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991.
RM Martín‐Aranda E Ortega‐Cantero ML Rojas‐Cervantes MA Vicente‐Rodríguez MA Baares‐Muoz 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2005,80(2):234-238
α,β‐Unsaturated nitriles have been synthesized by Knoevenagel condensation of a carbonylic compound with malononitrile, assisted by sonochemical irradiation. Two alkaline‐promoted clays (Li+‐ and Cs+‐exchanged saponites) have been employed as catalysts. The influence of the carbonylic compound (benzaldehyde or cyclohexanone) and the use of a solvent on the catalytic activity have been studied. Remarkable increase in the conversion values has been found when the reaction is activated by ultrasound, as compared with the thermal activation. In this green, solvent‐free procedure, α,β‐unsaturated nitriles have been produced in very high yields (97%) when the Cs+‐saponite is used as catalyst. Copyright © 2004 Society of Chemical Industry 相似文献
992.
Against the background of increasing nutrient concentrations in Irish water bodies, this study set out to gain information on the potential of agricultural grassland to lose nutrients to water. Overland flow, flow from artificial subsurface drains and stream flow were gauged and sampled during heavy rainfall events. Dissolved reactive phosphorus (DRP), potassium (K), total ammonia (TA), and total oxidised nitrogen (TON) were measured in water samples. When the nutrient concentrations in water were examined in relation to the grassland management practices of the study catchments it emerged that soil P levels, the application of organic and inorganic fertilisers before heavy rainfall and the presence of grazing animals could all influence nutrient concentrations in surface and subsurface drainage water. Overall, the drainage characteristics of soil were found to have a considerable influence on the potential of land to lose nutrients to water. 相似文献
993.
Dixon J. Moran L. Rodriguez E. Domke R. 《Proceedings of the IEEE. Institute of Electrical and Electronics Engineers》2005,93(12):2144-2164
This paper presents an overview of the state of the art in reactive power compensation technologies. The principles of operation, design characteristics and application examples of Var compensators implemented with thyristors and self-commutated converters are presented. Static Var generators are used to improve voltage regulation, stability, and power factor in ac transmission and distribution systems. Examples obtained from relevant applications describing the use of reactive power compensators implemented with new static Var technologies are also described. 相似文献
994.
The effect of nucleator additives on the surface relief and the degree of crystallization of material intended for the dentine and enamel layers of artificial denture is considered. It is established that hydroxyapatite additive is optimal for producing the required relief in the prime and dentine layers. 相似文献
995.
The forces of surface interaction between glass batch components are considered. A comparison between capillary and gravitational forces for particles of different sizes at different stages of glass batch preparation is carried out. The dependences of capillary force on the volume of liquid and the distance between particles are discussed.__________Translated from Steklo i Keramika, No. 3, pp. 7 – 9, March, 2005. 相似文献
996.
Goni O. Hossain F. Yusuf S.U. Rahman M. Kaneko E. Takahashi H. 《Power Delivery, IEEE Transactions on》2006,21(4):1778-1786
Simulation of very fast surge phenomena in a three-dimensional (3-D) structure requires a method based on Maxwell's equations, such as the finite-difference time-domain (FDTD) method or the method of moments, because circuit-equation-based methods cannot handle the phenomena. This paper uses a method of thin-wire representation of the vertical conductor system for the FDTD method which is suitable for the 3-D surge simulation. The thin-wire representation is indispensable to simulate electromagnetic surges on wires or steel frames in which the radius is smaller than a discretized space step used in the FDTD simulation. In this paper, a general surge analysis program named the virtual surge test lab based on the Maxwell's equations formulated by the FDTD method, is used to simulate the surge phenomena of a vertical conductor, including the effects of horizontal wave incidence and vertical wave incidence. Experimental results on the reduced scale model have been presented in order to compare among the simulation results by the FDTD method and the results using numerical electromagnetic code based on the MoM. 相似文献
997.
Results of a study of the wettability of the tundish periclase lining by molten steel using a sessile drop method are presented.
The wetting angle θ tends to decrease with increase in temperature and contact time on adding glass fiber and Fe2O3 powder in excess of 2% to the magnesite powder; a similar effect is observed in steels high in manganese. An increase in
angle θ is observed on adding carbon fiber or glass fiber (not in excess of 1%) to the magnesite powder; the angle θ tends
to increase with increase in MgO powder grain size and with carbon contained in steel in excess of 0.04%.
__________
Translated from Novye Ogneupory, No. 1, pp. 63–68, January, 2006. 相似文献
998.
E. GLASER 《Journal of microscopy》2005,218(1):1-5
It is well known that the estimation of an object's volume by means of serial cross-sections, the so-called Cavalieri method, yields an unbiased estimate. But by itself it provides no means by which to estimate how precise this estimate is unless the shape of the volume is fully known beforehand. This knowledge can only be partially determined from the serial section information that is collected. Methods have been developed that claim to surmount this difficulty by using the serial section data to create a mathematical model of the volume's shape properties. The model then is used to estimate (predict) the precision of the volume estimate (its CE) from the single set of data available. Unfortunately, the theory underlying the model is flawed and so the model itself amounts to no more than an unsubstantiated guess about the shape of the volume. Therefore, the precision of the volume estimates that one obtains from the method is only as good as the model and this cannot be ascertained from the single set of acquired data. In this letter I explain the inadequacies of the modelling method. I suggest that it be used only with caution, if at all. Instead I suggest two alternative ways to predict the CE, one that is based upon a rule-of-thumb approach to the object's shape, and another that is based upon spectral analysis of the measurement function and that is easy to implement with available computer software. 相似文献
999.
1000.
Plane-parallel packing of Mellapack 250X type (without perforations) is considered. Equation systems are given that describe the motion and heat and mass transfer in a layer of liquid and vapor. Calculations have been performed on nonstationary heat and mass transfer in cells of several types by the use of the STAR-CD software and the subroutines Star-Design and Pro-amm. Graphs are given for the velocity and vapor pressure distributions in cells of circular and triangular shape, as well as for the oxygen distribution in circular cells. 相似文献