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71.
Zhengshen Wang Huaiji Zheng Juan Yang Xingang Xie Xuegong She 《Advanced Synthesis \u0026amp; Catalysis》2015,357(9):2082-2088
An effective synthesis of structurally diverse pyrroline derivatives has been accomplished by a gold(I)‐catalyzed tandem 1,3‐acyloxy rearrangement/intramolecular azacylization reaction of γ‐amino‐substituted propargylic esters in good to excellent chemical yields (52–98%). The reaction proceeds under extremely mild conditions and has also demonstrated its potential in a concise formal synthesis of (±)‐aphanorphine with a catalyst loading as low as 0.5 mol% to provide the key intermediate 5‐(4‐methoxybenzyl)‐1‐tosyl‐2,5‐dihydro‐1H‐pyrrol‐3‐yl pivalate on a gram scale.
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73.
本文介绍了多级数字抽取滤波器CS5376A的特点及结构,分析了CS5376A芯片的参数设定、以及配合CS5371/72Delta-SigmaA/D转换器和TMS320LF2407DSP构成高精度数据采集系统应用于数字强震仪中的方法。 相似文献
74.
提出了一种自适应阻抗匹配系统.该系统给出了新的阻抗测量算法,并通过选择补偿电感值和变压器变比的方式使电力线阻抗维持在恒定的值上.实验表明,阻抗测量算法准确性很高,匹配方法可行,从而解决了因电力线载波通信中电力线阻抗实时变化带来的各种问题. 相似文献
75.
本文对以欧盟为主编制的标准中涉及混凝土施工养护方面的规定作了综述,重点介绍施工中常遇的质量问题以及采取的技术措施和理论分析等,以期从中借鉴有益的经验。 相似文献
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78.
P She A R Hippen J W Young G L Lindberg D C Beitz L F Richardson R W Tucker 《Journal of dairy science》1999,82(6):1118-1127
Twenty cows were assigned at parturition to two groups to study metabolic effects of continuous intravenous infusions of glucagon. Groups were control cows and cows treated with glucagon at 10 mg/d for 14 d starting at d 21 postpartum. Daily blood samples and nine liver biopsies were taken from d 7 to 49 postpartum. Plasma glucagon increased six- to seven-fold during infusions of treated cows. Plasma insulin was increased heterogeneously by glucagon infusions. Plasma glucose increased 11.5 and 9.0 mg/dl during wk 1 and 2 of glucagon infusions. No other plasma metabolites tested (nonesterified fatty acids, beta-hydroxybutyrate, and urea N) were affected by glucagon infusions. Liver glycogen decreased by d 2 of glucagon infusion but was repleted to preinfusion values by d 7 and increased to 169% of the preinfusion baseline values at 3 d after cessation of glucagon. Milk production decreased transiently during glucagon infusions. Both milk production and milk protein percentage decreased during glucagon infusion, which could imply a decreased availability of amino acids for milk protein synthesis. Feed intakes did not increase during glucagon infusions, which was in contrast to the control group. Results indicated that glucagon infusions caused liver glycogenolysis initially and probably enhanced gluconeogenesis but glucagon did not appear to increase lipolysis from adipose tissue in these early lactating dairy cows. 相似文献
79.
目的 目标检测是遥感智能解译中重要的研究方向之一,大多数目标检测算法难以实现密集排列的旋转目标的高精度检测。提出了一种基于关键点与引导向量预测的目标检测算法,实现高精度旋转目标检测的同时,还可对目标的朝向进行表征。方法 首先提出了一种新的旋转目标建模方式,将目标检测分解成中心点、头部顶点、引导向量以及目标宽度的参数回归以更贴合检测目标;其次设计旋转椭圆高斯核,能够更好地拟合遥感目标的形状,从而提升关键点的预测精度;最后通过预测中心点指向头部顶点的引导向量,完成同一个目标内中心点与头部顶点的匹配,从而生成一个精准的带方向的旋转矩形检测框。结果 在大长宽比舰船目标的HRSC(high-resolution ship collections)数据集上的实验结果表明,相比于其他主流的目标检测算法,本文算法获得了更好的检测结果,在VOC 2007(visual object classes)和VOC 2012的平均精度分别达到了90.78%和97.85%。在小长宽比飞机目标UCAS-AOD(UCAS-high resolution aerial object detection dataset)数据集上达到了98.81%的平均精度。实验结果表明了本文算法的可行性与有效性。结论 本文算法利用椭圆高斯核计算中心点与头部顶点,并设计引导向量对点匹配关系进行约束,实现了旋转目标的方向检测。 相似文献
80.
Absorption of long-chain polyunsaturated fatty acids from human milk and formula supplemented with fish oil was studied to
determine if the distribution route into lymphatic triacylglycerol (TAG) and phospholipid (PL) varies with the dietary source.
Rats were intraduodenally infused with human milk or formula containing graded amounts of fish oil (0, 0.5, or 1.0 g/100 mL),
and the mesenteric lymph was collected. Arachidonic acid (20∶4n−6) levels in lymphatic TAG and PL were highest from animals
fed human milk. In the animals infused with formula containing fish oil, as the amount of eicosapentaenoic acid (EPA, 20∶5n−3)
infused increased, there was essentially an equal increase of EPA associated with both lymphatic TAG and PL. Animals intraduodenally
infused with human milk or formula without fish oil had only minor levels (less than 1%) of EPA in the lymph. In the fish
oil-treated animals, as the amount of docosahexaenoic acid (DHA, 22∶6n−3) infused increased, there was a 16-fold increase
in DHA associated with lymphatic TAG, but only a 3-fold increase in DHA associated with lymphatic PL. The highest level of
DHA in rats infused with human milk was observed in lymphatic PL. Hence, fish oil can be added to formula as a source of long-chain
polyunsaturated fatty acids, but the distribution of fatty acids into lymphatic TAG and PL is not the same as that observed
with human milk. 相似文献