Synthesis of Single-Crystalline Silicon Nitride Nanobelts Via Catalyst-Assisted Pyrolysis of a Polysilazane

Recently, one-dimensional nanostructures have attracted extensive attention since they are potentially important for both applications and fundamental research. In this paper, we report the synthesis of ultra-long single crystal Si₃N₄ nanobelts via catalyst-assisted pyrolysis of polymeric precursors. The obtained products contain both α- and β-Si₃N₄ nanobelts, which are 50–100 nm in thickness, 400–1000 nm in width, and a few hundreds of micrometers to several millimeters in length. Different from previous techniques for synthesizing one-dimensional structures, the current nanobelts are synthesized through confined crystallization of an amorphous phase. A solid–liquid–gas–solid reaction/crystallization growth mechanism is proposed. The formation of nanobelts instead of nanowires is attributed to the anisotropy growth at an earlier stage.     

数字多用表的比例功能在电阻箱检测中的应用

本文提出了检测电阻箱的一种新方法--比例法.文章除介绍其原理和方法外,还对装置的不确定度进行了分析,并对比例法检测数据和数表法直接测量的检定结果进行比对.比例法检测电阻箱的特点是对标准器和辅助设备的要求低、工作效率高并可实现半自动检定.拥有数字多用表和标准电阻的检测部门可利用本方法.     

Fabrication of thick BOX SOI by Smart-cut technology

A SOI material with thick BOX (2.2 μm) was successfully fabricated using the Smart-cut technology. The thick BOX SOI microstructures were investigated by high resolution cross-sectional transmission electron mi-croscopy (XTEM), while the electrical properties were studied by the spreading resistance profile (SRP). Experimen-tal results demonstrate that both structural and electrical properties of the SOI structure are very good.     

Investigation of elastic modulus of nanoporous alumina membrane

Nanoporous alumina membranes containing parallel regular pores of uniform size and normal to substrate surface were fabricated by anodically oxidizing high purity aluminum foils in acid solutions and their elastic modulus was investigated. The continuous out-of-plane displacement and current load of the porous membranes were obtained through bulge test combining real-time ESPI (electronic speckle pattern interferometry) observation system. Then the elastic modulus was calculated through an analytical model and the pore distortion after load was characterized by HRSEM (high resolution scan electron microscope). Measurement of mechanical properties indicates unusual mechanical behavior of these anodic alumina films compared with bulk alumina materials. This observation may help shed light on fracture mechanism of these films with nanopore arrays and bring further understanding on connecting of micro-meso structure and mechanical properties.     

水产品加工废水深度处理的试验

进行了用"生物接触氧化-微滤膜"组合工艺对水产品加工废水深度处理的试验研究.试验结果表明:在进水COD约900~1 200 ms/L,水力停留时间>16 h的情况下,平均出水COD<50 ms/t,达到再生水杂用水质标准.同时,研究探讨了处理过程中膜组件的污染及清洗问题,为实际工程中膜的运行提供了必要的参考.     

k分Cantor集的Hausdorff测度的一种计算

以比较初等的方法重新证明了著名的Ｃａｎｔｏｒ三分集的Ｈａｓｄｏｒｒｆｆ维数为ｓ＝ｌｏｇ２／ｌｏｇ３，Ｈａｕｓｄｏｒｆｆｃ测度为１，并对直线上类似的一类构造集推广了此方法。     

系数传递法在某边坡稳定性计算中的应用

滑坡是现阶段工程建设过程中经常遇到的地质灾害现象,预见边坡的稳定性变得尤为重要,本文采用系数传递法对谷坡的工程稳定性进行了计算分析,从而达到预见边坡稳定性的目的.     

Rapid growth of angle-confined large-domain graphene bicrystals

In the chemical vapor deposition growth of large-area graphene polycrystalline thin films,the coalescence of randomly oriented graphene domains results in a high density of uncertain grain boundaries (GBs).The structures and properties of various GBs are highly dependent on the misorientation angles between the graphene domains,which can significantly affect the performance of the graphene films and impede their industrial applications.Graphene bicrystals with a specific type of GB can be synthesized via the controllable growth of graphene domains with a predefined lattice orientation.Although the bicrystal has been widely investigated for traditional bulk materials,no successful synthesis strategy has been presented for growing two-dimensional graphene bicrystals.In this study, we demonstrate a simple approach for growing well-aligned large-domain graphene bicrystals with a confined tilt angle of 30° on a facilely recrystallized single-crystal Cu (100) substrate.Control of the density of the GBs with a misorientation angle of 30° was realized via the controllable rapid growth of subcentimeter graphene domains with the assistance of a cooperative catalytic surface-passivation treatment.The large-area production of graphene bicrystals consisting of the sole specific GBs with a tunable density provides a new material platform for fundamental studies and practical applications.     

有限单元法在地下工程围护结构传热中的应用

分析总结现有地下工程围护结构传热研究不足的基础上,对实际贴壁式和离壁式衬砌地下工程围护结构进行合理的物理数学简化,建立了热传递过程的数学模型.该数学模型中详细考察了不同的边界条件.有限单元法对复杂区域具有良好的适应性,论述了有限单元法在地下工程维护结构传热中的应用.     

基于综合性能最优的小波域图像融合新方法

以提高融合图像的综合性能为目标,提出了一种基于综合性能最优的小波域图像融合方法。首先根据融合目的和专家经验,选择融合图像的多个客观评价标准,并由之构建综合性能指标。然后,对待融合图像分别进行多尺度小波分解,引入遗传算法创建初始种群作为小波域的图像融合参数,求解融合图像及其综合性能值;利用综合性能评价指标最优作为遗传算法的适应度函数,经过选择、交叉、变异等种群进化操作,快速逼近并定位最优性能参数,最后得到综合性能最优的融合图像,即该参数对应的融合图像。实验结果显示,所提融合方法的综合融合效果优于常见的小波变换、金字塔分解等多种融合方法。