水基Fe3O4磁流体的制备工艺研究

用共沉淀法制备Fe3O4磁流体,总结出用十二烷基磺酸钠与聚乙二醇作为表面活性剂制备水基磁流体的合适条件:(1)反应温度为室温或不高于35℃;(2)表面活性剂十二烷基磺酸钠的最佳用量为0.0030～0.0040 g/80 mL;(3)第一次包裹的最佳pH为9～10;(4)聚乙二醇作为第二次包裹的表面活剂时,体系最佳温度为40℃左右;(5)表面活性剂聚乙二醇的最佳用量为0.0050～0.0060 g/80 mL。通过实验制得了能稳定存在180 d的水基磁流体。并用透射电镜、红外光谱、分光光度计、古埃磁天平等进行了初步表征。     

An approach for minimizing a quadratically constrained fractional quadratic problem with application to the communications over wireless channels

Studies for the cognitive model are relatively new in the literature; however there is a growing interest in the communication field nowadays. This paper considers the cognitive model in the communication field as the problem of minimizing a fractional quadratic problem, subject to two or more quadratic constraints in complex field. Although both denominator and numerator in the fractional problem are convex, this problem is not so simple since the quotient of convex functions is not convex in most cases. We first change the fractional problem into a non-fractional one. Second, we consider the semi-definite programming (SDP) method. For the problem with m (m≤2) constraints, we use the SDP relaxation and obtain the exact optimal solution. However, for the problem with m (m>2) constraints, we choose the randomization method to gain an approximation solution in the complex case. At last, we apply this method to practical communications over wireless channels with good results.     

A surrogate-based optimization method with RBF neural network enhanced by linear interpolation and hybrid infill strategy

In engineering, it is computationally prohibitive to directly employ costly models in optimization. Therefore, surrogate-based optimization is developed to replace the accurate models with cheap surrogates during optimization for efficiency. The two key issues of surrogate-based optimization are how to improve the surrogate accuracy by making the most of the available training samples, and how to sequentially augment the training set with certain infill strategy so as to gradually improve the surrogate accuracy and guarantee the convergence to the real global optimum of the accurate model. To address these two issues, a radial basis function neural network (RBFNN) based optimization method is proposed in this paper. First, a linear interpolation (LI) based RBFNN modelling method, LI-RBFNN, is developed, which can enhance the RBFNN accuracy by enforcing the gradient match between the surrogate and the trend observed from the training samples. Second, a hybrid infill strategy is proposed, which uses the surrogate prediction error based surrogate lower bound as the optimization objective to locate the promising region and meanwhile employs a linear interpolation-based sequential sampling approach to improve the surrogate accuracy globally. Finally, extensive tests are investigated and the effectiveness and efficiency of the proposed methods are demonstrated.     

喷码机平台WinCE5.0系统的BSP开发

基于以S3C2440A处理器为核心的喷码机硬件开发平台,研究了嵌入式WinCE5.0操作系统板级支持包BSP的开发。分析了喷码机平台的硬件组成和BSP的框架结构,利用源代码重用的思想,完成了Bootloader、OAL、驱动程序、配置文件的开发工作并在BINFS文件系统的基础上实现Multi-bin成功将内核分块。实践表明该BSP在喷码机台上运行稳定,可靠性高,能有效提升系统的开机速度,并使平台拥有了运行大型喷印软件的能力。     

省级网站安全监控平台建设的几点建议

针对网站日益增多的安全问题,提出在监管方面重要的技术手段--省级网站安全监控平台,并针对平台实现功能、平台建设、运维等方面提出几点建议.     

Polymerization mechanisms and molecular weight distribution. II. AIBN-initiated polymerization of styrene at 60°C

An experimental study was carried out on the AIBN-initiated polymerization of styrene at 60°C. The kinetic rate constants were determined by the method of moments and the MWD method, which was proposed in a previous paper. The results compared favorably with the data in the literature and the MWD method was noted to yield more consistent results than the method of moments, which indicates the importance of considering the whole molecular weight distribution. The theoretical MWD was found to approximate the experimental MWD well. The chain-transfer constant to AIBN was found to be between 0.09 and 0.14.     

A two‐station embossing process for rapid fabrication of surface microstructures on thermoplastic polymers

An embossing strategy involving a hot station and a cold station for sequentially heating and cooling the embossing tool was investigated to reduce cycle times in hot embossing polymer microstructures. Experimental studies showed that aluminum stamps with a thickness of 1.4 mm can be rapidly heated from room temperature to 200°C in 3 s using contact heating against a hot station at 250°C. Microchannels and microlenses were successfully embossed onto high‐density polyethylene and acrylonitrile–butadiene–styrene substrates using a heating time less than 3 s and a total cycle time around 10 s. The two‐station embossing process for the microlens was also numerically studied. The simulated filling behavior agreed with the experimental observation and the predicted thermal and deformation history of the polymer offered a good explanation on the experimentally observed process characteristics. POLYM. ENG. SCI., 47:530–539, 2007. © 2007 Society of Plastics Engineers.     

The kinetics of B‐a and P‐a type copolybenzoxazine via the ring opening process

The structure of benzoxazines is similar to that of phenolic resin through thermal self‐curing of the heterocyclic ring opening reaction that neither requires catalyst nor releases any condensation byproduct. These polybenzoxazine resins have several outstanding properties such as high thermal stability and high glass transition temperature. To better understand the curing kinetics of this copolybenzoxazine thermosetting resin, dynamic and isothermal differential scanning calorimetry measurements were performed. Three models, the Kissinger method, the Flynn–Wall–Osawa method, and the Kamal method, were used to describe the curing process. Dynamic kinetic activation energies based on Kissinger and Flynn–Wall–Osawa methods are 72.11 and 84.06 KJ/mol, respectively. The Kamal method based on an autocatalytic model results in a total order of reaction between 2.66 and 3.03, depending on curing temperature. Its activation energy and Arrhenius preexponential are 50.3 KJ/mol and 7959, respectively. © 2004 Wiley Periodicals, Inc. J Appl Polym Sci 95: 730–737, 2005     

英语教学中的创造性思维培养

探讨William Gordon集思广益教学模式在英语教学实践中的运用。实践证实,活动中参与者的思考彼此相冲击,产生灵感,进而使思维更加灵活、通畅,同时,学生也更加乐于表达和倾听。英语教学中使用集体讨论,集思广义为基础的教学模式,不但可以锻炼学生语言的综合能力,而且可以开拓思路,引发创造性思维的产生,培养创造力。     

"团队项目训练法"在市场营销实践教学中的应用——以"与爱同行"营销策划综合训练为例

“团队项目训练法”是充分利用各种市场资源,按照市场营销工作实际,让学生自组团队、自寻商机、自设项目,理论联系实际分析营销环境．对真实对象进行市场营销方案设计、实施、评估,亲历市场营销的完整过程,以此进一步掌握理论,训练技能,提高能力。介绍了重庆科技学院对市场营销专业本科生运用“团队训练法”进行实践教学的做法及效果。