沈阳含蜡油稀释三榨脱蜡新工艺

本文研制出一种新型的含蜡油稀释三榨脱蜡新工艺,该工艺对加工沈北减二线含蜡油十分有效,提高了石蜡质量与产量。     

Seeded Crystallization of Leucite

The leucite crystallization kinetics from a hydrothermally derived precursor seeded with nano-crystalline leucite was investigated by X-ray diffraction and non-isothermal differential thermal analysis. The nano-crystalline leucite was prepared by high-energy milling of high-purity leucite powder and the leucite precursor was prepared by the hydrothermal method of silica sol, aluminum nitrate, and potassium nitrate. After the seeds were introduced, the crystallization temperature of the precursor was lowered by 100°C and the transition phase kalsilite did not appear during the crystallization process. When the seeded precursor was heat treated at 700°C, a small amount of cubic leucite was stabilized to room temperature. The seeded precursor showed an exothermic peak between 800° and 920°C under different heating rates. The activation energy for the growth of leucite from the seeded precursor was 256(SD9) kJ/mol.     

Synthesis and characterization of copolythiophene

Copolythiophenes (Co‐PTs), poly(3‐hexylthiophene‐co‐3‐thiophene carboxylic acid) (P3HT‐TCa), poly(3‐hexyloxylthiophene‐co‐3‐thiophene carboxylic acid) (P3HOT‐TCa), and poly(3‐phenylthiophene‐co‐3‐thiophene carboxylic acid) (P3PhT‐TCa), were synthesized by chemical oxidized polymerization to investigate the effect of copolymerization on the properties of polythiophenes (PTs). Gel permeation chromatography showed that the molecular weight (MW) of Co‐PT was lower than that of homopolythiophene. Fourier transform infrared (FTIR) spectra indicated that the copolymerization was successful between the monomers. The λ_max of Co‐PTs gave a “blue shift” in ultraviolet‐visible (UV‐VIS) spectra. Photoluminescence (PL) spectra showed that the PL intensity of Co‐PT became weaker than that of homopolythiophene and the disappearance of PL had been observed in P3HOT‐TCa. The thermal stability of Co‐PT was influenced by the carboxyl for its low decomposition temperature. Furthermore, the copolymerization between multi‐wall carbon nanotube containing thiophene ring (MWNT‐Th) and 3‐hexyloxylthiphene could also take place successfully. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 2007     

民间传统御寒器具——火桶设计研究

＂火桶＂是南方传统的御寒器物,它具有造型简单,取材方便,功能实用多样的特点,凝聚了民间朴素造物的思想。同时,火桶所具有着深厚的人文特点和文化内涵。文章以黔东南镇远地区民间火桶为例,分析其形态、结构、功能及人机关系等内容,探究民间造物的设计巧思。     

CaO-SiO2系玻璃的析晶动力学研究

利用溶胶-凝胶法制得CaO-SiO2系基础玻璃,通过差热分析曲线分析质量比为CaO-SiO2玻璃的析晶能力。经分析,其析晶活化能E=457.1kJ·mol-1,而晶化生长指数是随升温速率的不同而不同,速率越大,晶化生长指数越小。     

基于概率支持向量回归的产品设计时间预测模型

为使产品设计时间预测既克服小样本、异方差噪声问题,又提供除预测值以外的其他有用信息,建立概率支持向量回归(PSVR)模型。首先,在异方差回归模型基础上设计概率约束条件,以使预测值以较大概率位于真实值的某邻域,结合具有参数不敏感损失函数的支持向量回归确定优化目标,提出PSVR。然后,将最大完工时间知识嵌入进PSVR的约束条件,用以确定真实值邻域的宽度,将交叉验证与遗传算法相结合以确定PSVR的相关参数。最后,以注塑模具设计的实例进行分析,结果表明基于PSVR的时间预测方法可同时提供有效的预测值和预测区间。     

铝箔纸胶粘剂的制备

由醋酸乙烯和丙烯酸酯所制得的共聚物，能够极大地提高乳液对铝箔和纸张之间的粘合力，通过调整保护胶体聚乙烯醇的用量和增塑剂邻苯二甲酸二丁酯在反应过程中的不同加入方式，可以控制和生产所需要的乳液粘度，流平剂的加入，则改良了乳液在铝箔上胶时的流平性。     

Internet上化学化工资源

详细介绍了Internet上的化学化工资源及域名地址。     

Alekseevskii-Tate revisited:An extension to the modified hydrodynamic theory of long rod penetration

The modified hydrodynamic theory of long rod penetration into semi-infinite targets was established independently by Alek-seevskii and Tate over forty years ago and since then many investigators contributed much to the development of the high speed penetration mechanics.However,in all the models proposed so far,the target resistance Rt is not well defined and usually determined by adjusting it until the predicted depth of penetration comes to an agreement with experimental data.In this paper,assumptions are...     

中国银行利率风险实证分析

随着中国融入世界的步伐加快,加入WTO中要求中国放开金融市场的开放程度,利率管制的放松也将逐步的实行,利率风险日益成为中国商业银行面临的重要风险之一。本文从理论和实践角度对中国商业银行的利率风险进行了分析和研究,剖析中国商业银行存在的诸多障碍,指出了商业银行风险管理中存在的问题,并提出中国商业银行利率风险管理建议。