Decreasing miscibility with greater heterogeneity in ternary polymer blend: poly(cyclohexyl methacrylate), poly(α‐methyl styrene) and poly(4‐methyl styrene)

A ternary blend system comprising poly(cyclohexyl methacrylate) (PCHMA), poly(α‐methyl styrene) (PαMS) and poly(4‐methyl styrene) (P4MS) was investigated by thermal analysis, optical and scanning electron microscopy. Ternary phase behaviour was compared with the behaviour for the three constituent binary pairs. This study showed that the ternary blends of PCHMA/PαMS/P4MS in most compositions were miscible, with an apparent glass transition temperature (T_g) and distinct cloud‐point transitions, which were located at lower temperatures than their binary counterparts. However, in a closed‐loop range of compositions roughly near the centre of the triangular phase diagram, some ternary blends displayed phase separation with heterogeneity domains of about 1 µm. Therefore, it is properly concluded that ternary PCHMA/PαMS/P4M is partially miscible with a small closed‐loop immisciblity range, even though all the constituent binary pairs are fully miscible. Thermodynamic backgrounds leading to decreased miscibility and greater heterogeneity in a ternary polymer system in comparison with the binary counterparts are discussed. © 2003 Society of Chemical Industry     

Threshold‐Based Camera Motion Characterization of MPEG Video

We propose an efficient scheme for camera motion characterization in MPEG‐compressed video. The proposed scheme detects six types of basic camera motions through threshold‐based qualitative interpretation, in which fixed thresholds are applied to motion model parameters estimated from MPEG motion vectors (MVs). The efficiency and robustness of the scheme are validated by the experiment with real compressed video sequences.     

Self-Consistent Effects on the Starting Current of Gyrotron Oscillators

Self-consistent effects on the starting current of gyrotron oscillators are examined. Field profiles in the open cavity are shown to be sensitive to the interaction dynamics. This can either significantly raise or lower the oscillation threshold, particularly for the low-Q modes. The transition from resonant-mode oscillations at the low magnetic field to backward-wave oscillations at the high magnetic field is demonstrated.     

Medium access protocol design for delay-guaranteed multicode CDMA multimedia networks

To enable multimedia real-time applications over next-generation wireless code-division multiple access (CDMA) packet-switching networks, previous efforts show a proper scheduling policy is the key to provide delay-guaranteed access services to various traffic types with different bit error rate (BER) requirements. Considering the support of the prevailing Internet protocol (IP) with variable-length packets in future mobile networks, we develop a mathematically delay-optimal medium access control (MAC) protocol over multicode CDMA (MC-CDMA) environments under the continuous-time assumption. From our investigations, we suggest that a good MAC protocol should be designed by using a proper single-server scheduling policy to guarantee packet-delay, and controlling the maximal number of simultaneous spreading-code transmissions to maintain the required BER. We further evaluate the performance of some MC-CDMA MAC protocols supporting QoS on BER and packet-delay, and show that MAC schemes conforming to our design rules give better performance on packet-delay when maintaining acceptable BER of various traffic types.     

Catalytic dehydrogenation of ethylbenzene with carbon dioxide: promotional effect of antimony in supported vanadium–antimony oxide catalyst

Alumina-supported vanadium oxide, VO_x/Al₂O₃, and binary vanadium–antimony oxides, VSbO_x/Al₂O₃, have been tested in the ethylbenzene dehydrogenation with carbon dioxide and characterized by S_BET, X-ray diffraction, X-ray photoelectron spectroscopy, hydrogen temperature-programmed reduction and CO₂ pulse methods. VSbO_x/Al₂O₃ exhibited enhanced catalytic activity and especially on-stream stability compared to VO_x/Al₂O₃ catalyst. Incorporation of antimony into VO_x/Al₂O₃ increased dispersion of active VO_x species, enhanced redox properties of the systems and formed a new mixed vanadium–antimony oxide phase in the most catalytically efficient V_0.43Sb_0.57O_x/Al₂O₃ system.     

基于EPP模式下的数据采集系统

介绍了一种基于并口EPP模式通讯的数据采集系统的设计方法,该系统以ADSP2 1 81、E PLD为核心器件,AD7331 1芯片为模拟信号输入输出接口,非常适合便携式数据采集系统     

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天然气脱除Ｈ２Ｓ和ＣＯ２是天然气净化领域经常遇到的问题。Ｈ２Ｓ与醇胺的反应属瞬间质子反应，ＣＯ２与醇胺的反应则复杂得多，醇胺溶液对Ｈ２Ｓ的选择性分离主要依靠ＣＯ２与醇胺的反应速度差异来实现。文章介绍了伯胺，仲胺，叔胺及空间位阻胺溶液反应的机理和动力学。     

基于网络的家电产品故障诊断系统研究

介绍了基于网络的家电产品故障诊断系统的硬件拓扑结构、软件平台及系统开发。系统在硬件上采用了多种网络平台搭建方式及综合连接技术，软件上采用了IDRS诊断模型和基于事例的最新诊断技术。这也是诊断研究和应用的新领域。     

An electrooptic intensity modulator with improved linearity

A highly linear electrooptic modulator has been designed, fabricated, and evaluated. The design of this modulator consists of only a simple modification to the directional coupler. Two-tone testing has demonstrated that, for an optical modulation depth of 30% per channel, the third-order intermodulation distortion is more than 30 dB lower than that of the conventional directional coupler or Mach-Zehnder modulators. This improvement was not observed to be accompanied by any increase in second harmonic distortion. Also included are results of two-tone computer simulations which predict the improvement in linearity of this device for a range of modulation depths.<>     

Two schemes for detecting CMOS analog faults

A design-for-testability scheme for detecting CMOS analog faults was reported by Favalli et al. (see ibid., vol.25, no.5, p.1239-46, 1990). The authors propose two alternative designs, one for small circuits and another for large circuits, which require significantly less area overhead (about 1/4 to 1/3) than that of Favalli's design. With the proposed modification in the first design, the untestable problem, which occurred in Favalli's design, can be alleviated. Furthermore, the proposed schemes are also fit to be implemented in VLSI circuits