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41.
Jens Laube Valentin Baric Samir Salameh Lutz Mädler Lucio Colombi Ciacchi 《Granular Matter》2018,20(2):28
We develop a novel coarse-grained contact model for Discrete Element Method simulations of \(\hbox {TiO}_2\) nanoparticle films subjected to mechanical stress. All model elements and parameters are derived in a self-consistent and physically sound way from all-atom Molecular Dynamics simulations of interacting particles and surfaces. In particular, the nature of atomic-scale friction and dissipation effects is taken into account by explicit modelling of the surface features and water adsorbate layers that strongly mediate the particle-particle interactions. The quantitative accuracy of the coarse-grained model is validated against all-atom simulations of \(\hbox {TiO}_2\) nanoparticle agglomerates under tensile stress. Moreover, its predictive power is demonstrated with calculations of force-displacement curves of entire nanoparticle films probed with force spectroscopy. The simulation results are compared with Atomic Force Microscopy and Transmission Electron Microscopy experiments. 相似文献
42.
Electrochemical Behavior of Single CuO Nanoparticles: Implications for the Assessment of their Environmental Fate
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Giorgia Zampardi Jorg Thöming Hendrik Naatz Hatem M. A. Amin Suman Pokhrel Lutz Mädler Richard G. Compton 《Small (Weinheim an der Bergstrasse, Germany)》2018,14(32)
The electrochemical behavior of copper oxide nanoparticles is investigated at both the single particle and at the ensemble level in neutral aqueous solutions through the electrode‐particle collision method and cyclic voltammetry, respectively. The influence of Cl? and NO3? anions on the electrochemical processes occurring at the nanoparticles is further evaluated. The electroactivity of CuO nanoparticles is found to differ between the two types of experiments. At the single‐particle scale, the reduction of the CuO nanoparticles proceeds to a higher extent in the presence of chloride ion than of nitrate ion containing solutions. However, at the multiparticle scale the CuO reduction proceeds to the same extent regardless of the type of anions present in solution. The implications for assessing realistically the environmental fate and therefore the toxicity of metal‐based nanoparticles in general, and copper‐based nanoparticles in particular, are discussed. 相似文献
43.
固体有害废物安全填埋场基础弱渗透岩石的渗透性,大多数情况下都由实验室和野外方法测定.测定方法的适用性取决于岩石种类、岩体状态和渗透性数量级别.在同一实验段内采用不同的实验方法,一情况下导致产生两个数量级的误差,而更大的不可靠性与使用不同的评价方法有关.因为可靠并可引用的渗透性测定值在废物安全填埋场建设中对地质屏障的评价具有重大意义,如果各地能同时列出科研规划,共同研究对所有可能存在的地质屏障岩石进行全面分析评价,确定不同实验方法之间相关关系,以及使评价方法尽可能统一,是十分必要的 相似文献
44.
Domino Reactions in Organic Synthesis 总被引:1,自引:0,他引:1
Tietze LF 《Chemical reviews》1996,96(1):115-136
45.
Medium-sized, open-participation Open Source Software (OSS) projects do not usually perform explicit software process improvement
on any routine basis. It would be useful to understand how to get such a project to accept a process improvement proposal
and hence to perform process innovation. We want to determine an effective and feasible qualitative research method for studying
the above question. We present (narratively) a case study of how we worked towards and eventually found such a research method.
The case involves four attempts at collecting suitable data about innovation episodes (direct participation (twice), polling
developers for episodes, manually finding episodes in mailing list archives) and the adaptation of the Grounded Theory data
analysis methodology. Direct participation allows gathering rather rich data, but does not allow for observing a sufficiently
large number of innovation episodes. Polling developers for episodes did not prove to be useful. Using mailing list archives
to find data to be analyzed is both feasible and effective. We also describe how the data thus found can be analyzed based
on the Grounded Theory Method with suitable adjustments. By-and-large, our findings ought to apply to studying various phenomena
in OSS development processes that are similarly heavyweight and infrequent. However, specific details may block this possibility
and we cannot predict which details that might be. The amount of effort involved in direct participation approaches to qualitative
research can easily be underestimated. Also, survey approaches are not well-suited for many process issues in OSS, because
too few developers are sufficiently process-conscious. An approach based on passive observation is a viable alternative in
the OSS context due to the availability of large amounts of fairly complete archival data. 相似文献
46.
