基于J2EE和Eclipse的自动Web化平台实现

Web服务是当前企业在线业务处理的关键技术之一。论述了一个自动Web化平台的实现过程,此平台能够将企业原有在线业务的处理程序自动Web化成Web应用程序。通过将此Web应用程序部署到J2EE服务器上,构成Web服务。该自动Web化平台基于Eclipse插件技术,利用Eclipse的自动构建过程,实现Web应用程序的自动生成。     

3,5-二硝基水杨酸比色法测定麦冬多糖含量

采用3,5-二硝基水杨酸(DNS)比色法测定麦冬多糖含量。结果表明,麦冬多糖占麦冬总干重的40.4mg.g-1,RSD=2.48%(n=5),总糖供试液和单糖供试液的平均回收率分别是100.4%(RSD=0.17%)和101.1%(RSD=0.62%)。试验表明,DNS比色法测定多糖含量简单易行,且重现性好,可作为麦冬多糖含量的常规测定方法。     

AZ31镁合金薄板的CO2激光焊接接头性能

采用CO2激光焊接试验系统对AZ31镁合金薄板进行了焊接,研究了不同工艺条件下焊缝熔宽的变化,并对焊接接头的微观组织和接头性能进行了研究.试验结果表明,激光功率和焊接速度对焊缝熔宽有较大的影响.显微硬度测试和接头拉伸试验结果表明:焊接接头区域的显微硬度和抗拉强度都高于母材,焊接接头具有良好的力学性能.接头区域的晶粒细化和新的合金相的形成是接头性能改善的主要原因.     

磁性聚乙烯醇微球固定化α-淀粉酶的研究

磁性聚乙烯醇微球为载体,采用戊二醛交联法固定化α-淀粉酶,并对固定化酶的理化性质等进行了研究。结果表明,磁性固定化α-淀粉酶的总活力、蛋白载量、比活、活性回收率分别为1107.89U/g微球、125.36mg/g微球、8.84U/mg蛋白质和37.96%;固定化α-淀粉酶的反应最适温度和最适pH分别为110℃和7.0;固定化α-淀粉酶对金属离子Mg2+、Fe2+、Zn2+和Cu2+的抑制作用的忍耐性比自由酶的明显提高;α-淀粉酶被固定化后其热稳定性、操作稳定性、pH稳定性均比自由酶的明显提高。固定化α-淀粉酶在4℃,pH7.0的缓冲液中保存30d,其活力仍保持最初活力的91.6%,这比其自由酶的高12.3%。     

Investigation on surface figuration and microstructure of laser glazed nanostructure zirconia thermal barrier coatings

CO2 continuous wave laser beam had been applied to the laser glazing of plasma sprayed nanostructure zirconia thermal barrier coatings. The effects of luser glazing processing parameters on the surface figuration and microstructure change had been carried out, the microstructure and phase composition of the coatings had been evaluated by the scanning electron microscope (SEM) and the X-ray diffraction (XRD). SEM observation indicates that the microstructure of the as-glazed coating could be altered from single columnar structure to a combination of the columnar grain and fine equiaxed grain with the different laser glazing conditions. XRD analysis illustrates that the predominance phase of the as-glazed coating is the metastable tetragonal phase, and the glazed coating with the single columnar structure has shown the clear orientation in (220) and (400) peaks while the other coatings do not show that.     

纳米ZrO2激光重熔涂层组织与性能分析

采用金相试验、扫描电镜试验、热震试验和显微硬度试验对不同激光重熔工艺下的Y2O3部分稳定ZrO2纳米陶瓷涂层组织与性能进行研究.重点分析了涂层重熔宽度与深度、表面形貌、显微硬度和热震性能随激光比能量的变化规律.结果表明,ZrO2纳米陶瓷涂层的重熔深度和宽度随着激光比能量的增大而增加;涂层的表面成形与激光比能量密切相关;涂层的显微硬度随激光比能量的增大而升高;激光比能量对涂层热震性能的影响十分明显,当激光比能量为37.2 J/mm2时重熔涂层的热震性能最好.     

激光重熔Al2O3-13ωt%TiO2陶瓷涂层组织结构与热震性能

分析了激光重熔过程对Al2O3-13ωt%TiO2陶瓷涂层的物相结构变化、显微硬度和抗热震性能影响.结果表明:激光重熔过程可以获得稳定的α-Al2O3,且激光重熔工艺能够提高涂层的显微硬度和抗热震性能.     

Effect of filler wire on the joint properties of AZ31 magnesium alloys using CO2 laser welding

Laser welding with filler wire of AZ31 magnesium alloys is investigated using a CO2 laser experimental system. The effect of three different filler wires on the joint properties is researched. The results show that the weld appearance can be effectively improved when using laser welding with filler wire. The microhardness and tensile strength of joints are almost the same us those of the base metal when ER AZ31 or ER AZ61 wire is adopted. However, when the filler wire of ER 5356 aluminum alloy is used, the mechanical properties of flints become worse. For ER AZ31 and ER AZ61 filler wires, the microstructure of weld zone slws small dendrite grains. In comparison, for ER 5356 filler wire, the weld shows a structure of snowy dendrites and many intermetallic compounds and eutectic phases distribute in the dendrites. These intermetallic constituents with low melting point increase the tendency of hot crack and result in fiagile joint properties. Therefore, ER AZ31 and ER AZ61 wire are more suitable filler material than ER 5356 for CO2 laser welding of AZ31 magnesium alloys.     

锂离子电池正极材料LiMnPO4/C的固相法制备及性能研究

以碳酸锂、碳酸锰和磷酸二氢铵为原料,以蔗糖为碳源,采用固相法制备了Li Mn PO4/C复合正极材料。利用正交试验考察了焙烧温度、焙烧时间、球磨时间、锂锰摩尔比和蔗糖用量对材料首次放电比容量的影响,得到了最佳工艺条件。通过XRD、SEM、同步热分析仪和充放电测试仪等测试了材料的结构和电化学性能。所得材料在室温下电流密度为0.1 C、0.5 C和1 C时首次放电比容量分别为130.5 m Ah/g、125.8 m Ah/g和117.1 m Ah/g,经过50次循环性能测试后容量分别为113.2 m Ah/g、98.1 m Ah/g和85.4 m Ah/g;在电流密度为0.1 C且温度为60℃时,其首次放电比容量为156.4 m Ah/g,测试结果表明循环性能较好。     

YPSZ等离子涂层激光重熔组织性能

采用CO2激光焊接试验系统对YPSZ(8%Y2O3-ZrO2)等离子涂层进行了激光重熔,并对涂层进行了微观组织与性能分析.结果表明,经激光重熔后YPSZ涂层气孔和微裂纹明显减少,组织均匀致密,表面粗糙度低,强度和韧度提高.涂层硬度的变化与重熔过程中涂层相成分转变有关,经激光重熔处理后YPSZ涂层中主要相成分为t-ZrO2和少量的c-ZrO2,t-ZrO2具有较高的强度和韧度是改善涂层的表面力学性能的主要因素.