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91.
Summary In this study, new hydrogels in rod shape were prepared from N-acryloyl-TRIS(hydroxymethyl)aminomethane (NAT) using ethylene glycol dimethacrylate (EGDMA) or N,N’methylenebisacrylamide (BIS) as crosslinking agent, dimethylformamide (DMF) as solvent and benzoyl peroxide (BPO) as initiator. In most cases, 2-hydroxyethyl methacrylate (HEMA), acrylamide (Aam) or acrylic acid (Aac) were used as co-monomers. The polymeric matrices obtained by free radical polymerization exhibited different properties by changing crosslinker, crosslinker concentration, co-monomer and initial NAT/co-monomer mole ratio. Besides, hydrogels from HEMA, Aam and Aac with BIS in absence of NAT were prepared under the same experimental reaction conditions in order to compare the properties of these products with those synthesized from NAT and the respective co-monomers. Some of the final products were selected to perform urea release assays, conducted through swelling-controlled release. Urea was chosen as “model” plant fertilizer agent. 相似文献
92.
L. Mészáros B. Lengyel A. Frignani C. Monticelli G. Trabanelli 《Materials Chemistry and Physics》1985,12(2):189-197
Five different techniques (analytical determination of dissolved iron, Tafel line extrapolation, linear polarization method, impedance and Faradaic distortion measurements) were used for the evaluation of the inhibiting efficiency of N-decyl-3-hydroxypyridine bromide in 1 M hydrochloric acid solutions. The results obtained with the different methods were found to agree satisfactorily. High inhibiting efficiency value was obtained at 1× 10?4Mdm?3 concentration. 相似文献
93.
M. K. Bakhadyrkhanov O. É. Sattarov Kh. M. Iliev K. S. Ayupov Tuérdi Umaier 《Semiconductors》2005,39(7):789-791
It is experimentally ascertained that light stimulates the negative magnetoresistance observed in a high electric field in silicon doped with boron and manganese. The optimum conditions (the electric field, temperature, illumination, and resistivity of the material) for observation of the largest magnitude of negative magnetoresistance in (Si:B):Mn are determined. The dependence of the negative magnetoresistance on the concentration of compensating impurity is established. 相似文献
94.
Joaquim Pérez-Losada Elena Roget Xavier Casamitjana 《Canadian Metallurgical Quarterly》2003,129(9):734-737
High vertical wave-number modes clearly dominate the internal wave field during the stratification period in Boadella reservoir in northeast Spain. In this period, the extraction of hypolimnetic water, due to summer irrigation, brought the surface level down by 6 m in one month and the epilimnetic water progressively occupied the whole water column. The temperature profile, with the exception of a few meters at the surface layer, presented an almost constant temperature gradient of about 0.7°C/m. The period of the main vertical mode is 24 h with an amplitude of around 1 m. Thermistor chain records and meteorological data allow us to deduce that this mode is, at least, a third vertical mode forced by the wind, which normally has a typical periodicity of 24 h. However, when the wind changes direction from south to north, the circulation cells developed due to this forced nonstationary oscillation are destroyed. When this occurs, the Bulk Richardson number is Rib ~ 1. Similar vertical structures as a response to wind forcing should be expected in similar systems, although this has not been reported in the literature. 相似文献
95.
Ezequiel R. Soulé Guillermo E. Eliçabe Roberto J. J. Williams 《Polymer Bulletin》2008,60(2-3):417-423
An unexpected experimental finding is reported where the primary morphology developed during polymerization-induced
phase separation in a rubber-modified thermoplastic practically disappears at high conversions. This process
was evidenced by light scattering (LS) and scanning electron microscopy (SEM) for a particular composition
of solutions of polyisobutylene oligomers (PIB) in isobornylmethacrylate (IBoMA), during the free-radical
polymerization of the monomer. The primary phase separation produced a dispersion of domains rich in PIB
containing significant amounts of the monomer (IBoMA). Polymerization of the monomer in these domains occurred
at high overall conversions producing the filling of dispersed domains with a PIBoMA-PIB blend that could
not be distinguished from the matrix. Under these conditions the final material had the appearance of a
homogeneous blend. 相似文献
96.
