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71.
Juan P. Escobedo Ellen K. Cerreta Daniel T. Martinez Carl P. Trujillo Ricardo A. Lebensohn George T. Gray III 《Metallurgical and Materials Transactions A》2014,45(13):5877-5882
The influence of temperature on the dynamic tensile behavior of Zr has been investigated. Bullet-shaped Zr samples with two different textures were dynamically extruded at room temperature and 523 K (250 °C). A higher ductility was measured for samples deformed at elevated temperature as compared to those extruded at room temperature. This difference in ductility is discussed in terms of zirconium’s ability to accommodate plastic deformation via thermally enhanced slip activity, as evidenced by examination of the deformed microstructures. 相似文献
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Clay aerogels have many advantages as one of the lowest density family of materials current technology can provide; they possess very low thermal conductivities, high porosities, and high surface areas. Although the mechanical properties of native clay aerogels are rather low, incorporating water‐dispersible polymers into the clay gel before they are processed into aerogel forms can easily produce more robust, low‐density composites. Various processing modifications and additives can be employed to strengthen the aerogel material, but currently, the materials have some notable weaknesses in abrasion resistance, water absorption, and flexural properties. In this study, we employed a low‐cost rubber coating material to quickly and efficiently address all three of these problems. After coating, the aerogels gained significant mechanical reinforcement, a 20‐fold increase in flexural modulus and a 15‐fold increase in yield stress, while exhibiting an increase of only 8% in the thermal conductivity. Improvements such as these can improve the commercial applicability of clay/polymer aerogels as thermal insulation materials. © 2012 Wiley Periodicals, Inc. J Appl Polym Sci, 2012 相似文献
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Rocco P. Viggiano III Edward E. Ball Ronald E. Park Karl W. Haider David A. Schiraldi 《应用聚合物科学杂志》2015,132(39)
The feasibility of incorporating ground recycled polyurethane (PU) foam into clay/polymer aerogels was demonstrated, and a range of compositions were prepared and characterized to determine the effect of variation in the formulations on density and mechanical properties of the resulting materials. This study followed a modified combinatorial approach. Initially, experiments were performed in water using either sodium exchanged montmorillonite or laponite clay, poly(vinyl alcohol) (PVOH) solution as the polymer binder, and the recycled PU foam. Freezing and freeze‐drying the aqueous gels produced aerogels, which were characterized through density and mechanical testing, scanning electron microscopy, and thermal gravimetric analysis. The study was expanded by exploring alternative binder chemistries, including the use of an alginate polymer in place of the PVOH or adding a polyisocyanate as a crosslinking agent for PVOH. The effect of recycled PU foam content, clay type and level, and binder type and level on the mechanical properties of the aerogels were determined and will be discussed herein. © 2015 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2015 , 132, 42586. 相似文献
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Grant O. Cook III Carl D. Sorensen 《Metallurgical and Materials Transactions A》2013,44(13):5754-5772
Partial transient liquid-phase (PTLP) bonding is currently an esoteric joining process with limited applications. However, it has preferable advantages compared with typical joining techniques and is the best joining technique for certain applications. Specifically, it can bond hard-to-join materials as well as dissimilar material types, and bonding is performed at comparatively low temperatures. Part of the difficulty in applying PTLP bonding is finding suitable interlayer combinations (ICs). A novel interlayer selection procedure has been developed to facilitate the identification of ICs that will create successful PTLP bonds and is explained in a companion article. An integral part of the selection procedure is a filtering routine that identifies all possible ICs for a given application. This routine utilizes a set of customizable parameters that are based on key characteristics of PTLP bonding. These parameters include important design considerations such as bonding temperature, target remelting temperature, bond solid type, and interlayer thicknesses. The output from this routine provides a detailed view of each candidate IC along with a broad view of the entire candidate set, greatly facilitating the selection of ideal ICs. This routine provides a new perspective on the PTLP bonding process. In addition, the use of this routine, by way of the accompanying selection procedure, will expand PTLP bonding as a viable joining process. 相似文献
78.
A limit cycle is the stability boundary for linear and non-linear control systems. Hamiltonian mechanics and power flow control are employed to demonstrate this property of limit cycles. The presentation begins with the concept of linear limit cycles which is extended to non-linear limit cycles. Many examples are used to demonstrate these concepts including linear and non-linear oscillators, power engineering, and an extension to a class of plane differential systems. Power flow control based on Hamiltonian mechanics is shown to be applicable to a large class of non-linear systems. Finally, eigenanalysis and flight stability for linear systems are extended to non-linear systems and is referred to as ‘the power flow principle of stability for non-linear systems’. 相似文献
79.
A rapid and selective liquid chromatography–electrospray ionisation mass spectrometry (LC–ESI-MS) method to screen citrus samples for limonoid glucosides and estimate their relative concentrations has been developed. This method utilises a phenyl stationary phase, whereas previous methods have relied on C-18. Samples may be analysed directly without treatment other than dilution. Peak areas from the extracted deprotonated molecular ion mass signals for individual limonoid glucosides were normalised against the sum of the areas to establish their relative concentrations. The method was successfully applied to the analysis of various juice, extracts, and liquid samples of partially purified limonoid glucosides. 相似文献
80.
Computerized displays of continuously acquired audience response measures have become an increasingly common component in television, particularly in political campaign media coverage. However, the effect of such presentations on consumer’s perceptions of both the presenters and their messages remain unclear. To address this concern, simulated computerized continuous response measurement (CRM) graphics were overlaid onto apolitical video content to produce three (negative, neutral, positive) experimental manipulations. The findings revealed considerable symmetry between the valence of the CRM graphics and research participant responses. Evaluations of the presenter and message were significantly more negative following negative CRM graphic manipulation exposure (compared against the neutral and positive conditions) suggesting that CRM graphics can be a powerful device for influencing viewers’ judgments. 相似文献