Anne Martens Heiko Koziolek Lutz Prechelt Ralf Reussner 《Empirical Software Engineering》2011,16(5):587-622
Model-based performance evaluation methods for software architectures can help architects to assess design alternatives and save costs for late life-cycle performance fixes. A recent trend is component-based performance modelling, which aims at creating reusable performance models; a number of such methods have been proposed during the last decade. Their accuracy and the needed effort for modelling are heavily influenced by human factors, which are so far hardly understood empirically. Do component-based methods allow to make performance predictions with a comparable accuracy while saving effort in a reuse scenario? We examined three monolithic methods (SPE, umlPSI, Capacity Planning (CP)) and one component-based performance evaluation method (PCM) with regard to their accuracy and effort from the viewpoint of method users. We conducted a series of three experiments (with different levels of control) involving 47 computer science students. In the first experiment, we compared the applicability of the monolithic methods in order to choose one of them for comparison. In the second experiment, we compared the accuracy and effort of this monolithic and the component-based method for the model creation case. In the third, we studied the effort reduction from reusing component-based models. Data were collected based on the resulting artefacts, questionnaires and screen recording. They were analysed using hypothesis testing, linear models, and analysis of variance. For the monolithic methods, we found that using SPE and CP resulted in accurate predictions, while umlPSI produced over-estimates. Comparing the component-based method PCM with SPE, we found that creating reusable models using PCM takes more (but not drastically more) time than using SPE and that participants can create accurate models with both techniques. Finally, we found that reusing PCM models can save time, because effort to reuse can be explained by a model that is independent of the inner complexity of a component. The tasks performed in our experiments reflect only a subset of the actual activities when applying model-based performance evaluation methods in a software development process. Our results indicate that sufficient prediction accuracy can be achieved with both monolithic and component-based methods, and that the higher effort for component-based performance modelling will indeed pay off when the component models incorporate and hide a sufficient amount of complexity. 相似文献
47.
The construction of a new generation of MEMS which includes micro-assembly steps in the current microfabrication process is a big challenge. It is necessary to develop new production means named micromanufacturing systems in order to perform these new assembly steps. The classical approach called “top-down” which consists in a functional analysis and a definition of the tasks sequences is insufficient for micromanufacturing systems. Indeed, the technical and physical constraints of the microworld (e.g. the adhesion phenomenon) must be taken into account in order to design reliable micromanufacturing systems. A new method of designing micromanufacturing systems is presented in this paper. Our approach combines the general “top-down” approach with a “bottom-up” approach which takes into account technical constraints. The method enables to build a modular architecture for micromanufacturing systems. In order to obtain this modular architecture, we have devised an original identification technique of modules and an association technique of modules. This work has been used to design the controller of an experimental robotic micro-assembly station. 相似文献
48.
For a number of programming languages, among them Eiffel, C, Java, and Ruby, Hoare-style logics and dynamic logics have been developed. In these logics, pre- and postconditions are typically formulated using potentially effectful programs. In order to ensure that these pre- and postconditions behave like logical formulae (that is, enjoy some kind of referential transparency), a notion of purity is needed. Here, we introduce a generic framework for reasoning about purity and effects. Effects are modelled abstractly and axiomatically, using Moggi’s idea of encapsulation of effects as monads. We introduce a dynamic logic (from which, as usual, a Hoare logic can be derived) whose logical formulae are pure programs in a strong sense. We formulate a set of proof rules for this logic, and prove it to be complete with respect to a categorical semantics. Using dynamic logic, we then develop a relaxed notion of purity which allows for observationally neutral effects such writing on newly allocated memory. 相似文献
49.
Standard path control laws of autonomous vehicles use the shortest distance between the vehicle’s position and the path as a control error. In order to determine this distance, the projection point onto the path needs to be determined continuously. This requires fast algorithms that feature high numerical reliability in the field of vehicle application.This paper presents two different observer-based approaches for the projection problem. The identity observer reconstructs all states of interest for path control. The second one, a reduced observer, only possesses the curve parameter as a state and calculates the other values by algebraic formulas. Both algorithms consider the continuous movement of the vehicle, the run of the curve, and work without any approximation of the curve. Furthermore, they are applicable for arbitrary parameterized smooth curves, guarantee the required numerical stability, have short calculating time, and show good statistical properties. The performance is shown in several simulations as well as under real conditions. 相似文献
50.
Minimum size of a graph or digraph of given radius 总被引:1,自引:0,他引:1
In this paper we show that a connected graph of order n, radius r and minimum degree δ has at least edges, for n large enough, and this bound is sharp. We also present a similar result for digraphs. 相似文献