铁（Ⅲ）－1，10－二氮杂菲－甲基橙三元络合物光度法测定铁的研究

提出了铁（Ⅲ）－１,１０－二氮杂菲（Ｐｈｅｎ）－甲基橙（ＭＯ）三元络合物体系光度法测定Ｆｅ（Ⅲ）的新方法。该方法的灵敏度高（ε＝８．１×１０４）,选择性好,准确可靠,用于测定金属和化学试剂中痕量铁,结果满意。     

Effects of Technical Conditions on Structure, Morphology and Crystalline Size of Nanocrystalline Nd-Doped Ceria Powders

Nanocrystalline solid solution CeO2-Nd2O3 powders were prepared by low temperature combustion process.Special attention was paid to the influence of the glycine/metal ratio and calcination temperature on the powders phase structure, morphology and particle size.TG-DSC curves and XRD peaks of different glycine/metal ratio show that smaller particle size can be obtained with a slightly fuel-deficient ratio.XRD results indicate that the as-prepared powders are crystallized in a single fluorite structure.The crystalline size ranges from 9 to 24 nm, which increases with the increase of calcination temperature.The lower SEM images were characterized by the spongy and form-like microstructure of the powders.Organic agent may be gradually eliminated by high temperature calcination process.     

金矿矿源层和含金建造刍议

在矿源层评价中,相对于岩石中的金丰度,金的赋存状态具有更重要的意义,因此在工作中应恢复岩石的原始含金性,并计算区域金丰度值.本文还讨论了含金建造的概念、分布和评价准则等问题.     

p53 codon 72 polymorphism in Taiwanese lung cancer patients: association with lung cancer susceptibility and prognosis

Previous studies have indicated that milrinone, a specific type III phosphodiesterase inhibitor, may be able to induce chloride secretion in cystic fibrosis (CF) tissues. We have now assessed the effect of this agent in vivo on the nasal epithelium of CF mutant mice and also in the nose and lungs of human subjects with CF. Wild-type mice showed a small hyperpolarization of the nasal potential difference (PD) in response to milrinone (100 microM, 1.6 +/- 0.6 mV, n = 8, P < 0.05). In contrast, CF mice carrying either the most common human mutation of the gene for the CF transmembrane regulator (CFTR), DeltaF508 (protein mislocalized), or the G551D mutation (protein normally localized) failed to demonstrate this response. Milrinone perfused alone had no significant effect on the baseline nasal PD of human subjects without CF (14.7 +/- 4.0 mV preperfusion; 15.3 +/- 4.6 mV postperfusion), but significantly (P < 0.05) augmented the hyperpolarization induced by a subsequently perfused low-chloride solution (with milrinone, 36.8 +/- 3.0 mV, n = 6; without milrinone, 18.1 +/- 2.2 mV, n = 19). In contrast, in human subjects with CF (n = 6), milrinone alone significantly (P < 0. 05) altered the nasal baseline PD (52.2 +/- 3.3 mV preperfusion; 57. 4 +/- 4.2 mV, postperfusion) but not the subsequent responses to the low-chloride solution (with milrinone, 1.1 +/- 2.2 mV, n = 4; without milrinone, 0.6 +/- 0.5 mV, n = 28) or to isoproterenol (100 microM). In a separate study in subjects (n = 6) with the DeltaF508 mutation, nasal coadministration of milrinone with isoproterenol produced no effect in the presence of amiloride and a low-chloride solution (-0.8 +/- 0.5 mV). This was also the case in the nasal epithelium of CF subjects (n = 4) carrying at least one G551D allele (-0.3 +/- 0.8 mV). Similarly, milrinone did not hyperpolarize the PD of either the tracheal (n = 6) or segmental (n = 6) airways of CF subjects (DeltaF508) when applied topically in vivo in the presence of amiloride, isoproterenol, or adenosine triphosphate (all 100 microM) in a low-chloride solution. These data do not support the use of milrinone to induce chloride secretion in CF airways in vivo.     

Thermodynamic Study on the Rare Earth Vapour Complex PrAl_3Cl_(12)

ＴｈｅｒｍｏｄｙｎａｍｉｃＳｔｕｄｙｏｎｔｈｅＲａｒｅＥａｒｔｈＶａｐｏｕｒＣｏｍｐｌｅｘＰｒＡｌ３Ｃｌ１２ＷａｎｇＬｉｎｓｈａｎ（王林山），ＧａｏＲｏｎｇｊｉｅ（高荣杰），ＳｕＹｉ（苏轶），ＷａｎｇＺｈｉｃｈａｎｇ（王之昌）（Ｄｅｐａｒｔｍｅｎｔ...     

基于西门子数字驱动伺服611U 的钢轨锯钻床控制系统

近年来,我国铁路客运专线的建设得到高速发展,对钢轨质量提出了更高要求,对钢轨定尺的准确性和钻孔的质量要求也越来越高,通过采用西门子数字驱动伺服611U装置结合上位机PLC系统的步序逻辑控制,能够很好的完成钢轨的定尺和锯钻,大大提高了产品的加工精度.     

炮塔加热过程数学模型与计算机仿真研究

通过对炮塔热处理加热过程的分析研究,取局部最大壁厚处作为二维非稳定态传热问题进行离散化处理,建立了工件加热过程显式有限差分仿真模型。并对计算机仿真结果与实测数据进行了比较验证。     

具有边梁的悬臂矩形板的弯曲问题

本文建议一个求解具有边梁悬臂矩形板弯曲问题的解析解法。该法将有边梁和无边梁悬臂矩形板弯曲问题的解融为一体,在有边梁悬臂矩形板的解中令边梁弯曲刚度为零即得到无边梁悬臂矩形板的解。     

拔染剂的应用性能研究

综合分析了三种拔染剂在拔染浆中的稳定性、吸湿性和渗透性等应用性能，并得出一些重要结论。