便携式GC-MS在应急监测中的应用

随着我国经济的高速发展,企业生产的不断扩张,企业的环境突发事故的多变性,对现场监测提出了更高的要求。建立便携式GC-MS,由于其体积小,分析精度高,非常适合于现场挥发性有机物的分析,在国内已被成功用于多起现场环境应急监测工作,本文以一次监测实例说明通过充分利用该仪器快速检测极低浓度挥发性有机污染物的功能,可将之进一步应用于被污染环境空气的实时现场监测,从而为复杂情况下环境污染源的快速排查工作提供强有力的技术支持。     

紧急切断阀过流性能检测装置的研制

文章介绍了紧急切断阀过流性能检测装置的总体设计方案,解决了紧急切断阀的自动夹紧的关键问题和人工读取试验结果的误差问题。通过本装置,能够实现紧急切断阀密封性能、耐压性能和过流性能试验。电脑检测系统自动记录相关试验数据,自动判断其性能是否符合有关标准要求并打印出报告,有效地提高紧急切断阀检验结果的准确性。     

儿童用品中邻苯二甲酸盐的检测

文章采用超声震荡萃取—气相色谱法建立测定儿童用品中邻苯二甲酸酯的方法;以正己烷为萃取溶剂,然后采用气相色谱法—氢火焰离子检测器,进行检测分析,该方法的平均回收率为69.0%~103.2%,相对平均偏差为1.8%~5.9%。该方法用于儿童用品样品中14种邻苯二甲酸酯的测定,具有较好的准确性。     

不同溶剂对野葛中葛根素提取效果影响的研究

目的考察不同溶剂对葛根素提取效果的影响。方法以水和不同浓度的乙醇提取野葛根中的葛根素,以葛根素的提取率和含量为考察指标,通过L9(34)正交试验,比较不同溶剂提取的最佳条件。结果热水提取法的最适条件为料水比1∶10、提取时间2.0 h、提取次数2次;醇提的最佳条件为料液比1∶6,提取时间2.0 h,乙醇体积分数为30%,提取3次。结论优选的两种溶剂提取工艺条件都合理可行,相比之下,水提取的综合指标更高一些。     

新型α+β双相钛合金板抗高速冲击损伤行为研究

采用直径7.5 mm钢丸对新型Ti-Mo-V系α+β双相钛合金板材进行高速冲击试验,使用光学显微镜及扫描电镜,对等轴组织板材抗高速冲击损伤行为进行分析。结果表明：钢丸高速冲击后,损伤部位均未观察到明显的分区现象。冲击着板瞬间,相比于钢丸垂直高速冲击,钢丸冲击方向与板法线方向存在较小偏角时,板材更易发生高速冲击破坏失效,沿板材正面冲击损伤中轴线侧剖后可观察到非对称形态的冲击损伤。冲击损伤部位均形成绝热剪切带,主要分布在正面冲击损伤部位中心及两侧区域,其分布形式主要包括：(1)在冲击损伤中心处呈半弧状分布;(2)在冲击损伤部位两侧沿高速冲击方向约呈45°分布,绝热剪切失效是板材防护失效的主要原因。     

测井资料处理软件的开发

本文详细介绍了固体矿产测井中资料的各种实用处理方法、计算模型.其软件的屏幕解释分层功能不仅能对煤层(矿层)进行分层定厚,还可进行快捷方便的全孔岩性解释和复杂煤层(矿层)的结构分析.通过对测井资料的综合处理,可以计算岩石强度参数,煤质参数和岩石沙、泥、水百分含量,实现了计算机的自动成图,成果资料的多样化输出,极大提高了测井资料处理的精度和速度.     

A Survey on Routing Algorithms for Opportunistic Mobile Social Networks

Opportunistic Mobile Social Networks(OMSNs)are kind of Delay Tolerant Networks(DTNs)that leverage characteristics of Mobile Ad Hoc Networks(MANETs)and Social Networks,particularly the social features,to boost performance of routing algorithms.Users in OMSNs communicate to share and disseminate data to meet needs for variety of applications.Such networks have attracted tremendous attention lately due to the data transmission requirement from emerging applications such as IoT and smart city initiatives.Devices carried by human is the carrier of message transmission,so the social features of human can be used to improve the ability of data transmission.In this paper,we conduct a comparative survey on routing algorithms in OMSNs.We first analyze routing algorithms based on three social features.Since node selfishness is not really considered previously in aforementioned routing algorithms,but has significant impact on network performance,we treat node selfishness as another social feature,classify and elaborate routing algorithms based on incentive mechanism.To assess the impact of social features on routing algorithms,we conducted simulation for six routing algorithms and analyzed the simulation result.Finally,we conclude the paper with challenges on design of routing in OMSNs and point out some future research directions.     

电磁兼容技术研究现状与趋势

本文在阐述电磁兼容概念的基础上,对电磁兼容技术的发展、电磁兼容理论研究、电磁兼容标准、测试技术以及发展趋势进行了综述.     

屈家岭管理区图斑赋值方法研究

在土地质量评价前,为了使未采样的空白图斑有一个最接近实际的值,需要对赋值方法进行研究,可以最大程度地保证评价结果的合理性和真实性.选取1 km2赋值研究区,采集样品30件,利用三种不同赋值方法进行赋值评价,研究结果表明按照耕园草图斑10件/km2的采样密度,开展屈家岭管理区1:5万土地质量地球化学调查,利用距离加权反比...     

Hierarchically 1D CdS decorated on 2D perovskite-type La_2Ti_2O_7 nanosheet hybrids with enhanced photocatalytic performance

In this paper,a heterojunction of hierarchically one-dimensional(1 D) cadmium sulfide(CdS) nanowires decorated on the two-dimensional(2 D) La_2 Ti_2 O_7(LTO)has been fabricated by a simple two-step hydrothermal process.The structure,morphology and surface chemical composition of CdS/LTO were studied by a variety of characterizations,in which the X-ray photoelectron spectroscopy(XPS) results showed a strong interaction between CdS and LTO through S-O bonds.The type Ⅱ band alignment of CdS/LTO for favorable electron transfer from CdS to LTO and hole transfer from LTO to CdS was clarified by ultraviolet-visible(UV-Vis) diffuse reflectance spectroscopy and Mott-Schottky(M-S) plot measurements.In the absence of any co-catalyst,H_2 production from water splitting and Rhodamine B(RhB) decomposition in aqueous solution were carried out to evaluate the photocatalytic activities,showing that the photocatalytic performance of CdS/LTO was superior to that of pure LTO and CdS under visible light and simulated sunlight.The optimal CdS content in the CdS/LTO system was determined to be 7.5 wt%.The present results show an effective pathway to design a 1 D/2 D heterojunction photocatalyst in the face of overwhelming problems of energy crisis and environmental pollution.