Growth characteristics and kinetics of niobium carbide coating obtained on AISI 52100 by thermal-reactive diffusion technique

Niobium carbide coating was produced by thermal-reactive diffusion technique on AISI 52100 steel in salt bath at 1 123 K, 1 173 K, and 1 223 K for 1, 2, 4, and 6 hours. The salt consisted of borax, sodium fl uoride, boron carbide, and niobium pentoxide. The presence of NbC phase on the steel surface was confi rmed by X-ray diffraction analysis. Microscopic observation showed that niobium carbide coating formed on the substrate was smooth and compact. There was a distinct and fl at interface between the coating and substrate. The micro-hardness of niobium carbide coating was 2892±145HV. The thickness of coating ranged from 1.6 μm to 14μm. The forming kinetics of niobium carbide coating was revealed. Moreover, a contour diagram derived from experimental data was graphed for correct selection of process parameters. Some mathematical equations were built for predicting the coating thickness with predetermined processing temperature and time. The results showed that these mathematical equations are very practical as well as the kinetics equation.     

知识开源化背景下信息安全类课程教学改革初探

本文针对当前知识开源化的现状,结合信息安全类相关课程在北京电子科技学院授课的实际情况,以利用知识开源化所带来的优势,改善课程的教学效果、提高学生的动手实践能力为目的,研究和探讨了信息安全类部分课程的教学模式改革方式和所取得的效果。     

Multiple Venting Behavior of Inner Dust Explosions

Combustion, Explosion, and Shock Waves - Explosion venting experiments of corn starch are carried out in a small-scale container. With the help of a high-speed camera and a pressure sensor, an...     

D杯形砂轮修整碟形金刚石砂轮试验研究

本文采用了D杯形砂轮与碟形砂轮对磨法来修整大直径树脂结合剂碟形金刚石砂轮。在分析研究杯形砂轮修整碟形砂轮的修整原理及修整方式的基础上，用自行研制的专用修整装置，从主轴转速、修整深度、修整工具结合剂类型等方面进行了对比工艺试验研究，总结了杯形砂轮修整碟形砂轮的不同工艺参数与修整效率、修整质量之间的工艺规律。试验结果表明，在本试验条件下主轴转速500r／min，修整深度0．02mm的修整效率较好；细粒度、中等浓度的青铜结合剂杯形金刚石砂轮与粗粒度、高浓度的杯形砂轮修整碟形砂轮相比，后者具有较好的修形效果和修整效率；D杯形砂轮与GC杯形砂轮交替配合使用可以大大提高碟形金刚石砂轮的修形效率和修锐效果。     

基于车磨试验台的超高速陶瓷CBN砂轮研究

本文论述了一个用于超高速磨削试验的陶瓷CBN砂轮的研制过程.通过ANSYS分析我们发现,对于砂轮基盘的材料,钛合金是本次试验最佳的选择;锥形是砂轮形状最佳的选择.基于分析结果和试验台的限制得出了砂轮基盘的精确截型.而且,根据试验数据,我们选择了30%的高韧性CBN500和70%的中等韧性CBN Ⅰ混合磨料及一种低温高强陶瓷结合剂.通过810℃烧结温度得到了理想的砂轮贴片.并经良好的粘结技术制出了用于200m/秒超高速磨削试验的CBN砂轮.最后,该砂轮的良好磨削性能得到了验证.     

高强度耐候钢焊接性分析与研究

通过对高强度耐候钢焊接性分析，采用与之匹配的焊接材料，对高强度耐候钢与不同钢种间焊接接头进行低温抗裂性、力学性能、耐大气腐蚀性能和焊接工艺性等进行试验，并对焊接接头金相组织进行分析，提出了高强度耐候钢焊接工艺及适宜的焊接材料。     

基于工业局域网的微机与PLC数据通信实现方法

以美国A－B公司PLC2系列为例，介绍了一种借助VisualBasic通信控件编制微机与工业。PLC之间数据通信软件的方法。对于不同系列的PLC均能用此法简易地开发出实现微机与PLC通信的软件。     

HA—微孔钛基涂层种植体的复合强度

研究了羟基磷灰石(HA)和中性玻璃(G)的混合涂料在TC4多孔钛基体上的界面复合强度。探讨了中性玻璃含量、基体表面状态以及烧结工艺对这种涂层复合种植体的复合强度的影响。指出:复合的实质是中性玻璃与基体的润湿结合,最合适的玻璃含量为50 wt%,提高复合强度的关键,在于基体表面的TiN蒸镀处理,当TiN厚度为2～3 μm时,复合强度可达7.2 MPa。最佳烧结工艺为:900～950℃/30 min。     

化学共沉淀法制备LixCoO2的高温化学相变过程研究

以从废旧锂离子电池中回收的钴、锂为原料制备了LiCoO2粉体.讨论和分析了不同温度下的热处理对LixCoO2结构的影响.随温度升高,立方相减少,六方层状相增多.600℃时尖晶石相向六方相转变,温度继续升高(650℃～800℃)只有六方层状结构存在.再升至较高温度,层状属性增强,结构出现不稳定性,锂出现挥发,在860℃左右,产生新的相变;经过高温XRD分析,900℃时,出现大量的立方相LixCo1-xO和Co3O4,并随温度持续升高,六方LiCoO2相与立方Co3O4均有所减少,而立方LixCo1-xO相增加,1050℃时以LixCo1-xO为主,当x＜0.07时,立方LixCo1-xO为结构稳定相.     

A comparison between atmospheric water vapour content retrieval methods using MSG2-SEVIRI thermal-IR data

Atmospheric water vapour content (WVC) is a vital parameter in the study of climate change. Various methods have been developed to derive atmospheric WVC from remotely sensed data. In this study, we compared three methods for retrieving atmospheric WVC from thermal infrared data in the Meteosat Second Generation-SEVIRI channels 9 (10.8 μm) and 10 (12.0 ?m). The three methods are (1) the split-window covariance-variance ratio method using a spatial moving window (method 1); (2) the split-window covariance-variance ratio method using a temporal moving window (method 2); and (3) the varying surface temperature method using split-window channel data (method 3). The derived WVC using these three methods was compared to two WVC data sets from European Centre for Medium-Range Weather Forecasts (ECMWF) reanalysis data and the MODIS WVC product. Compared with these two data sets, the derived WVC using method 1 performed proved optimal. The valid pixels using methods 1 and 2 are greater than those using method 3. Furthermore, method 2 can be used to retrieve WVC over pixels where method 1 is invalid.