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11.
A prospective clinical trial comparing adverse postmyelographic effects and myelographic quality of metrizamide and iohexol was conducted. Using a predetermined, randomized assignment, 24 horses exhibiting neurologic signs were administered either metrizamide (180 mgl/ml) or iohexol (180 mgl/ml) via cerebellomedullary puncture. Each horse was evaluated postmyelographically for adverse effects. Myelographic quality was assessed by a numerical scoring method. Adverse effects were observed more frequently with metrizamide (21) compared with iohexol (6) myelography (p < 0.05). Seizures, intensification of preexisting neurologic signs and prolonged anesthetic recovery were the most common complications after myelography. There was no difference in myelographic quality (p > 0.05). We conclude that iohexol is safer than metrizamide for equine myelography and that quality myelograms can be obtained with either contrast medium. 相似文献
12.
High concentrations of Zn2+ are found in presynaptic terminals of excitatory neurons in the CNS. Zn2+ can be released during synaptic activity and modulate postsynaptic receptors, but little is known about the possibility that Zn2+ may enter postsynaptic cells and produce dynamic changes in the intracellular Zn2+ concentration ([Zn2+]i). We used fura-2 and magfura-2 to detect the consequences of Zn2+ influx in cultured neurons under conditions that restrict changes in intracellular Ca2+ and Mg2+ concentrations. The resulting ratio changes for both dyes were reversed completely by the Zn2+ chelator, N,N,N',N'-tetrakis(2-pyridylmethyl)ethylenediamine, indicating that these dyes are measuring changes in [Zn2+]i. We found that fura-2 was useful in measuring small increases in [Zn2+]i associated with exposure to Zn2+ alone that may be mediated by a Na+/Ca2+ exchanger. Magfura-2, which has a lower affinity for Zn2+, was more useful in measuring larger agonist-stimulated increases in [Zn2+]i. The coapplication of 300 microM Zn2+ and 100 microM glutamate/10 microM glycine resulted in a [Zn2+]i increase that was approximately 40-100 nM in magnitude and could be inhibited by the NMDA receptor antagonist, MK-801 (30 microM), or extracellular Na+. This suggests that Zn2+ influx can occur through at least two different pathways, leading to varying increases in [Zn2+]i. These findings demonstrate the feasibility of measuring changes in [Zn2+]i in neurons. 相似文献
13.
The tokamak and tandem mirror concepts are compared with alternate confinement concepts using the criteria established in DOE/ET-0047, An Evaluation of Alternate Magnetic Fusion Concepts 1977. The concepts are evaluated and rated in each of three broad categories: confidence in physics and technology, and reactor desirability. The STARFIRE and MARS reactors are used as a basis for comparing the mainline tokamak and tandem mirror concepts with the alternate concepts evaluated in DOE/ET-0047. Two recent alternate concepts, theohmically heated toroidal experiment (OHTE) and thecompact reversed field pinch reactor (CRFPR), are also evaluated. Results indicate that the physics of the mainline tokamaks and tandem mirrors is better understood than that of most alternate concepts. Both mainline concepts rank near the middle for technology requirements, and both rank near or at the bottom when compared with the reactor desirability of alternate concepts. 相似文献
14.
The surface and bulk microstructure of Mn-Zn ferrite single crystals oxidized at 0.7% o
2 have been investigated using SEM and TEM methods, assisted by energy- dispersive X-ray micro analysis. In samples heat-treated at 1000° C, haematite formed as an irregular surface layer and as laths which grew throughout the bulk, parallel with the {1 1 1 } planes (where F = ferrite). The haematite laths were related epitaxially to the ferrite host through the relationships (0001)H | {1 1 1 }F (where H = haematite) and
. However, it was found that the latter parallelism was not exact because the haematite and ferrite lattices were rotated by 1.1 ± 0.2° about the axis perpendicular to the interface between them (i.e. [0001]H, <1 1 1 >F). The sites for the nucleation of haematite second phase were also observed in highly oxidized ferrite. The formation of small planar defects (< O.1 m in length) in the ferrite, lying parallel to {1 10} planes, is interpreted as the combination of a local shear with the ordering of cation vacancies resulting from the oxidation. Small volumes of other second phases were also recognized, by virtue of both compositional and microstructural differences from the host ferrite. 相似文献
15.
