硼离子注入对多晶Ni力学性能及微观结构的影响

用能量为50keV,剂量为3×10~(17)ions/cm_2的B~+注入多晶Ni,通过力学性能实验研究了多晶Ni注入前后表面硬度和疲劳性能的变化,以及多晶Ni表面层注入和疲劳前后化学成分、滑移特征、裂纹萌生、断裂方式和微观结构的变化。结果表明,B~+注入多晶Ni后,表面区域形成一个不同组织结构的由Ni-B非晶、Ni_3B和Ni_4B_3第二相以及辐照损伤组成的多层次的注入层,提高了多晶Ni的表面硬度,并使其疲劳极限提高16％。探讨了B~+注入影响多晶Ni疲劳极限的几种可能机制。     

Effect of solid fraction on steel-mushy Cu-graphite pressing bonding

The pressing bonding of steel plate to QTi3.5-3.5graphite slurry was studied. The bonding conditions were 620℃ for preheating temperature of steel plate, 530℃ for preheating temperature of dies, 50 MPa for pressure and 2 min for pressing time. The relationship between the solid fraction of QTi3.5-3.5graphite slurry and the interracial mechanical property of bonding plate was obtained. The results show that when the solid fraction of QTi3.5-3.5graphite slurry is smaller than 45.8%, the interracial shear strength of bonding plate increases with the increasing of solid fraction. When the solid fraction is larger than 45.8%, the interracial shear strength decreases with the increasing of solid fraction. When the solid fraction is 45.8%, the largest interracial shear strength of bonding plate 127 MPa can be got, and the interface is made up of Fe-Cu solid solution.     

38CrSi钢表面纳米结构层力学性能的研究

采用超音速微粒轰击技术在38CrSi合金钢表面制备了厚度约为25μm纳米晶层.利用X射线衍射、扫描电镜和透射电镜对表面结构进行分析.纳米结构层的最表面层的晶粒尺寸约为16nm,晶粒尺寸随着距表面距离的增加而增大.利用纳米压痕仪对表面纳米结构层的力学性能进行研究,结果表明,当表面晶粒尺寸降低到纳米量级时力学性能明显改善,最表面纳米结构层的硬度是基体的2倍左右,并服从Hall-Petch关系;表面纳米结构层的弹性恢复系数明显提高;利用该方法制备的纳米晶对弹性模量的影响较小;对表面纳米化样品进行低温退火处理可使纳米结构层的性能更加稳定.分析表明表面纳米结构层力学性能的改善主要是表面晶粒细化的结果.     

四辊轧机轧辊弹性变形解析模块的开发

采用影响函数方法开发了四辊轧机轧辊弹性变形解析模块，完善了辊间压扁和工作辊压扁影响函数计算模型，克服了轧辊压扁影响函数计算过程浮点数被零除的缺陷，提出了平滑指数和收敛指标取值的处理方法，有效地解决了四辊轧机辊系弹性变形计算精度及收敛问题。该模块适应于普通四辊轧机、PC轧机和CVC轧机轧辊弹性变形计算，为热轧带钢板形控制提供了解析工具。     

基于神经网络的FCD絮凝控制系统的研究

神经网络具有很强的自学习和自适应能力,对于大滞后、非线性的复杂系统有较好的控制效果.针对水处理过程中系统环境不断变化,特别是流量有较大、频繁变化的情况下,在FCD絮凝控制系统的基础上,提出了神经网络控制方法.解决了混凝控制中的目标等效直径动态确定问题.实际运行表明,该方法取得了很好的控制效果,具有广阔的应用前景.     

