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131.
Ming-Jen Pan Patricia A. Hoffman David J. Green John R. Hellmann 《Journal of the American Ceramic Society》1997,80(3):692-698
The spontaneous microcracking of particulate TiB2 –SiC composites is studied as a function of TiB2 volume fraction. The degree of microcracking was examined by measuring elastic properties from room temperature to 1300°C. The results showed that only one composition contains microcracks. All other compositions did not microcrack regardless of TiB2 volume fraction. This was attributed to the difference in the sintering aids. In particular, the Al2 O3 sintering aid needed in these compositions had reacted with SiO2 to form an amorphous grain boundary phase that allowed residual stresses to relax by viscous flow at moderate to high temperatures. The existence of this amorphous grain boundary phase was directly observed by transmission electron microscopy. 相似文献
132.
Preparation and characterization of porous carbon beads and their application in dispersing small metal crystallites 总被引:2,自引:0,他引:2
Porous carbon beads were prepared by the pyrolysis of poly(vinylidene chloride) beads that were synthesized by suspension polymerization. After prolysis treatment at 180–300 °C under argon stream, the polymeric beads were further carbonized at 1000 °C for 3 h under argon stream to acquire porous carbon beads, of which the specific surface area was about 1000 m2/g, and pore size was mainly in the width range of 0.8–1.2 nm. The carbon structure and surface chemical composition characterized by X-ray diffraction and X-ray photoelectron spectroscopy, depended on the preparation temperature and the relations between them were examined. The characterization of the carbon beads by scanning electron microscopy, atomic force microscopy presented the morphological structure of the carbon beads surface and a global view of pores. The dispersion of nickel crystallites on the carbon beads surface was characterized by electron microprobe analysis. This study reveals that uniform surface morphological structure leads to the fine dispersion of metal crystallites. 相似文献
133.
Guang Su Huang Xiang Ru He Jing Rong Wu Qi Ying Pan Jing Zhen Zhuo Hong 《应用聚合物科学杂志》2006,102(4):3127-3133
In this study, a kind of novel damping materials was prepared based on the blend of chlorinated butyl rubber (CIIR) and polyacrylate (PAc) synthesized by different molar ratio of butyl methacrylate and ethyl acrylate. Research results from experiments and analyses by employing DMA, TEM, and FTIR show that whether at a cocured system or noncocured system, it can be achieved to shift a loss peak of CIIR towards a higher temperature region and to keep the damping value from markedlly decreasing, which broadens the effective damping function area of CIIR to the vicinity of ambient temperature. In the former system, the thermodynamical miscibility of CIIR and PAc, to some extent, is predominated by the molecular design of PAc, while in the latter system, covulcanized networks play a more significant role in improving compatibility and abating the peak split, though the suppression effect of thermal stress on the transition of CIIR Tll transition still can not be neglected. Furthermore, transition state derived from the cocuring CIIR and PAc cannot make the phase separation completely take place, and consequently results in the deformation of phase morphology of the cocured CIIR/PAc blend. It is the influence of thermodynamics miscibility and forced compatibility in different size that makes the suppression effect of foreign PAc on CIIR Tll transition be controllable. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 3127–3133, 2006 相似文献
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136.
大丝束聚丙烯腈基预氧丝炭化研究 总被引:1,自引:0,他引:1
采用正交实验法研究了炭化温度、炭化时间、升温速率等因素对两种聚丙烯腈基预氧丝炭化产物结构和性能的影响.结果表明,进口东邦48 K大丝束聚丙烯腈基预氧丝环化程度优于国产吉林6 K小丝束聚丙烯腈基预氧丝,在炭化温度950℃,升温速率4℃/min,保温时间10 min条件下,炭化可取得最佳性能,炭化产物纤维拉伸强度达2.96 GPa,而国产吉林6 K小丝束在炭化温度1 100℃,升温速率4℃/min,保温时间5 min条件下炭化产物性能最佳,产物炭纤维拉伸强度近3.80 GPa.伴随两种预氧丝炭化过程,纤维颜色加深,表面缺陷减少,拉伸断裂模式均由假塑性向脆性过渡,为复合材料低成本开发中预氧丝坯体制备与炭化工艺提供了参考依据. 相似文献
137.
本文主要叙述了环氧-丙烯酸酯聚合乳液的合成,以及该乳液粘合剂的配制;讨论了该乳液粘合剂的粘合性能及耐水、耐溶剂性能。 相似文献
138.
本文用照相法测定了锚式搅拌槽中高粘度流体的流型和速度分布.利用最小二乘法获得速度分布拟合方程以及槽中剪切率γ和耗散能Φ分布方程.比较了槽壁区域剪切率和全槽平均剪切率、Metzner常数k_S和搅拌器特性参数C_3,指出k_S是表征槽中高剪切区域剪切率大小的特征量,C_3表征了全槽平均剪切率的大小.对于均匀剪切场,两者是一致的.可以用单位体积剪切率分布系数φ_V来描述槽中剪切率分布的均匀程度.本文还研究了Re数对速度分布流型的影响,发现在低Re数下,流型是对称的.高Re数下,流型则不对称. 相似文献
139.
Cortajarena AL Kajander T Pan W Cocco MJ Regan L 《Protein engineering, design & selection : PEDS》2004,17(4):399-409
Protein design aims to understand the fundamentals of protein structure by creating novel proteins with pre-specified folds. An equally important goal is to understand protein function by creating novel proteins with pre-specified activities. Here we describe the design and characterization of a tetratricopeptide (TPR) protein, which binds to the C-terminal peptide of the eukaryotic chaperone Hsp90. The design emphasizes the importance of both direct, short-range protein-peptide interactions and of long-range electrostatic optimization. We demonstrate that the designed protein binds specifically to the desired peptide and discriminates between it and the similar C-terminal peptide of Hsp70. 相似文献
140.