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361.
Quantitative image analysis as a diagnostic tool for identifying structural changes during a revival process of anaerobic granular sludge 总被引:3,自引:0,他引:3
Due to unspecified operational problems, the specific acetoclastic activity (SAA) of the anaerobic granular sludge present in an industrial UASB reactor was considerably damaged (from 250 to less than 10mL CH(4)@STP/gVSS.d), significantly reducing the biogas production of that industrial unit. The hydrogenotrophic methanogenic activity exhibited a value of 600mL CH4@STP/gVSS.d, the settling velocity was 31.4+/-9.8m/h, the average equivalent diameter was 0.92+/-0.43mm, and about 70% of the VSS were structured in aggregates larger than 1mm. In order to study the recovery of the SAA, this sludge was collected and inoculated in a lab-scale expanded granular sludge blanket (EGSB) reactor. Ethanol was fed as the sole carbon source during a trial period of 106 days. Process monitoring included COD removal efficiency, methane production, and periodic determination of the specific methanogenic activity in the presence of acetate, propionate, butyrate, ethanol and H(2)/CO(2). Quantitative image analysis allowed for information to be obtained on granular fragmentation/erosion and filaments release. During the first operational period, biogas production was mainly due to the hydrogenotrophic activity. However, after 40 days, the SAA steadily increased achieving a maximum value of 183+/-13mL CH4@STP/gVSS.d. The onset of SAA recovery, granules breakdown and filaments release to the bulk occurred simultaneously. Further increase in SAA was accompanied by granular growth. In the last 25 days of operation, the size distribution was stable with more than 80% of projected area of aggregates corresponding to granules larger than 1mm (equivalent diameter). Confocal images from FISH hybridized sections of the granules showed that after SAA recovery, the granules developed an organized structure where an acidogenic/acetogenic external layer was apparent. Granular fragmentation and increase of filaments in the bulk, simultaneously with the increase in the acetoclastic activity are described for the first time and might represent a structural response of granular sludge to promote the optimal substrate uptake at minimal diffusion limitations. 相似文献
362.
Graziele C. da Cunha Carolina M. Abreu Janaina A. Peixoto Luciane P. C. Romão Zélia S. Macedo 《Journal of Inorganic and Organometallic Polymers and Materials》2017,27(3):674-684
The aim of this work was to produce Cr-doped alpha-alumina nanoparticles using a modified sol–gel method that employs the complexation capacity of natural organic matter (NOM). For this synthesis, the initial pH of the sol was adjusted to 4.0, and final calcination of the xerogel was performed at 1100?°C for 4 h. XRD and FTIR analyses confirmed that the hexagonal α-Al2O3 phase was produced under these conditions. Chromaticity analyses revealed that more intense pink colors were obtained for the samples with higher Cr concentrations. XANES measurements showed that the oxidation state of chromium in the alumina matrix was strongly dependent on the dopant concentration and that it was possible to produce samples free from Cr(VI). The photo- and radioluminescence spectra of the nanoparticles were found to be sensitive to the dopant concentration. All these findings demonstrated that the synthesis procedure using NOM could provide considerable environmental, technological, and economic benefits. 相似文献
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Ribamar Giovani Gonçalves Andrade Tathiane Caminha de Miranda Hélio Cordeiro de Abreu Hamilton Ferreira Gomes 《Metallurgical and Materials Transactions A》2020,51(9):4812-4825
Metallurgical and Materials Transactions A - Stacking fault energy (SFE) is related to activating complex high strength and ductility mechanisms such as transformation-induced plasticity and... 相似文献
368.
Guilherme Abreu Faria Kamalnath Kadirvel Alejandro Hinojos Wei Zhang Yunzhi Wang 《Science & Technology of Welding & Joining》2019,24(5):446-456
ABSTRACTMany models have been developed to explore solidification segregation and dendrite structure in additively manufactured parts. However, these models tend to be computationally expensive and consider only a limited number of alloying elements, compromising their practical application. In this work, a methodology to extend the Scheil model, based on interface metastable equilibrium assumptions, is established to predict the spatial compositional maps due to micro-segregation for a laser-powder bed fusion (L-PBF) build of alloy 718. The compositional maps are contrasted against experimental data measured in a unit dendrite cell by transmission electron microcopy. The validity of Scheil's implicit assumptions under the rapid solidification conditions in L-PBF is further discussed. The extended Scheil model is shown to be computationally efficient and readily applicable to multi-component systems. 相似文献
369.
Joaquina Pinheiro Carla Alegria Marta Abreu Elsa M. Gonçalves Cristina L.M. Silva 《Journal of food engineering》2013
The effects of storage at different temperatures (2, 5, 10, 15 and 20 °C) conditions on whole tomato (Solanum lycopersicum, cv. ‘Zinac’, fruits harvested at mature-green stage) quality parameters, such as colour, chilling injury, firmness, weight loss and total phenolic content, were investigated during a month period. 相似文献