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11.
Fernando J. Muzzio Marcos Llusa Christopher L. Goodridge Nhat-Hang Duong Elizabeth Shen 《Powder Technology》2008,186(3):247-254
This paper investigates the effects of processing and equipment parameters of a ribbon blender (i.e. loading method of lubricant, fill level, blade speed and blade design) on magnesium stearate homogeneity. A core sampling technique is used to obtain at least one hundred samples per sampling event, which are extracted throughout the blender and yield a thorough characterization of the entire bed. The results presented here can be used as a guideline to develop appropriate blending processes and characterization protocols for ribbon blenders. 相似文献
12.
We report the growth of highly C-axis orientation of Sr
x
Ba1−x
Nb2O6 (SBN) thin films on p-type (100) Si substrates by using a potassium-substituted SBN template layer with the sol–gel method. The crystallization of SBN thin films was found closely related to the potassium ion doping concentration and the postannealing temperature of the K-SBN template layer. Secondary ion mass spectrometry analysis showed that potassium elements were accumulated at the interface of the template layer and silicon substrate. SBN films postannealed at 750 °C with K-SBN template layer has a smaller full width at half maximum of X-ray rocking curve of 2.45° than that of 5.40° for the pure SBN films. By introducing a template layer, the surface morphologies of SBN films fabricated on silicon substrate were greatly improved. 相似文献
13.
Ring‐opening polymerization of D,L ‐lactide (LA) has been successfully carried out by using rare earth 2,6‐dimethylaryloxide (Ln(ODMP)3) as single component catalyst or initiator for the first time. The effects of different rare earth elements, solvents, monomers and catalyst concentration as well as polymerization temperature and time on the polymerization were investigated. The results show that La(ODMP)3 exhibits higher activity to prepare poly(D,L ‐lactide) (PLA) with a viscosity molecular weight of 4.5 × 104 g mol?1 and the conversion of 97 % at 100 °C in 45 min. The catalytic activity of Ln(ODMP)3 has following sequence: La > Nd > Sm > Gd > Er > Y. A kinetic study has indicated that the polymerization is first order with respect to both monomer and catalyst concentration. The apparent activation energy of the polymerization of LA with La(ODMP)3 is 69.6 kJ mol?1. The analyses of polymer ends indicate that the LA polymerization proceeds according to ‘coordination–insertion’ mechanism with selective cleavage of the acyl–oxygen bond of the monomer. Copyright © 2004 Society of Chemical Industry 相似文献
14.
Yun‐Hwei Shen 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2005,80(5):581-586
A novel strategy of sweep coagulation to treat low turbidity water is presented herein. Study findings demonstrated that an Na+‐saturated bentonite with medium cation exchange capacity (CEC) resulted in significant turbidity removal at a bentonite dosage of 30 mg dm?3. Bentonite dispersion with fully delaminated platelets tended to undergo a more porous type of coagulation with intense face‐to‐face interactions of platelets and effectively entrapped TiO2 particles in band‐type structures. This type of coagulation usually results in a large volume of settled flocs with a fluffy structure and excellent turbidity removal efficiency for sweep coagulation. The sign and magnitude of electrical charge on TiO2 particles has a minor effect on the efficiency of sweep coagulation. Copyright © 2005 Society of Chemical Industry 相似文献
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Al,Ga取代Bi:DyIG薄膜的磁和磁光特性的研究 总被引:1,自引:0,他引:1
本文报道用热分解法在玻璃衬底上制备了Al和Ga取代的Bi:DYIG薄膜,对其磁和磁光特性做了详细研究.Al和Ga取代的薄膜均可获得好的矩形比和高的矫顽力.对于Bi1.2Dy1.8Fe5-xMXO12(M=A1,GZ)薄膜,A1和G2的最佳替代成份分别为1.0和G.7;最佳晶化温度分别为700o℃和675℃.在波长510nm附近,法拉第旋转角可达8°/um左右.光学吸收和品质因子的研究结果表明,Al和Ga取代能够影响光学吸收和品质因子,其中Ga取代对光学吸收和品质因子的影响较大. 相似文献
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