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91.
Certain new sulfide-smelting processes and coal-gasification processes generate high-strength sulfur dioxide streams, for
which a new process for converting sulfur dioxide to elemental sulfur needs to be developed because no process exists that
is generally and economically applicable to the treatment of such streams. A thermodynamic and experimental investigation
to develop a new process for converting sulfur dioxide to elemental sulfur by a cyclic process involving calcium sulfide and
calcium sulfate without generating secondary pollutants was carried out. In this process, the starting raw material, calcium
sulfate, is reduced by a suitable reducing agent, such as hydrogen, to produce calcium sulfide, which is used to reduce sulfur
dioxide to elemental sulfur vapor and calcium sulfate. The latter is, in turn, reduced to regenerate calcium sulfide. In this
Part I, detailed experimental results are presented on the kinetics of the reaction between sulfur dioxide and calcium-sulfide
pellets, which produces elemental sulfur and calcium sulfate. The experiments were carried out at temperatures between 1023
and 1088 K and sulfur-dioxide partial pressures between 9 and 60 kPa by the use of a thermogravimetric analysis (TGA) technique.
The rate of this reaction was demonstrated by the conversion of 40 pct calcium-sulfide pellets obtained from the hydrogen
reduction of fresh calcium sulfate in 10 minutes at 1073 K under a sulfur-dioxide partial pressure of 43 kPa. The reactivity
decreased somewhat during the first three cycles but remained largely unchanged thereafter up to the tenth cycle. This characteristic
of the pellets is important because the solids must be reusable for repeated cycles to avoid generating secondary pollutants.
A pore-blocking model was found to fit the reaction rate. The reaction is first order with respect to sulfur-dioxide partial
pressure and has an activation energy of 101 to 134 kJ/mol (24 to 32 kcal/mol) for calcium-sulfide pellets reacted and regenerated
several different times. Sulfur dioxide-containing streams from certain sources, such as the regenerator off-gas from an integrated-gasification,
combined-cycle, desulfurization unit and new sulfide-smelting plants, contain much higher partial pressures of SO2. In these cases, the rate of the first reaction is expected to be proportionally higher than in the test conditions reported
in this article. The reduction kinetics of calcium-sulfate pellets with hydrogen gas is reported in the accompanying Part
II. 相似文献
92.
辽河石化分公司减粘裂化装置改炼辽河超稠油的减压渣油后 ,分馏塔顶系统由HCl -H2 S -HCN -有机酸 -H2 O引起的电化学腐蚀严重 ,其中油水分离器局部腐蚀速率达 3.1mm/a ,12AlMoV管束的空冷器运行不足两个月即发生泄漏。塔顶系统采用BZH - 1中和缓蚀剂、无机氨BZH - 913油溶性缓蚀剂综合注剂方案 ,使腐蚀得到控制 相似文献
93.
泽74-1X井是为评价泽74断块奥陶系潜山油气情况,在泽74-1井开窗侧钻的一口评价井,该井井斜变化大,井眼轨迹呈螺旋型,地层特性复杂。该井通过采用ZJ-2低失水、零析水水泥浆体系配合双凝双压固井工艺,固井施工顺利,全井主要封固段固井质量良好。现场应用表明,ZJ-2降失水水泥浆体系具有流动性好、水泥浆初始稠度低、析水为零等特点,稠化时间易于控制,十分适合大斜度井和井眼轨迹不佳的井的固井要求,能够很好地保护油气层;双凝双密度水泥浆体系应用于压力变化大的超长裸眼封固段固井,施工安全,固井质量好,只要水泥浆密度设计合理,工程上采取小排量替浆,可防止固井漏失,提高作业成功率。 相似文献
94.
Microbiological denitrification of red beet juice 总被引:1,自引:0,他引:1
Dorota Walkowiak-Tomczak 《European Food Research and Technology》2002,215(5):401-406
The purpose of study was the determination of optimal conditions for red beet juice denitrification by Paracoccus denitrificans bacteria as well as the evaluation of the usefulness of microbiologically treated juice for the production of a natural colouring preparation for foods. Total reduction of nitrates was found during bacterial culturing at 25 and 30 °C, at an initial pH of 7.0-8.0 and juice osmotic pressure of 900-1100 mOsm/kg. Microbiological denitrification procedure affected colour, taste and aroma of the juice. However, the use of juice as food colouring and component was made feasible by acidification and partial evaporation of water together with volatile substances. 相似文献
95.
96.
叶秀娇 《现代塑料加工应用》2002,14(4):12-14
介绍了苯乙烯单体热引发本体聚合的特点及美国FINA石油化学公司聚苯乙烯生产工艺的特点,探讨了影响HIPS产品质量的多种因素,并对HIPS产品质量的改善提供提出建议和看法。 相似文献
97.
George Ter-Stepanian 《Bulletin of Engineering Geology and the Environment》2002,61(3):197-205
The paper discusses the postulated suspension force, by which it is possible to explain some enigmatic phenomena observed
in different types of mass movements. This force is generated in thick suspensions as a result of friction between sinking
solid particles and static water. The suspension force is related to the seepage force but they have opposite directions.
Both forces form flow networks. Having explained the suspension force, the paper describes how this influences the movement
of material, particularly in debris flows. Enigmatic features and the mechanism of debris flows and lahars are explained by
virtue of the suspension force.
Electronic Publication 相似文献
98.
高质量ZnO薄膜的退火性质研究 总被引:3,自引:0,他引:3
在LP-MOCVD中,我们利用Zn(C2H5)2作Zn源,CO2作氧源,在(0002)蓝宝石衬底上成功制备出皮c轴取向高度一致的ZnO薄膜,并对其进行500℃-800℃四个不同温度的退火。利用XRD、吸收谱、光致发光谱和AFM等手段研究了退火对ZnO晶体质量和光学性质的影响。退火后,(0002)ZnO的XRD衍射峰强度显著增强,c轴晶格常数变小,同时(0002)ZnOX射红衍射峰半高宽不断减小表明晶粒逐渐增大,这与AFM观察结果较一致。由透射谱拟合得到的光学带隙退火后变小,PL谱的带边发射则加强,并出现红移,蓝带发光被有效抑制,表明ZnO薄膜的质量得到提高。 相似文献
99.
We consider the problem of rescheduling trains in the case where one track of a railway section consisting of two tracks
in opposing directions is closed due to construction activities. After presenting an appropriate model for this situation
we derive a polynomial algorithm for the subproblem of finding an optimal schedule with minimal latenesss if the subsequences
of trains for both directions outside the construction site are fixed. Based on this algorithm we propose a local search procedure
for the general problem of finding good schedules and report test results for some real world instances.
Received: December 8, 1999 / Accepted: May 2, 2001 相似文献
100.
Three interesterified vegetable oils (IVOs) prepared from palm, cottonseed, and olive oil, respectively, have been studied for application to Frankfurters. Beef fat (10%) was replaced by one of the IVOs at 20, 60 or 100%. Fatty acid composition of the lipid fraction in the Frankfurters and saturated/unsaturated ratios were established for all batches. We found that total or partial replacement of beef fat by IVOs did not lead to significant changes in appearance, colour, texture, flavour or sensory score. We conclude that IVOs may be successfully applied as beef fat substitutes in Frankfurters. 相似文献