The new emerging area of Enterprise Wide Optimization (EWO) has focused the attention in effectively solving the combined production/distribution scheduling problem. The importance of logistic activities performed in multi-site environments comes from the relative magnitude of the associated transportation costs and the good chance of getting large savings on such expenses. This paper first develops an exact MILP mathematical formulation for the multiple vehicle time-window-constrained pickup and delivery (MVPDPTW) problem. The approach is able to account for many-to-many transportation requests, pure pickup and delivery tasks, heterogeneous vehicles and multiple depots. Optimal solutions for a variety of benchmark problems with cluster/random distributions of pickup and delivery locations and limited sizes in terms of customer requests and vehicles have been discovered. However, the computational cost exponentially grows with the number of requests. For large-scale m-PDPTW problems, a local search improvement algorithm steadily providing a better solution through two evolutionary steps is also presented. A neighborhood structure around the starting solution is generated by first allowing multiple request exchanges among nearby trips and then permitting the reordering of nodes on every individual route. If a better set of routes is found, both steps are repeated until no improved solution is discovered. Compact MILP mathematical formulations for both sub-problems have been developed and solved through an efficient branch-and-bound algorithm. A significant number of large-scale m-PDPTW benchmark problems, some of them including up to 100 transportation requests, were successfully solved in reasonable CPU times. 相似文献
97.
Vanesa Rodríguez-Amor Juan P. Fernández-Blázquez Antonio Bello Ernesto Pérez María L. Cerrada 《Polymer Bulletin》2008,60(1):89-96
Summary The effect of molecular weight on the uniaxial orientation process has been analyzed in two samples of thermotropic poly(diethylene
glycol p,p′-bibenzoate), evaluating the influence of that parameter on the type of orientation obtained. Several strain rates and deformation
temperatures have been tested in order to map out the conditions for obtaining the two different kinds of orientation. The
results show that in the lower molecular weight PDEB sample (Mw=31200) it is rather easy to get exclusively perpendicular “anomalous” orientation, with the molecular axes aligned transversely
to the stretching direction. However, it is extremely difficult to obtain 100% parallel “normal” orientation. On the contrary,
either type of orientation or a mixture of them can be easily developed for the higher molecular weight PDEB sample (Mw=102900). 相似文献
98.
99.
N. Hémono J. Rocherullé M. Le Floch B. Bureau P. Bénard-Rocherullé 《Journal of Materials Science》2006,41(2):445-453
The glass forming region in the B2O3-Al2O3-Y2O3 composition diagram has been determined by a melting and quenching procedure at temperatures up to 1800°C. Different physical
characteristics (density, coefficient of thermal expansion, glass transition and crystallization peak temperatures) have been
determined for a 35B2O3-40Al2O3-25Y2O3 glass composition (in mol.%). By using a predictive model and some NMR structural data, different elastic moduli (Young's
modulus, bulk modulus, shear modulus and Poisson's ratio) have been calculated. The devitrification behaviour has also been
studied. Internal crystallization is the dominant mechanism and a new (Y, Al)BO3 ternary phase has been characterized by X-ray powder diffraction. The temperature and time nucleation dependence have been
determined from DTA experiments as well as the crystallization kinetics (i.e. the Avrami exponent and the activation energy
for crystal growth). 相似文献
100.
Sebastián López Gustavo M. Callicó Félix Tobajas Valentín de Armas José F. López Roberto Sarmiento 《ETRI Journal》2008,30(6):862-864
This letter presents a novel approach for organizing computational resources into groups within H.264/AVC motion estimation architectures, leading to reductions of up to 75% in the equivalent gate count with respect to state‐of‐the‐art designs. 相似文献