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采用微波等离子体原子发射光谱法(MP-AES)测定皮革和纺织品中9种可萃取重金属的含量。样品经过人工酸性汗液萃取,MP-AES测定其As、Cd、Co、Cr、Cu、Hg、Ni、Pb、Sb的可萃取含量。结果表明:方法检出限在0.004~0.330mg/kg之间,加标回收率在89%~108%之间,相对标准偏差小于1.5%。该方法操作简便,可实现多种元素同时测定,检出限低、线性范围宽并具有良好的准确度和精密度,与ICP-OES法具有极佳的吻合性,适用于皮革和纺织品中可萃取重金属含量的检测。 相似文献
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Tang Hongbo Lin Haibo Li Yanping Dong Siqing 《International Journal of Food Science & Technology》2015,50(4):1009-1018
Pea starch (PS) appears to be very attractive for the peculiar physicochemical characteristics, which is used for the vermicelli, film‐forming material due to the high amylose content. The aim of this study was to optimise the hydroxypropylation technology parameters of the microcrystalline pea starch based on pea starch as a raw material, hydrochloric acid as an hydrolysis reagent, epoxy propane as an etherisation reagent by the Box–Behnken method. The thermal properties of hydroxypropylated microcrystalline pea starch were characterised by the thermogravimetric analyser and differential scanning calorimeter, respectively. Through the analysis of Design‐Expert software, the regression model and corresponding variances were obtained. In this case, the determination coefficient (R2) was 0.9631. This implied that 96.31% of the variation could be explained by the regression model. The best reaction conditions for preparing the hydroxypropylated microcrystalline pea starch were as follows: reaction temperature 40 °C, reaction time 16 h, amount of epoxy propane 14%, amount of sodium hydroxide 1.2% and amount of anhydrous sodium sulphate 12%. After the microcrystalline pea starch was hydroxypropylated, its peak temperature, melting enthalpy, temperature range of the endothermic peak increased, but its the thermal stability, onset temperature decreased. 相似文献
997.
Ying‐Pei Shen Jhen‐Jhan Wong Chi‐Ching Yang Ta‐Chen Lin 《International Journal of Food Science & Technology》2012,47(8):1720-1727
Roasted sweet potato is a popular food because of the attractive aroma produced by the Maillard reaction. However, the roasting process may lead to charred skin. Cooking with superheated (saturated) steam provides a solution to this problem. As the results show, when comparing sweet potatoes cooked by superheated steam, and those roasted for 40 min, respectively, the degree of gelatinisation could reach as high as 95% with only 140 °C superheated steam, while roasting required temperatures up to 240 °C. Moreover, in appearance, the skins of the sweet potatoes cooked using superheated steam were not charred like the roasted ones. However, sweet potatoes roasted at 240 °C for 60 min had the highest overall sensory score. When comparing the antioxidant activity, the sweet potatoes cooked by superheated steam had the highest content of total phenol and flavonoids, the best scavenging ability of 1,1‐diphenyl‐2‐picrylhydrazyl (DPPH) and the highest ferric‐reducing ability of plasma (FRAP). 相似文献
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Lijun You Lin Zheng Joe M. Regenstein Mouming Zhao Dong Liu 《International Journal of Food Science & Technology》2012,47(12):2574-2581
The effects of thermal treatment on the changes in the colour, the molecular weight distribution, amino acid profiles and the overall antioxidant activities of loach peptide were investigated. When the thermal temperature was rising, the browning was enhanced. The contents of free amino acids Gly, Arg, Thr and Tyr were increased, whereas those of Asp, Ser, Met, Cys, Trp and Lys were decreased. The scavenging activities (1,1‐diphenyl‐2‐picrylhydrazyl (DPPH) radical scavenging activity, the oxygen radical absorbance capacity (ORAC) and the reducing power of loach peptides after different thermal treatments were lower than those of the control, whereas the Cu2+ chelating activity was higher (except from the sample treated at 100 °C, 20 min). The heat treatment at 121 °C, 15 min was shown to be the best thermal processing, as it caused the least loss in radical scavenging activity and showed relatively higher Cu2+ chelating activity. 相似文献
999.
通过对广绣产品营销现状的了解,进行SWOT分析及市场定位,提出将广绣归为奢侈品消费的基本概念,结合广绣产品的特色总结出适宜珠三角地区的广绣产品营销策略. 相似文献
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