In the quest on improving composite formulations for environmental sustainability, maleic acid (MA) cross-linked poly(vinyl alcohol) (PVA)-α-chitin composites reinforced by oil palm empty fruit bunch fibers (OPEFB)-derived nanocellulose crystals (NCC) had been successfully prepared. Based on the Fourier transform infrared (FTIR) spectroscopic analysis, it was proven that molecular interactions of the cross-linker to the polymeric networks was through conjugated ester linkage. Differential scanning calorimetry (DSC) showed that the influence of MA was minimal toward crystallization in the PVA/chitin/NCC composite. Maximum tensile strength, elongation at break and Young's modulus of the respective PVA/chitin/NCC composites were achieved at different content of MA, dependent on the PVA/chitin mass ratio. Among all compositions, a maximum Young's modulus was achieved at 30 wt% MA loading in PVA/chitin-30/NCC, amounting to 2,413.81 ± 167.36 MPa. Moreover, the mechanical properties and selected physicochemical properties (swelling, gel content, and contact angle) of the PVA/chitin/NCC composites could be tailored by varying the chitin content (10–30 wt%) and MA content (10–50 wt% based on total mass of composite). In brief, this chemically cross-linked PVA-based biocomposites formulated with sustainable resources exhibited tunable physicochemical and mechanical properties. 相似文献
This paper studies the thermal behavior of a wireless powered micropump operated using thermo-pneumatic actuation. Numerical analysis was performed to investigate the temporal conduction of the planar inductor-capacitor (LC) wireless heater and the heating chamber. The result shows that the temperature at the heating chamber reaches steady state temperature of 46.7°C within 40 seconds. The finding was further verified with experimental works through the fabrication of the planar LC heater (RF sensitive actuator) and micropump device using MEMS fabrication technique. The fabricated device delivers a minimum volume of 0.096 μL at the temperature of 29°C after being thermally activated for 10 s. The volume dispensed from the micropump device can precisely controlled by an increase of the electrical heating power within the cut-off input power of 0.22 W. Beyond the power, the heat transfer to the heating chamber exhibits non-linear behavior. In addition, wireless operation of the fabricated device shows successful release of color dye when the micropump is immersed in DI-water containing dish and excited by tuning the RF power.
Low-temperature solders have wide applications in integrated circuits and micro-electromechanical systems packaging. In this
article, a study on Ag-In solder for chip-to-chip thermocompression bonding was carried out. The resulting joint consists
of AgIn2 and Ag9In4 phases, with the latter phase having a melting temperature higher than 400°C. Complete consumption of In solder into a Ag-rich
intermetallic compound is achieved by applying a bond pressure of 1.4 MPa at 180°C for 40 min. We also observe that the bonding
pressure effect enables a Ag-rich phase to be formed within a shorter bonding duration (10 min) at a higher pressure of 1.6 MPa.
Finally, prolonged aging leads to the formation of the final phase of Ag9In4 in the bonded joints. 相似文献
In this paper, modeling of the vibration of cylindrical shell components of space structures incorporating piezoelectric sensor/actuators (S/As) for optimal vibration control is proposed and formulated. The parameters of the control system, which include the placement and sizing of the piezoelectric S/As and the feedback control gains, were considered as design variables and optimized simultaneously. The effect of the amount of piezoelectric patches was investigated as well. The criterion based on the maximization of energy dissipation was employed for the optimization of the control system. A modified real-encoded genetic algorithm (GA) dealing with various constraints has been developed and applied to search for the optimal placement and size of the piezoelectric patches as well as the optimal feedback control gains. The results of three numerical examples, which include a simply supported plate, a simply supported cylindrical shell, and a clamped-simply supported plate, demonstrated significant vibration suppression based on the optimal design of the control system. It was also found that for specific controlled vibration modes, the optimal distribution of the piezoelectric S/As should be located at the areas separated by the nodal lines to achieve the optimal control effect. This finding would be useful for the practical design of smart structures. 相似文献
Two patients with sinus tracts from retained T-fasteners following PEG tube placement are reported. Both patients had the PEG tubes subsequently removed and presented with purulent discharge and granulations near well-healed gastrostomy sites. The management of this complication and a possible method of prevention are discussed. 相似文献