高纯竹叶碳苷黄酮复合纳米生物材料的制备及其结构表征（急）

采用离子交联法，以高纯竹叶碳苷黄酮制剂（碳苷总质量分数﹥90%，记为H-BLF）和芫根阴离子多糖（TP）为原料，通过ε-聚赖氨酸（ε-PL）的阳离子桥键合而成竹叶碳苷黄酮纳米混悬液（H-BLFnd），进一步在混悬液中添加8%（w/v）的γ-环糊精、经真空冷冻干燥得到纳米冻干粉（H-BLFnp），采用粒径分析、TEM、UV、FTIR、TG和DSC对其外观、性能、结构进行表征。结果表明： H-BLFnp外观为白色粉状，表面光洁平整，色泽均匀，平均粒径为（679±10.2）nm，分散系数为（0.349±0.004），包埋率为（92.39±0.34）%。     

Effects of the reinforcement and toughening of acrylate resin/CaCO3 nanoparticles on rigid poly(vinyl chloride)

Novel composite particles based on nanoscale calcium carbonate (nano‐CaCO₃) as the core and polyacrylates as the shell were first synthesized by in situ encapsulating emulsion polymerization in the presence of the fresh slush pulp of calcium carbonate (CaCO₃) nanoparticles. Subsequently, these modified nanoparticles were compounded with rigid poly(vinyl chloride) (RPVC) to prepare RPVC/CaCO₃ nanocomposites. At the same time, the effects of the reinforcement and toughening of these modified nanoparticles on RPVC were investigated, and the synergistic effect of modified nanoparticles with chlorinated polyethylene (CPE) was also studied. The results showed that in the presence of nano‐CaCO₃ particles, the in situ emulsion polymerization of acrylates was carried out smoothly, and polyacrylates successfully encapsulated on the surface of nano‐CaCO₃ to prepare the modified nanoparticles, breaking down nano‐CaCO₃ particle agglomerates, improving their dispersion in the matrix, and also increasing the particle–matrix interfacial adhesion. Thus, the effects of the reinforcement and toughening of these modified nanoparticles on RPVC were very significant, and the cooperative effect of the nanoparticles with CPE occurred in the united modification system. Scanning electron microscopy analyses indicated that large‐fiber drawing and network morphologies coexisted in the system of joint modification of nanoparticles with CPE. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 103: 3940–3949, 2007     

PLC控制电梯教学模型的设计

根据电梯系统的结构特点及控制要求,设计了基于PLC控制的电梯教学模型。详细阐述了模型电梯系统的硬件构成和软件实现方法。试验表明,该实验装置提高了PLC实验课的教学质量。     

基于几何特征的流体动画控制方法

在流体动画中,流体控制是生成可控流体运动的关键技术.为产生视觉逼真、行为可控的流体动画效果,提出一种基于几何特征的流体控制方法.首先通过构建流体形状的时变几何分区,实现对可控流体形状的表达及动态跟踪;在此基础上设计异构控制模型,以增强流体运动控制的灵活性,该模型采用了带约束优化的刚性控制和基于弹簧模型的柔性控制2种方法;最后将异构控制模型与高精度流体物理模型相耦合,生成视觉逼真的可控流体运动效果.实验结果表明,该方法能够在保持流体角色形状的同时产生丰富的流体细节,满足动画师的设计需求.     

单幅图像多尺度小波深度提取算法

针对浅景深图像中平滑前景区域深度提取误差大的问题,基于像素点分类思想对深度值进行修正,提出一种基于多尺度小波线索的、可同时面向单幅浅景深图像和广角图像的深度图提取算法.首先使用小波分析法在多个尺度下提取图像深度信息;然后提出自适应分类法并根据尺度与深度变化规律对像素点做深度修正,得到深度图;最后结合区域生长与边缘分割算法对深度图进行区域优化.为了加快深度计算,还提出了快速zerocount法以及多尺度加速法来满足标清视频实时处理要求.实验结果证明,采用文中算法获得的深度图相对深度正确,前景和背景区域深度一致性好.     

稀疏表示分类中遮挡字典构造方法的改进

针对稀疏表示分类算法中遮挡字典维数高且无冗余的问题,提出一种遮挡字典构造方法.首先通过图像分块得到各级的遮挡基图像;然后将所有互不相同的遮挡基图像按字典顺序转化为向量,并用这些向量作为遮挡字典的列,从而构造出维数相对较低且具有一定冗余度的遮挡字典.实验结果表明,该方法不仅明显提高了稀疏表示分类算法对遮挡人脸的识别率,而且还能通过减少图像的分块级数降低稀疏分解的耗时量,提高运算效率.     

秋季太湖叶绿素a浓度荧光反演研究

基于2007年11~12月太湖全湖实测水质参数和光谱数据,首先利用高斯方程对遥感反射率进行过滤分解,找出叶绿素a(chl\|a)吸收峰675 nm以后的荧光反射峰(Fluorescence Peak:FP),再以662 nm处的反射率为基准,采用归一化荧光高度法进行叶绿素a浓度(C chl-a)反演,得到chl-a反演模型。基于高斯分解获取的chl-a的荧光反射峰值R(FP)与662 nm处的反射率R (662)比值［R(FP)/R(662)］与C chl-a之间存在显著的相关性,该模型为秋季太湖水体C chl-a的最佳反演模型。在高悬浮泥沙条件下,该模型能够较好地表示出叶绿素荧光高度与叶绿素浓度之间的关系,为C chl-a反演提供新的方法和依据,并为传感器敏感波段的选取和设置提供参考。     

常减压蒸馏装置配剂方法比较

对常减压装置的三种配剂方法进行分析比较，从而选出经济、合理的配剂方法。     

Effects of the o‐aromatic ring in the molecular chain on the properties of polyester polyols

A series of liquid polyester polyols from adipic acid (AA), phthalic anhydride (PA), ethylene glycol, propanediol‐1,2, and trihydroxymethylpropane, varying in the molar ratio of PA to AA, were prepared. The effects of the o‐aromatic ring in the molecular chain, which came from PA, on the viscosity, glass‐transition temperature, and thermal degradation temperature of the polyester polyols were studied with viscometry, differential scanning calorimetry, and thermogravimetry. The intrinsic viscosity and glass‐transition temperature increased with the concentration of the o‐aromatic ring increasing. The temperature of the maximum thermal degradation rate for aliphatic polyester polyols was 434.20°C. Two steps of thermal degradation were found when there were o‐aromatic rings in the molecular chain. One thermal degradation temperature was 358.36–360.48°C, and the other was 412.85–427.18°C. Polyester polyols with o‐aromatic rings had higher stability at lower temperatures (<240.00°C). However, aliphatic polyester polyols had higher stability at higher temperatures (300.00–480.00°C). The activation energy and order of degradation were calculated from thermogravimetric curves. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 83: 1617–1624, 2002     

工业变换炉最佳催化剂粒度

本文在建立数学模型的基础上，用计算机模拟变换炉的操作工况，考察改变催化剂粒度对经济效益的影响，从而得到工业变换炉催化剂颗粒最佳尺寸，开发了以经济效益为考察依据，工业反应器中催化剂颗粒最佳尺寸的计算方法。