Mechanical Properties of Dental Porcelain with Different Leucite Particle Sizes

This research aims to investigate the effect of leucite particle size on the mechanical properties of dental porcelain with a similar leucite content and chemical composition. Leucite powders of different particle sizes were synthesized by a hydrothermal method and a high-temperature fusing-crystallization method, respectively. Dental porcelains with different average leucite particle sizes (i.e., 0.5±0.2, 1.2±0.3, and 5±2 μm) were prepared by sintering the mixture of different leucite powders and a low temperature frit. The crystalline phase, crystalline content, relative density, hardness, flexural strength, and fracture toughness of the porcelains were measured by X-ray diffraction (XRD), quantitative XRD analysis, the Archimedes method, a Vickers microhardness tester, a universal testing machine, and a single-edge precracked beam method, respectively. The microcrack density and the distribution of leucite particles were also quantitatively assessed from micrographs. The results showed that the leucite particle size did not have a significant effect on the average of the measured flexural strength, fracture toughness, and hardness of dental porcelains. However, because of a existence of the large number of microcracks, the relative density and the Weibull modulus of the sample groups with an average leucite particle size of 5 μm were statistically lower.     

振动场中HDPE/UHMWPE及其吹塑薄膜的性能

利用电磁振动挤出机制备高密度聚乙烯/超高相对分子质量聚乙烯(HDPE/UHMWPE)共混物,对比了静态和动态下共混吹塑薄膜的力学性能及薄膜的表观,用振动毛细管流变仪测定了静态和动态下共混物的流变行为,用差示量热扫描仪(DSC)探讨了共混物的结晶行为。结果表明,电磁振动挤出机制备的共混物吹制薄膜的力学性能均比稳态下的高;振动态时共混物的结晶度高,结晶峰型更为尖锐;振动力场中的共混物的表观粘度低于稳态的,振动力场改善HDPE/UHMWPE共混物的成型加工性能。     

DC04钢板胀形-渐进复合成形锥形件成形能力的实验研究

为了提高渐进成形过程中板料的成形极限和加工效率,提出了胀形-渐进成形的复合成形方法,通过胀形-渐进成形复合成形锥形件实验,研究了DC04钢板胀形-渐进成形复合成形锥形件和纯渐进成形锥形件的成形极限角和应变变化以及壁厚分布规律。结果表明:预成形高度为h=15 mm和h=25 mm时,复合成形零件的成形极限角分别为α极=66°和α极=69°;采用胀形-渐进成形复合成形锥形件,当胀形的最大减薄量发生在局部渐进成形区内,并且胀形和渐进成形的最大减薄量位置方向相反时,锥形件壁厚趋于均匀,提高了胀形-渐进成形的复合成形能力。     

Oxidation Behavior of NBD 200 Silicon Nitride Ceramics

The oxidation behavior of NBD 200 Si₃N₄ containing 1 wt% MgO sintering aid was investigated in oxygen at 900°-1300°C. The oxide growth followed a parabolic rate law with an apparent activation energy of 260 kJ/mol. The oxide layers were enriched with sodium and magnesium because of outward diffusion of intergranular Na⁺ and Mg²⁺ cations in the ceramics. The 2-4 orders of magnitude higher oxidation rate for NBD 200 Si₃N₄ than for other Si₃N₄ ceramics with a similar amount of MgO could be attributed to the presence of sodium. The oxidation process was most likely rate limited by grain-boundary diffusion of Mg²⁺.     

耐候钢在2.0%NaCl中性溶液中的腐蚀过程

采用电化学阻抗谱技术研究了耐候钢Q400NQR1和09CuPCrNi在2.0％NaCl中性溶液中的腐蚀行为,建立了其腐蚀等效电路模型并分析了其相关电化学参数随时间的演化规律,结果表明,两种耐候钢的溶液腐蚀过程均可以分为四个阶段,即点蚀诱导期、点蚀发展期、腐蚀中期和腐蚀后期;Q400NQR1较09CuPCrNi具有较高的抗溶液腐蚀能力,前者在腐蚀的中期生成保护性较强的内层锈层,而后者形成的内层锈层难以稳定且易于出现均匀腐蚀的现象。     

T6态2090 Al-Li合金在EXCO溶液中的剥蚀行为和剥蚀发展过程中的电化学阻抗谱

采用电化学阻抗谱（EIS）和光学显微镜原位观察等方法研究了T6态峰时效的2090 Al-Li合金在EXCO溶液中的剥蚀行为.在浸泡过程中局部腐蚀形态演变经历了4个阶段：点蚀、晶间腐蚀、剥蚀和剥蚀后期.在点蚀阶段形成的以杂质相为局部阴极生成的大蚀孔成为剥蚀引发的中心,剥蚀鼓泡沿大蚀孔边缘生长,直到把表层以下完全穿透.点蚀引发阶段的EIS由一个高频容抗弧和一个中低频感抗弧构成,在点蚀发展阶段感抗弧消失.晶间腐蚀阶段的EIS的容抗部分中很难分辨出腐蚀区域对应的时间常数,剥蚀发展阶段和剥蚀后期的EIS由两个容抗弧构成.     

低成本Q345系列厚钢板的控轧控冷(TMCP)工艺

以两种不同Mn含量的工业生产连铸板坯为原料,采取控轧控冷(TMCP)工艺,成功试制了20 mm厚低成本Q345钢板。研究表明,终冷温度显著影响试验钢的组织与性能,通过选择合适的终冷温度,两种试验钢的强韧性均能达到GB/T 1591-2008中Q345的要求。提出低成本Q345系列厚钢板的成分与工艺:Mn含量为0.9%(质量分数),两阶段轧制,精轧温度低于890℃,终轧温度为800～850℃,终冷温度为(600±20)℃。     

化学共沉淀法制备NiCuZn铁氧体及其性能研究

利用化学共沉淀法制备了NiCuZn铁氧体微粉,研究了反应温度、搅拌速率和盐溶液流速对前驱体粒径的影响。通过XRD、TEM、激光粒度仪（LPS）、精密阻抗分析仪、振动样品磁强计(VSM)等手段对最优条件下得到的样品进行表征。结果表明：当反应温度为70 ℃,盐溶液的流速为0.5 mL/min,搅拌速率为300 r/min时得到尖晶石相的粉体,粒度约为30 nm。将微粉体在500 ℃预烧,在900 ℃烧结后得到样品的相对密度为98%,起始磁导率μi约为200,品质因数Q约为150。截止频率约为70 MHZ     

氦氖激光器输出功率与总气压的关系

本文介绍了氦氖激光器的氦氖配气压强公式推导和测试方法以及氦氖激光器的输出功率与氦氖总气压的关系。     

热核中子皮厚度的微观研究

本文从扩展Skyrme相互作用出发,利用有限温度自洽半经典(FTSCSC)方法,确定热核核子密度ρ_q.(q=n、p),微观地研究了热核~(40)Ca、~(90)Zr、~(120)Sn在不同温度下的中子皮厚度.