Synthesis of TiO<Subscript>2</Subscript> Hybrid Molecular Imprinted Polymer for Ethofumesate Linked by Silane Coupling Agent

TiO₂ hybrid molecular imprinted polymer (MIP) for ethofumesate using methacrylic acid (MAA) as the functional monomer and silane coupling agent 3-(trimethoxysilyl) propylmethacrylate (KH570) as organic–inorganic connective bridge was synthesized via photo-excitation method. Hydrogen bond was proved to act between MAA and ethofumesate for pre- and post-polymerization binding properties as testified by UV spectrometric method. KH570 modified TiO₂ nanoparticles were prepared via sonochemical reaction, which can accelerate hydrolysis, increase collision chance for the reactive system and improve the dispersion of the nanoparticles. Scanning electron microscope (SEM), transmission electron microscope (TEM), binding and the adsorption kinetics experiments as well as thermogravimetric analysis (TGA) were employed for characterization. The results indicated that the hybrid MIP revealed a larger surface area and more ordered imprinting cavities with improved thermal stability compared to organic-only MIP. Furthermore, faster adsorption kinetics and enhancive adsorption capacity were achieved, which made it promising in chemical sensor applications.     

Growth of highly orientated strontium barium niobate thin films on Si substrates through the sol–gel process using a K: SBN template layer

We report the growth of highly C-axis orientation of Sr _x Ba_1−x Nb₂O₆ (SBN) thin films on p-type (100) Si substrates by using a potassium-substituted SBN template layer with the sol–gel method. The crystallization of SBN thin films was found closely related to the potassium ion doping concentration and the postannealing temperature of the K-SBN template layer. Secondary ion mass spectrometry analysis showed that potassium elements were accumulated at the interface of the template layer and silicon substrate. SBN films postannealed at 750 °C with K-SBN template layer has a smaller full width at half maximum of X-ray rocking curve of 2.45° than that of 5.40° for the pure SBN films. By introducing a template layer, the surface morphologies of SBN films fabricated on silicon substrate were greatly improved.     

赴日无线电监测技术考察报告

首先介绍了日本总务省关东综合通信局电波监理部的情况，然后对日本安立公司生产的RR510A型无线电监测接收机和技术参数以及MS8609A型数字移动无线发射机测试仪的功能进行了分析和介绍。     

广州地铁二号线民用移动通信工程简介

简单介绍了广州地铁二号线民用移动通信工程概况，并就地铁民用移动通信系统引入地铁的主要技术难点进行了论述。     

On a three-dimensional axisymmetric boundary-value problem of nonlinear elastic deformation: Asymptotic solution and exponentially small error

In this paper, we study a three-dimensional axisymmetric boundary-value problem of a slender cylinder composed of a nonlinearly elastic material subjected to an axial force. Starting from the field equations, after a transformation and proper scalings, we identify a small variable and two small parameters, which characterize the present problem. Then, by an approach involving compound series-asymptotic expansions, a nonlinear ODE is derived, which governs the axial strain (the first-term in the series expansion). By imposing the zero radial displacement conditions at two ends, we manage to get the analytical solution of the axial strain, from which all other physical quantities can be deduced and thus the three-dimensional displacement field can be determined. Graphical results are presented, which show that there are two boundary layers near the two ends while the middle part is in a state of almost uniform extension. The asymptotic structure of the analytical solution is derived, which offers clear explanations to the structure of the deformed configuration and shows that the thickness of both boundary layers is of the order of the radius. We also point out the relevance of the present results to the St. Venant’s problem. In particular, we obtain the explicit uniformly-valid exponentially small error term, when the obtained deformed configuration is compared to the configuration of a uniform extension.     

Free-Edge and Ply Cracking Effect in Angle-Ply Laminated Composites Subjected to In-Plane Loads

This paper presents a semianalytical method for the prediction of interlaminar stresses and displacements near the free edges and ply cracks in general angle-ply laminates subjected to biaxial extensions and/or in plane shear deformation. The method is based on a state space representation of the three-dimensional equations of elasticity. Numerical solutions are obtained by using layer refinement in the through thickness direction and Fourier series expansion in the other directions. By this approach, an angle-ply laminate may be composed of an arbitrary number of monoclinic layers and each layer may have different material property and thickness. This method guarantees continuous fields of all interlaminar stresses across interfaces between material layers. Numerical results are compared with those obtained from other methods. It is found that the theory provides a satisfactory approximation to the stress singularities near the free edges and ply cracks. Numerical solutions for antisymmetric laminates under extension and general laminates under shearing are new in the literature and can be used as benchmarks for validating new models.     

安棚深层系凝析气井射孔压井液技术研究

介绍了一种保护油气层的射孔压井液技术，该技术所用的配方具有低密度，低表面张力且具有较强的防膨能力等特点，在安棚深层系低孔低渗油田安3003等凝析气井作业中现场试验，解决了安棚深层系低压气井的水锁伤害等问题，对低孔低渗油气田作业入井流体的研究与应用具有较好的借鉴意义。     

The changes of lipid metabolism and hemorrheology in intrahepatic cholestasis during pregnancy

OBJECTIVE: To identify the influence of the increased level of serum cholyglycine (CG) on lipid metabolism and hemorrheology in patients with intrahepatic cholestasis during pregnancy (ICP). METHODS: The concentrations of serum CG, total cholesterol (CH), triglycerides (TG), high density lipoprotein-cholesterol (HDL-C), low density lipoprotein-cholesterol (LDL-C), high shear and low shear of blood specific viscosity (HS and LS), plasma specific viscosity (PV) and hematocrit (HCT) were measured in 68 cases of primiparas with single pregnancy and 30 healthy nonpregnant women respectively. The group of ICP was composed of 35 cases with CG > 6 mumol/L, the group of normal pregnancy, 33 cases with CG < 6 mumol/L. RESULTS: The means of CG and the lipidic parameters in the two pregnant groups were significantly higher than those in the non-pregnancy group (P < 0.02-0.001) except the means of HDL-C between the groups of ICP and non-pregnancy. The levels of LDL-C, LDL-C/HDL-C, LS, PV and HCT in the ICP were significantly higher than those in the normal pregnancy group (P < 0.02-0.001). CONCLUSIONS: There are significant changes of lipid metabolism and hemorrheology in patients with ICP. However, these changes could be corrected after pregnancy termination, when the level of serum CG returned to normal. The results suggest that the pathophysiologic changes of ICP are associated with increased level of serum CG.     

硬件握手双向选通型串行通信共享器的设计

本文介绍了ＩＢＭ－ＰＣ系列计算机通过ＲＳ－２３２Ｃ串行口与多个单片微机组成的分布式系统中一种可双向选通串行通信共享器的设计方法。给出通信共享器的设计电路；并对电路工作原理进行了详细剖析。