零析水水泥浆配合双凝双压固井工艺在泽74-1X井固井作业中的应用

泽74－1X井是为评价泽74断块奥陶系潜山油气情况，在泽74－1井开窗侧钻的一口评价井，该井井斜变化大，井眼轨迹呈螺旋型，地层特性复杂。该井通过采用ZJ－2低失水、零析水水泥浆体系配合双凝双压固井工艺，固井施工顺利，全井主要封固段固井质量良好。现场应用表明，ZJ－2降失水水泥浆体系具有流动性好、水泥浆初始稠度低、析水为零等特点，稠化时间易于控制，十分适合大斜度井和井眼轨迹不佳的井的固井要求，能够很好地保护油气层；双凝双密度水泥浆体系应用于压力变化大的超长裸眼封固段固井，施工安全，固井质量好，只要水泥浆密度设计合理，工程上采取小排量替浆，可防止固井漏失，提高作业成功率。     

聚苯乙烯生产工艺及其产品性能的改善

介绍了苯乙烯单体热引发本体聚合的特点及美国FINA石油化学公司聚苯乙烯生产工艺的特点，探讨了影响HIPS产品质量的多种因素，并对HIPS产品质量的改善提供提出建议和看法。     

高质量ZnO薄膜的退火性质研究

在LP－MOCVD中，我们利用Zn(C2H5)2作Zn源，CO2作氧源，在（0002）蓝宝石衬底上成功制备出皮c轴取向高度一致的ZnO薄膜，并对其进行500℃-800℃四个不同温度的退火。利用XRD、吸收谱、光致发光谱和AFM等手段研究了退火对ZnO晶体质量和光学性质的影响。退火后，（0002）ZnO的XRD衍射峰强度显著增强，c轴晶格常数变小，同时（0002）ZnOX射红衍射峰半高宽不断减小表明晶粒逐渐增大，这与AFM观察结果较一致。由透射谱拟合得到的光学带隙退火后变小，PL谱的带边发射则加强，并出现红移，蓝带发光被有效抑制，表明ZnO薄膜的质量得到提高。     

纵横波测井资料在储层评价中的应用

将弹性波基础理论，Gasman理论，Biot理论和实验研究结果相结合，探讨了沉积岩地层中速度和弹性模量，弹性模量和孔隙度，剪切模量和孔隙度，速度和孔隙度，孔隙度和Biot系数之间的关系，利用从各种声学测井资料中提取出的P波和S波时差（或速度）定量评价地层孔隙度和骨架物质，辅以泥质指示测井曲线，可以计算地层孔隙度，饱和度，岩性等参数，在M，Krief方法的基础上，采用优化算法寻求适合于任何岩性地层的孔隙度与Biot系数之间的关系式，提高了Biot系数的计算精度，该评价方法有坚实的实验基础和理论基础，评价结果与实验室岩心分析数据吻合。     

Improvement of RCA transistor using RTA annealing after theformation of interfacial oxide

A polysilicon emitter RCA transistor (an ultra-thin interfacial oxide layer exists between polysilicon and silicon emitter) is presented which can operate at 77 K for the first time. An ultra-thin (1.5 nm) interfacial oxide layer is grown deliberately between polysilicon and silicon emitter using RCA oxidation and excellent device stability is obtained after rapid thermal annealing (RTA) treatment in nitrogen atmosphere. The RCA transistor exhibits good electrical performance at very low temperature for an emitter area of 3 × 8 μm². The maximum toggle frequency of a 1:2 static divider is 1.2 GHz and 732 MHz at 300 K and 77 K, respectively     

Dy3+激活的几种硼酸盐在VUV-VIS范围的光谱性质

本文报道了SrAl2B2o7:Dy^3 、BaAl2B2O7:Dy^3 、SrAl3BO7:Dy^3 、La2CaB10O19:Dy^3 的紫外－真空紫外（UV－VUV）激发光谱和UV激发下的发射光谱。根据发射光谱讨论了Dy^3 离子在这几种基质中发光的黄蓝比（Y／B）。在VUV激发光谱中推测了Dy^3 的f-d跃迁及电荷迁移态（CTS）和基质吸收的位置。     

Synthesis and Characterization of Poly （L-lactide-co-ε-caprolactone） Copolymers

A series of random and block poly（ L-lactide-co-e-caprolactone ） （ PCLA ） copolymers whh different composition are prepared using stannous octaoate as catalyst.The effects of the amount of initiator on the intrinsic viscosity have been investigated. The structure of the PCLA copolymers is characterized by means of nuclear magnetic resonance（ NMR ）, Fourier transform infrared spectrum （ FTIR ）, differential scanning calorimetry （ DSC ） and X- ray diffraction （ XRD ） methods. It is shown that the synthesis condition and the composition of copolymers obrious influence on the structure of PCLA copolymers. Hydrolytic degradation of the copolymers in a PBS solution of pH 7.4 at 37.0℃ shows that the copolymers of different composhions degrade at different rates.     

High-resolution electron microscopy of the twinning and intergrowth in Ca4Al6SO16 and Ca3SrAl6SO16

The microstructures of unhydrated calcium aluminosulphate Ca₄Al₆SO₁₆ and Ca₃SrAl₆SO₁₆ have been studied by high-resolution electron microscopy (HREM). The results showed that twinning and twinned slabs could be introduced taking the [1 1 2] direction as the twin axis so that it seems to be coincident with the law of twinning formed in body-centred cubic structures. A previously reported superlattice with a repeat period twice that of the fundamental structure along the 〈1 1 0〉 direction has also been found in both matrix and twin variants. The close intergrowth of Ca₃SrAl₆SO₁₆ and another phase, possibly Sr₃Al₂O₆ existing as an inclusion between these two twin variants, was determined and clearly revealed by electron diffraction and HREM images. The coherent interphase boundaries and orientation relationship between them can also be deduced.     

Impact of nonlinear phase noise on direct-detection DQPSK WDM systems

The performance degradation of differential quadrature phase-shift keying (DQPSK) wavelength-division-multiplexed (WDM) systems due to self-phase modulation (SPM)- and cross-phase modulation (XPM)-induced nonlinear phase noise is evaluated in this letter. The XPM-induced nonlinear phase noise is approximated as Gaussian distribution and summed together with the SPM-induced nonlinear phase noise. We demonstrate that 10-Gb/s systems, whose walkoff length is larger than 40-Gb/s systems', are more sensitive to XPM-induced nonlinear phase noise than 40-Gb/s systems. Furthermore, DQPSK WDM systems show lower tolerance to both SPM- and XPM-induced nonlinear phase noise than differential phase-shift keying WDM systems.     

属性证书的管理与应用

公钥基础设施PKI很好地解决了身份认证问题,但是无法满足权限管理问题,而属性证书(Attribute Certificate)提供了全新的方法来解决细粒化访问控制问题,将PKI框架扩展到了授权领域。本文就当前有关属性证书的标准和相关文献,针对其技术概貌作了一些综述,并介绍了属性证书的应用。