Detection and quantitation of multiple volatile compounds in tissues by GC and GC/MS

Qualitative and quantitative analysis of tissues and body fluids for multiple volatile organic compounds were performed by a combination of packed and open tubular capillary GC and GC/MS. This paper describes methods for such analyses in a case involving the exposure of two persons to methyl ethyl ketone, methyl isobutyl ketone, toluene and the three isomeric xylenes. Tissue and body fluid concentrations of these substances in the two decedents are presented and discussed briefly.     

Kurzzeitkriechverhalten des Warmarbeitsstahles X40 CrMoV 51

Untersuchung des Kriechverhaltens des Warmarbeitsstahles X40 CrMoV 51, vergütet auf 40 HRC, bei Temperaturen zwischen 500°C und 700°C. Zusammenhang zwischen Bruchverlängerung, Brucheinschnürung und wahrer Dehnung beim Bruch einerseits und Spannung und Temperatur andererseits. Gültigkeit der Monkman-Grant-Regel. Einfache empirische Interpolationsformel für Zeitstanddaten im untersuchten Temperaturbereich, mit der auf anschauliche Weise der Einfluß von Temperatur und Spannung auf die Standzeit bestimmt werden kann.     

A representation of trees by languages I

A tree can be represented by a language consisting of a suitable coding of its finite branches. We investigate this representation and derive a number of reductions between certain equivalence problems for context-free tree grammars and recursive program schemes and the (open) equivalence problem for DPDA's. This is the first part of this work: it is devoted to technical results on prefix-free languages and strict deterministic grammars. Application to context-free tree grammars will be published in the second part.     

Analysis of the exudate produced by Streptococcus mutans SL-1 colonies of sucrose-containing agar media

The watery exudate produced by Streptococcus mutans SL-1 colonies on sucrose-containing agar media was found to contain about 7% (wt/vol) of a water-soluble, branched dextran, 4% sucrose, and smaller (less than 1%) amounts of fructose, Folin-phenol-positive material, and lactic acid.     

Effect of copper and platinum intrauterine devices on endometrial morphology and implantation in the rabbit

The response of the rabbit endometrium to the copper IUD was investigated. A plastic IUD bearing copper foil (42 mm2) was inserted into one horn of the rabbit uterus and a physically similar platinum-bearing IUD in the contralateral horn served as a control. The Pt-IUD caused no tissue damage and little if any inflammatory reaction in ovariectomized, oestrous or pregnant animals, whereas the Cu-IUD produced endometrial ulcers in 14 out of 15 does in all hormonal states. The associated inflammation was particularly intense in the pregnant animals in which a unilateral pyometra was usually present. Despite the endometrial trauma produced, the Cu-IUD was only partly effective as a contraceptive agent, 36% of the ova shed from the ovary ipsilateral to the Cu-IUD implanting, compared with 63% of the ova ipsilateral to the Pt-IUD. However, almost half of the implantation swellings in the copper-bearing horns were abnormally small or distorted in shape at 9 days post coitum. The tissue destruction observed in the rabbit endometrium emphasizes the need for careful histological studies of the effect of the copper IUD on the human uterus.