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A commercial Co---Mo/Al2O3 catalyst was labeled with the radioisotope 35S in hydrodesulfurization (HDS) of 35S-labeled dibenzothiophene (35S-DBT) in a high-pressure flow reactor at 50 kg/cm2. Then, HDS of 4-methyldibenzothiophene (4-MDBT) and 4,6-dimethyldibenzothiophene (4,6-DMDBT) or sulfur exchange of H2S were carried out on the labeled catalyst at 50 kg/cm2 and 260–360°C. The amounts of labile sulfur participating in the reaction were determined from the radioactivity of 35S---H2S released from the 35S-labeled catalyst. In the HDS reactions, the amount of labile sulfur participating in the reaction decreased in the order: DBT> 4-MDBT> 4,6-DMDBT. In the sulfur exchange reaction with H2S, the adsorption of H2S on the catalyst reached saturation above a H2S partial pressure of 0.36 kg/cm2. It was suggested that the release of H2S from the labile sulfur may be the rate determining step of the HDS reaction. 相似文献
203.
Supramolecular assemblies from chitosan-graft-β-cyclodextrin (CS-g-CD) and benzimidazole ended poly(ethylene glycol)-block-poly(ε-caprolactone) (PEG-b-PCL-BM) were formed based on the inclusion complexation between β-cyclodextrin and benzimidazole. The supra-amphiphiles self-assembled into complex vesicles with PCL/β-CD as the hydrophobic membrane, hydrophilic PEG and CS as the corona. The hydrophobic membrane and aqueous lumen of vesicles exhibited efficient entrapment both for hydrophobic curcumin (CUR) and hydrophilic doxorubicin (DOX). The drug loading of vesicles was more than 20.2% and 38.4% for CUR and DOX, respectively. Decreasing pH to acidic condition or increasing temperature, more controllable and rapid release of two drugs was observed. Cytotoxicity assays revealed that dual drug-loaded vesicles retained high cell proliferation inhibition efficiency than free drugs.GRAPHICAL ABSTRACT 相似文献
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Dynamics modeling and analysis of a flexible-base space robot for capturing large flexible spacecraft 总被引:2,自引:0,他引:2
Wenfu Xu Deshan Meng Yongquan Chen Huihuan Qian Yangsheng Xu 《Multibody System Dynamics》2014,32(3):357-401
Space robots are in huge demand due to the rapid growth of their service targets, i.e., spacecraft. There are generally large flexible components on spacecraft, such as antenna reflectors and solar paddles. Due to the vibratility of their structure, it is challenging for a space robot with flexible appendages (the base is then called flexible-base) to capture and repair the large flexible spacecraft. After capturing, the two spacecraft with flexible appendages are connected by a space manipulator, and a compounded system is formed. In this paper, we developed a dynamic model and a closed-loop simulation system, to provide a means to verify path planning and control algorithms. Initially, the dynamic characteristics of different capturing stages (preimpact and post-impact) were analyzed. The topologies of a flexible-base space robot and the compounded system were described based on incidence and channel matrices. Secondly, the recursive dynamics was formulated and resolved by an effective numerical method. The modeling was verified by Adams’ model. Thirdly, we implemented a dynamics calculation block in Matlab/Simulink environment using the S-function package for the C program, and developed a closed-loop simulation system, which was composed of the Planning and Controller, the Multibody Dynamic, and the 3D Display modules. Finally, based on the simulation system, two typical missions—target berthing and on-orbital manipulation of the target along a circle, were simulated and evaluated. Dynamics analysis results presented some useful rules for the path planning and control to suppress the vibration of the flexible structure. 相似文献
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Large volume of online review data can reveal consumers’ major interests on domain product, which attracts great research interests from the academic community. Most of the existing works focus on the problems of review summarization, aspect identification or opinion mining from an item’s point of view such as the quality or popularity of products. Considering the fact that users who generate those review texts draw different attentions to product aspects with respect to their own interests, in this article, we aim to learn K users’ interest groups indicated by their review writings. Such K interest groups’ identification can facilitate better understanding of major and potential consumers’ concerns which are crucial for applications like product improvement on customer-oriented design or diverse marketing strategies. Instead of using a traditional text clustering approach, we treat the groupId/clusterId as a hidden variable and use a permutation-based structural topic model called KMM. Through this model, we infer K interest groups’ distribution by discovering not only the frequency of product aspects (Topic Frequency), but also the occurrence priority of respective aspects (Topic Order). They jointly present an informative summarization on the raw review corpus. Our experiment on several real-world review datasets demonstrates a competitive solution. 相似文献
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在人才培养中推行素质教育,不仅要让学生学习知识,还要促进学生素质的全面发展,特别是创新精神和创新能力的培养。只有这样,才能解决高等院校毕业生与就业市场不相适应的问题。具体的途径就是改革当前的教育、管理模式,注重因材施教。主要从当前制药工程专业学生培养的现状入手,阐述了实施双导师制的必要性和意义。 相似文献
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针对模糊有限自动机及模糊Petri网在模糊离散事件系统(Fuzzy Discrete Event System,FDES)行为建模中的不足,提出一种扩展模糊Petri网(Extended Fuzzy Petri Net,EFPN),并基于EFPN构造了FDES行为模型及系统故障诊断器。EFPN以一种新的事件模型为基础对FDES的系统行为进行建模,并根据事件触发矩阵计算下一系统状态中各分量的可能性分布。与模糊有限自动机及模糊Petri网的对比分析表明,在描述FDES模糊事件时,对于同步距离为0的一组事件所造成的影响,EFPN的表达能力强于经典模糊Petri网;在对含有多个状态分量的FDES建模时,EFPN模型的规模远小于模糊有限自动机。在基于EFPN构造的系统行为模型中,运用可达状态标识图分析系统状态集,可有效地构造FDES的故障诊断器,并可据此进行系统可诊断性分析。 相似文献