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51.
D. Brynn Hibbert Alfred C. C. Tseung 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》1979,29(12):713-722
The semiconducting perovskite oxide, La0.5Sr0.5CoO3, is a catalyst for the reduction of sulphur dioxide by carbon monoxide. Unlike aluminia-supported metal catalysts, La0.5Sr0.5CoO3 tolerates high levels of oxygen in the gas stream if sufficient carbon monoxide is present to react with all the oxygen. Water vapour (2%) does not adversely affect the reaction; unwanted byproducts H2S and COS are reduced for contact times less than 0.25 s. A computer model is used to predict equilibrium gas compositions for systems containing oxygen and water vapour. During the reaction the catalyst itself reacts with sulphur producing metal sulphides, possibly of simple cubic structure. The perovskite sulphides LaCoS3 and La0.5Sr0.5CoS3 are theoretically unstable. 相似文献
52.
Synthesis of graphene-based nanosheets via chemical reduction of exfoliated graphite oxide 总被引:27,自引:0,他引:27
Sasha Stankovich Richard D. Piner Alfred Kleinhammes Yue Wu Rodney S. Ruoff 《Carbon》2007,45(7):1558-1565
Reduction of a colloidal suspension of exfoliated graphene oxide sheets in water with hydrazine hydrate results in their aggregation and subsequent formation of a high-surface-area carbon material which consists of thin graphene-based sheets. The reduced material was characterized by elemental analysis, thermo-gravimetric analysis, scanning electron microscopy, X-ray photoelectron spectroscopy, NMR spectroscopy, Raman spectroscopy, and by electrical conductivity measurements. 相似文献
53.
This paper is an update of the overview given by Baker RC [Coriolis flowmeters: Industrial practice and published information. Flow Meas Instrum 1994;5(4):229–46]. Overviews about mass flowmetering are also given in Baker RC [Flow measurement handbook. Cambridge University Press; 2000]. Furthermore, Drahm W and Linnartz H [Coriolis-massflowmeters: State of the art review and innovations. In: Proceedings FLUCOME 2003. 2003] reported about latest innovations in Coriolis technology.
The published information of the last decade is reviewed and the conclusions of the different papers are briefly described. 相似文献
54.
Alfred Zeman 《Lubrication Science》1988,5(2):133-148
The versatility of a differential scanning calorimetry (DSC) cell in studying thermal and/or thermal-oxidative degradation of lubricants is shown using ester-based aviation turbine oils as an example. The following applications are discussed: 1. quality control of fresh and used oils by pressure differential scanning calorimetry; 2. influence of metal catalysis on oil degradation; 3. identification of volatile degradation products by PDSC gas chromatography-mass spectrometry via a TENAX trap; 4. determination of spontaneous ignition temperatures; 5. influence of metall metal oxides, wear debris and oil degradation products on ignition behaviour; 6. inhibition of spontaneous ignition by antioxidants. 相似文献
55.
56.
Ford Kentya H.; Diamond Pamela M.; Kelder Steven H.; Sterling Kymberle Landrum; McAlister Alfred L. 《Canadian Metallurgical Quarterly》2009,23(2):271
Attitudes toward smoking, self-efficacy to avoid smoking, and smoking intention, widely cited correlates of youth smoking prevention, are often measured in large-scale youth tobacco surveys. The psychometric properties of these scales have not been well studied among middle school youth. We examined the factorial, discriminate, and convergent validity of these scales among sixth to eighth graders from a convenience sample of 22 Texas middle schools (51.2% female; 51.21% White, 32.1% Hispanic, 16.9% African American, and 8.8% Other; 67.8% nonsmokers, 21.9% experimental smokers; 3.3% former smokers; and 7.6% current smokers). Confirmatory factor analysis and invariance testing suggest that smoking attitudes, self-efficacy, and intention have evidence of construct validity in this multiethnic sample, and the scales are appropriate to assess these constructs among middle school adolescents. Additional studies are needed to establish additional evidence of validity of these constructs in other middle school samples and other subgroups (e.g. current, experimental, and former smokers). (PsycINFO Database Record (c) 2010 APA, all rights reserved) 相似文献
57.
The paper deals with the internal structure of hydraulic jumps in near-critical single-layer flows which replaces the discontinuities predicted by hydraulic theory if viscous effects acting inside a thin laminar boundary layer are properly accounted for. In the limit of large Reynolds number this leads to a structure problem formed by the classical triple-deck equations supplemented with a novel nonlinear interaction relationship which allows for the passage through the critical state. Hydraulic jumps are shown to represent eigensolutions of the structure problem where this passage is achieved by the local thickening of the boundary layer which acts as a viscous hump. The effects of detuning and dispersion due to streamline curvature and surface tension on the internal structure of hydraulic jumps are studied in detail. In addition, the interaction of hydraulic jumps with surface mounted obstacles is investigated. 相似文献
58.
Selective oxidation of alcohols by combinatorial catalysis 总被引:1,自引:0,他引:1
Peter Desrosiers Anil Guram Alfred Hagemeyer Bernd Jandeleit Damodara M. Poojary Howard Turner Henry Weinberg 《Catalysis Today》2001,67(4):397-402
High-throughput synthesis and screening of polyoxometalate (POM) and supported-metal libraries have been developed for the selective aerobic oxidation of alcohols to the corresponding aldehydes/ketones in the liquid phase. Libraries consisting of 96 catalysts were prepared in multi-well reactors and screened for catalytic activity using TLC, GC and NMR detection methods. Promising hits identified in the high-throughput primary screens were successfully scaled up and optimized in conventional laboratory test units. Isolated yields confirm high selectivities of more than 90% with quantitative conversions. Substrates tested include primary and secondary alcohols. Specific results will be presented for hydroxymethyl-substituted heterocycles and bicyclo-octanols. 相似文献
59.
James W. Rosner Alfred E. Thal Jr. Christopher J. West 《Canadian Metallurgical Quarterly》2009,135(8):710-717
The design-build (DB) method for construction project delivery continues to grow in both the private and public sector; additionally, research has shown that the DB method outperforms the design-bid-build (DBB) method. The Air Force has applied the results of these previous research efforts to its military construction (MILCON) program without performing empirical studies to validate the approach. Therefore, the objective of this study was to compare the performance of the DB delivery method with the traditional DBB approach for the Air Force MILCON program. Data related to 835 (278 DB and 557 DBB) MILCON projects for fiscal years 1996–2006 were subsequently analyzed. The DB method had better performance in three of six metrics with the performance being significantly better for cost growth and the number of modifications per million dollars. The traditional DBB method performed significantly better in terms of total project time. Furthermore, the DB method was best suited for various facility types. This study provides empirical evidence of how the DB method provides an advantage over the traditional DBB method for Air Force MILCON projects. 相似文献
60.
Alfred M. Bruckstein Robert J. Holt Arun N. Netravali 《International journal of imaging systems and technology》2009,19(1):27-36
In previous work, we designed space fiducials with the aim of making camera pose determination as noise‐insensitive as possible. These fiducials turned out to be sets of points that formed concentric regular polyhedra. Here, we apply an idea of Dementhon and Davis and test and analyze an iterative linear algorithm in conjunction with our optimal fiducials to increase the accuracy of the computed camera pose. We also analyze under what circumstances this iterative algorithm is guaranteed to converge to the correct solution. Comprehensive computer simulations illustrate the behavior of the algorithm and the degree of improvement in pose determination in case of convergence. © 2009 Wiley Periodicals, Inc. Int J Imaging Syst Technol, 19, 27–36, 2009 相似文献