Haixue Yan Hongtao Zhang Rick Ubic Mike Reece Jing Liu Zhijian Shen 《Journal of Materials Science: Materials in Electronics》2006,17(9):657-661
Grain-oriented Aurivillius phase BaBi2Nb2 O9 ceramics were fabricated using Spark Plasma Sintering (SPS). Their relaxor behaviour was confirmed by a strong frequency
dispersion of the dielectric response. The dielectric behaviour has been fitted using different relaxor models. The relaxor
parameters are isotropic, while the dielectric constants are highly anisotropic. The piezoelectric constant d
33 is zero perpendicular and parallel to the hot pressing direction, and the P–E response is dominated by losses. The inability to pole the samples at room temperature is consistent with the T
f temperature (∼
∼115 K) estimated from fitting the experimental data to the Vogel–Fulcher model. This suggests that it may be possible to
observe piezoelectric and ferroelectric properties at very low temperatures. 相似文献
16.
17.
Reece N. Oosterbeek Kalliope I. Margaronis Xiang C. Zhang Serena M. Best Ruth E. Cameron 《Journal of the European Ceramic Society》2021,41(1):901-911
Phosphate glasses for bioresorbable implants display dissolution rates that vary significantly with composition, however currently their mechanisms of dissolution are not well understood. Based on this systematic study we present new insights into these mechanisms. Two-stage dissolution was observed, with time dependence initially parabolic and later linear, and a two-stage model was developed to describe this behaviour. Dissolution was accelerated by lower Ca concentration in the glass, and lower pH in the dissolution medium. A new dissolution mechanism is proposed, involving an initial stage where diffusion-controlled formation of a conversion layer occurs. Once the conversion layer is stabilised, layer dissolution reactions become rate-limiting. Under this mechanism the transition time is sensitive to the nature of the conversion layer and solution conditions. These results reveal the dependence of P2O5–CaO–Na2O glass dissolution on solution pH, and provide new insight into the dissolution mechanisms, particularly regarding the transition between the two dissolution stages. 相似文献
18.
L. Zhao J. M. Klopf C. E. Reece M. J. Kelley 《Materialwissenschaft und Werkstofftechnik》2015,46(7):675-685
Improved energy efficiency and reduced cost are greatly desired for advanced particle accelerators. Progress toward these goals can be made by atomically‐smoothing the interior surface of the niobium superconducting radiofrequency (SRF) accelerator cavities at the heart of these machines. Laser polishing offers a green alternative to the present aggressive chemical processes. We found parameters suitable for polishing niobium in all surface conditions that are expected for cavity production. Careful measurement of the resulting surface chemistry revealed a modest thinning of the surface oxide layer, but no contamination. 相似文献
19.
Crystallographic Structure and Ferroelectricity of (AxLa1−x)2Ti2O7 (A = Sm and Eu) Solid Solutions with High Tc
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Chen Chen Zhipeng Gao Haixue Yan Mike J. Reece 《Journal of the American Ceramic Society》2016,99(2):523-530
The solubility and ferroelectric properties of (AxLa1?x)2Ti2O7 (A = Sm and Eu) solid solutions were investigated. The crystallographic structure of the solid solutions was studied using X‐ray diffraction and Raman spectroscopy. The solubility limits of Eu and Sm in (AxLa1?x) 2Ti2O7 were found to be greater than x = 0.5 and 0.8, respectively. The solid solutions had a monoclinic perovskite‐like layered structure (PLS), similar to that of the pure La2Ti2O7, when x was less than the solubility limit. When x was above the solubility limit the materials were biphase. The biphases of (SmxLa1?x)Ti2O7 (x = 0.9) consisted of (SmxLa1?x)2Ti2O7 with PLS and pure Sm2Ti2O7 with pyrochlore structure, and the biphases of (EuxLa1?x)Ti2O7 (x = 0.6, 0.7, and 0.8) consisted of (EuxLa1?x)2Ti2O7 with PLS structure and La3+ doped Eu2Ti2O7 with pyrochlore structure. The effect of A‐site substitution on the properties of La2Ti2O7 was investigated by measuring the dielectric permittivity and loss at different frequencies and temperatures. The highest piezoelectric constant d33 was 2.8 pC/N for (Sm0.1La0.9)Ti2O7. 相似文献
20.
The crystal structure is reported of a complex between an ethyl derivative of the minor-groove drug furamidine and the dodecanucleotide duplex d(CGCGAATTCGCG)2, which has been refined to 1.85 A resolution and an R factor of 16.6% for data collected at -173 degreesC. An exceptionally large number (220) of water molecules have been located. The majority of these occur in the first coordination shell of solvation. There are extensive networks of connected waters, both in the major and minor grooves. In particular, there are 21 water molecules associated with the minor-groove drug, via hydrogen bonds from the four charged nitrogen atoms. One cluster of four waters is situated in the groove itself; the majority are on the outer edge of the groove, and serve to bridge between the outward-directed drug nitrogen atoms and backbone phosphate oxygen atoms. These bridges are both intra- and inter-strand, with the net effect that the outer edge of the drug molecule is covered by ribbons of water molecules. 相似文献