Electrochemical performance of nanocrystalline Li3V2(PO4)3/carbon composite material synthesized by a novel sol–gel method

A novel sol–gel method based on V₂O₅·nH₂O hydro-gel was developed to synthesize nanocrystalline Li₃V₂(PO₄)₃/carbon composite material. In this route, V₂O₅·nH₂O hydro-gel, NH₄H₂PO₄, Li₂CO₃ and high-surface-area carbon were used as starting materials to prepare precursor, and the Li₃V₂(PO₄)₃/carbon was obtained by sintering precursor at 750 °C for 4 h in flowing argon. The sol–gel synthesis ensures homogeneity of the precursors and improved reactivity. The sample was characterized by XRD, SEM and TEM. X-ray diffraction results show Li₃V₂(PO₄)₃ sample is monoclinic structure with the space group of P2₁/n. The TEM image indicates that the Li₃V₂(PO₄)₃ particles modified by conductive carbon are about 70 nm in diameter. The Li₃V₂(PO₄)₃/carbon system showed that the discharge capacities in the first and 50th cycle are about 155.3 and 143.6 mAh/g, respectively, in the range of 3.0–4.8 V. The sol–gel method is fit for the preparation of Li₃V₂(PO₄)₃/carbon composite material which may offer some favorable properties for commercial application.     

乙环唑的合成研究

介绍了以2,4-二氯苯乙酮为原料通过催化溴化、缩合反应、与三氮唑钠反应制得原药,原药含量达到92%以上.并对合成条件进行了研究,取得了较为满意的结果.     

广角摄像机在机器人视觉定位中的应用

为了保证广角摄像机在现代机器人视觉定位应用中的准确性,以广角摄像机像素坐标的反畸变过程为研究对象,提出一种在畸变对应表的基础上使用中心迭代法以及区域插值法确定物体实际位置的方法。通过实验证明了该方法能够测量物体的位置,其精度能够满足工业使用要求。     

入侵检测技术在消防信息网安全中的应用

消防信息网作为公安网子网,与互联网物理分隔,网络安全相对薄弱,自身的安全防护能力并不高。非法入侵、病毒破坏屡有发生,给消防信息网带来不可预测的后果。     

巴洛沙星的合成研究

巴洛沙星是一种新型喹诺酮类抗感染药物。从反应温度、反应时间、反应物料摩尔配比和反应溶剂等对合成的影响进行了详细研究。结果表明,其优惠工艺合成条件为:以S1为溶剂,反应温度40℃,反应时间4 h,反应物料摩尔配比n螯合物Ⅰ∶nMAP=1∶1,产品收率79.5%,含量91.4%。     

发电系统短期可靠性评估的等效机组法

本文提出了等效机组的概念,有效地解决了发电系统短期可靠性评估中的“状态爆炸”难题该方法不仅提高了短期可靠性评估的速度和精度,而且极大地压缩了计算存贮量,使发电系统短期可靠性评估更趋于实用化.通过对示例发电系统进行短期可靠性评估,其结果证明了该方法的正确性和有效性.     

注塑产品动态装配模型的集成知识模型研究

基于MBR(基于模型的推理)技术，建立了注塑模具动态装配结构模型；基于RBR(基于规则的推理)技术，应用面向对象的规则模型(OOR)，建立了动态装配规则的知识表示模型。最后，该文将两种知识表示模型集成，建立了完整的知识模型，为整个系统的后续工作奠定了基础。     

L波段微波功率合成技术研究

无人机机载功率放大器的性能一直是限制无人机技术发展的主要因素,为此提出了将功率合成技术应用于无人机数据系统的方法解决上述问题。利用微带线技术结合系统性的电路调试方法,辅以Advanced Design System仿真软件优化设计,同时采用实频技术法进行宽带功放设计,成功研制了频段在1.3 GHz~1.7 GHz的功率放大器,单路功率放大器采用级联的技术输出功率为8 W,两路合成后,实测总输出功率为15.67 W,合成效率达97%,性能稳定,达到实用水平。     

Trust-based group services selection in web-based service-oriented environments

Multi-agent technologies have been widely employed for the development of web-based systems, including web-based e-markets, web-based grid computing, e-governments and service-oriented software systems. In these service-oriented systems, service provider agents and service consumer agents are autonomous and rational entities, which can enter and leave the environments freely. For simplicity, we use terms ‘provider’ and ‘consumer’ to represent this two types of agents. How to select the most suitable service providers according to a service request from a consumer in such an open environment is a very challenging issue. In this paper, we propose an innovative trust model, called the GTrust model, for service group selection in general service-oriented environments. In the GTrust model, the trust evaluation for a service group is based on the functionality coverage of the group, the dependency relationships among individual services in the group, the ratings of individual services on the attributes of the service request and a similarity measurement of the extent to which reference reports can reflect the service request in terms of the priority distribution of attributes. The experimental results and analysis demonstrate the good performance of the GTrust model on the service group selection in service-oriented environments.     

Image inpainting algorithm based on TV model and evolutionary algorithm

With the development of modern image processing techniques, the numbers of images increase at a high speed in network. As a new form of visual communication, image is widely used in network transmission. However, the image information would be lost after transmission. In view of this, we are motivated to restore the image to make it complete in an effective and efficient way in order to save the network bandwidth. At present, there are two main methods for digital image restoration, texture-based method and non-textured-based method. In the texture-based method, Criminisi algorithm is a widely used algorithm. However, the inaccurate completion order and the inefficiency in searching matching patches are two main limitations of Criminisi algorithm. To overcome these shortcomings, in this paper, an exemplar image completion based on evolutionary algorithm is proposed. In the non-textured-based method, total variation method is a typical algorithm. An improved total variation algorithm is proposed in this paper. In the improved algorithm, the diffusion coefficients are defined according to the distance and direction between the damaged pixel and its neighborhood pixel. Experimental results show that the proposed algorithms have better general performance in image completion. And these two new algorithms could improve the experience of network surfing and reduce the network communication cost.