %。     

赫尔巴特管理论与高校教学管理改革

赫尔巴特的教育管理思想是传统教育管理理论的基础,对推进高校教育管理体制改革有一定的借鉴意义。剖析高校教学管理上存在的主要问题,提出从管理观念、硬件设备、管理人员三方面入手进行改进。     

整合在信息技术环境下的接受性教学模式

信息技术与课程整合是当前信息技术教育普及进程中的一个热点问题,在我们国家,接受性教学模式还大量存在,合理有效地利用信息技术的优势来克服传统教学模式的弱点,提高教学效率.     

Effects of Copper Coating on the Crystalline Structure of Fine Barium Titanate Particles

We have investigated the effect of a metal coating—copper—on the tetragonal structure of fine barium titanate (BaTiO₃) particles. The BaTiO₃ particles were synthesized by a sol-gel method and heat treated at temperatures >900°C for various amounts of time before coating. The copper coating was achieved by an electroless coating technique. The transmission electron microscopy micrographs revealed that the coated powder contained fine BaTiO₃ particles that were embedded in copper patches. The X-ray diffractometry patterns showed that the copper coating increased the c/a ratio of the fine BaTiO₃ particles. For powders that were heat treated at 900°C for 10 h and were initially cubic, the copper coating changed the c/a ratio, from 1 to 1.0034. For powders that were calcined at 900°C for 20 h and were initially tetragonal, the copper coating further enhanced the c/a ratio, from 1.0028 to 1.0043. When the copper-coated BaTiO₃ particles were oxidized, the c/a ratio was reduced to a value that was approximately equal to or below that of the uncoated powders. A conductive coating can eliminate the depolarization energy of an insulating polar particle. The fact that the copper coating promoted the polar tetragonal phase but the nonconductive copper-oxide coating did not was consistent with the interpretation that the presence of the cubic phase (nonpolar) in small BaTiO₃ particles was caused by the depolarization effect.