Determination of N-nitrosodimethylamine at part-per-trillion levels in drinking waters and contaminated groundwaters

The carcinogen N-nitrosodimethylamine (NDMA) may be quantitated routinely at ultratrace (ng/L) levels in drinking water or contaminated groundwater. The aqueous sample is passed through a preconditioned Empore C18 filter disk to remove neutral nonpolar species and then extracted continuously overnight with highest purity dichloromethane. The latter is then concentrated to 1 mL, and a large aliquot (up to 200 microL) is loaded onto a dual-stage carbon sorbent trap, after which the solvent is removed with ultrapure helium. The concentrated residues are then injected onto a gas chromatographic column using a short-path thermal desorber. NDMA is selectively detected using a chemiluminescent nitrogen detector (CLND) operated in its nitrosamine-selective mode. The reporting limit for this procedure, evaluated using two independent statistically unbiased protocols, is 2 ng of NDMA/L. A related procedure, employing an automatic sampler instead of the short-path thermal desorber, provides convenient analysis of heavily contaminated samples and exhibits a reporting limit (same protocols cited previously) of 110 ng of NDMA/L. When the two methods are used together in a "two-tiered" protocol, NDMA concentrations spanning 4 orders of magnitude (ng/L to microgram/L levels) may be measured routinely. The low-level procedure employing only the short-path thermal desorber was applied successfully to three sources of drinking water, where NDMA concentrations ranged between 2 and 10 ng of NDMA/L. The two-tiered protocol was applied to a series of contaminated groundwaters whose NMDA concentrations ranged between approximately 10-7000 ng of NDMA/L. The results agreed with those obtained from an independent collaborating laboratory, which used a different analytical procedure.     

Improved measurement of transketolase activity in the assessment of "TPP effect"

The indirect estimation of thiamine levels in human blood by measuring thiamine pyrophosphate effect on erythrocyte transketolase activity is the method of choice in most clinical laboratories. We describe here an optimized, time-saving, and accurate method to determine the thiamine pyrophosphate effect in as many as 16 blood samples simultaneously. The method is based on a multi-point determination using a computer remote-controlled microplate reader. For multiple sample handling, three pooled reaction mixtures are freshly prepared and loaded onto a 96 well microtitre plate. A pre-written software is then initiated to remote-control the system. The data is retrieved and processed to calculate thiamine pyrophosphate effect by a self-written "macro" on a "Quattro-Pro" worksheet database. This method proves to be highly accurate (coefficient of variance: 2.7%), reproducible (coefficient of variance: 4.1%) and economical.     

Effects of antioxidant state on individual susceptibility to silicosis (an experimental study)

The authors proved that animals having higher natural antioxidant activity and lower intensity of lipid peroxidation are more resistant to fibrogenic effects of quartz. The peritoneal macrophages obtained from those animals show higher resistance to quartz exposure "in vitro". Parameters characterizing antioxidant system should be included into a group of indexes describing propensity to silicosis.     

Effects of subject- versus experimenter-selected reinforcers on the behavior of individuals with profound developmental disabilities

Results from a number of studies have shown that individuals with profound developmental disabilities often show differential approach behavior to stimuli presented in a variety of formats, and that such behavior is a reasonably good predictor of reinforcement effects when these "preferred" stimuli are used subsequently in a contingent arrangement. Recent data suggest that reinforcement effects may be enhanced further by allowing individuals to select, just prior to training sessions, which (of several) preferred stimuli would be used as reinforcers, but whether this method is superior to one based on selection by a teacher or therapist has not been adequately addressed. We compared the effects of these two methods of reinforcer selection on rates of responding on a free-operant task, using stimuli previously identified as potential reinforcers. Results obtained with 4 subjects indicated little or no difference in reinforcement effects when stimuli were selected by subjects rather than experimenters. Implications of these results with respect to choice and its relation to reinforcement are discussed.     

考虑频率与区间联络线功率安全约束的两区互联电力系统机组组合

随着电源结构与电网形态的转变,互联电力系统频率时空分布特征日益显著,区域频率差异与区间联络线功率振荡增大,基于统一频率假设的频率安全约束机组组合方法不再适用。针对考虑频率时空分布特征的两区互联电力系统安全约束机组组合,推导区域频率与区间联络线功率闭式解,并基于闭式解的两项划分,推得区域频率最低点、最大变化率、准稳态值以及区间联络线功率振荡峰值、准稳态值等一系列解析安全量化指标。基于所得指标,构建考虑区域频率与区间联络线功率安全约束的机组组合模型。并根据调度模式与指标特点,提出兼顾区域能力保障与区间能力协调的两级两阶段迭代求解算法。结果表明,所得指标可准确描述两区互联电力系统的安全特征,所提模型和算法可有效保障两区互联电力系统机组组合方案的运行安全。