生物降解型聚碳酸顺丁烯二酸亚乙酯 1、合成和表征

用CO_2、环氧乙烷、顺丁烯二酸酐进行三元共聚首次得到聚碳酸顺丁烯二酸亚乙酯(PECM),并用IR、~1H NMR、DSC等进行了表征,共聚物链中CO_2和MA单元随机分布,不饱和单元可在0～0.5mol分数之间调节。共聚过程不发生双键交联和构型转化。环氧乙烷的转化率可高达到93％。控制PECM链上的双键含量并使之发生自由基加成反应,得到对热较稳定的可溶性产物。     

含淀粉聚乙烯膜的时控光降解研究

使用复合光降解剂，得到了可光降解的生物降解膜。对膜的光降解进行了考察，并对影响光降解的因素进行了讨论，结果表明，我们所制得的膜是一种较好的时控光降解膜。     

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本文提出了油井稳定生产状态下的脉冲试井数学模型,利用时间和空间叠加原理求得其解析解。并用非线性回归分析方法来进行脉冲试井分析。     

高频脉冲微束等离子电弧温度场的测试及分析

本文首次采用单波长激光干涉技术，对恒定直流和高频脉冲电流微束等离子电弧温度场进行了测试，并做了分析比较。以电弧温度分布为基础分析了高频脉冲电流微束等离子电弧收缩、稳定的原因。     

局域网服务器缓冲区容量的Petri网设计方法

本文在分析局域网服务器信息缓冲区、数据包接受和发送缓冲区的相互关系基础上提出一种新的局域网服务器缓冲区设计方法─—广义随机Ｐｅｔｒｉ网方法，并给出了局域网服务器信息缓冲区的广义随机Ｐｅｔｒｉ网模型。该设计方法理论完备、严谨实用，且不再局限于追求某一边界值（上限或下限），并且避免了排队理论处理多级服务的繁琐公式。最后本文用一例题说明了这种方法的应用。     

Influences of artificial pre-stressing on ply stresses and tensile properties of Vinylon fibre-reinforced aluminium laminates (VIRALL)

A simple micromechanical model based primarily upon the rule-of-mixtures is developed which allows prediction of the effects of fibre preload on the ply stresses (i.e., the initial residual stresses of fibre, adhesive and matrix) induced within VIRALL laminates, and the tensile stress-strain curves and mechanical properties of VIRALL laminates. The analysis of the ply stresses of VIRALL laminates indicates that pre-stressing will dramatically influence the ply stresses. The predicted tensile stress-strain curves of VIRALL laminates are in good agreement with the experimental curves and the results show that the stress-strain curves of VIRALL laminates move upwards when the prestress increases. The predicted tensile mechanical properties of VIRALL laminates at room temperature show good agreement with those obtained experimentally; both show that prestress can improve the tensile properties (i.e., elastic limit strength, 0.2% yield strength and failure strength) of VIRALL laminates.     

Synthesis of ultrafine LiCoO2 powders by the sol-gel method

Ultrafine high-temperature (HT) LiCoO₂ powders were synthesized by the sol-gel method using polyacrylic acid (PAA) as a chelating agent. The decomposition process of the gel precursor was examined to determine the crystallization temperature and the dependence of the physicochemical properties of HT-LiCoO₂ powders on the PAA quantity was extensively investigated. Polycrystalline HT-LiCoO₂ powders, composed of very uniformly sized ultrafine particulates with an average particle size of 30–50 nm and a specific surface area of 2.3–17 m²g^–1, could be obtained at the lower calcination temperature of 550 °C and the shorter calcination time of 1 h compared to the solid-state reaction.     

化学镀SiCp／Ni－P复合镀层与基体结合强度及其影响因素

论述了ＳｉＣｐ／Ｎｉ－Ｐ复合镀层与钢基体的结合强度及其影响因素。复合镀层中离界面５μｍ厚度以内区域的组成及应力状态对镀层／基体的界面结合有决定性作用，在该区域以外ＳｉＣ粒径变化不影响镀层的结合强度。适当的热处理可提高界面结合力。     

电子型／离子型导电高分子共混物

用苯胺在酸性水溶液中的进行化学氧化聚合合成了能溶于Ｎ－甲基吡咯烷酮的高分子量聚苯胺（ＰＡｎ），并用这种ＰＡｎ与一种高分子固态离子导体－－聚乙二醇聚醚氨酯脲（ＰＥＵＵ）和ＬｉＣｌＯ４的复合物（ＰＥＵＵ－ＬｉＣｌＯ４）进行溶液共混制得了具有电子型／离子型两种导电功能的新型高分子共混物。用差示扫描量热法、动态粘弹仪、应力－应变试验、四探针法和交流阻抗谱对这种高分子共混物进行研究。实验结果表明，上述ＰＡｎ