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951.
952.
Weiping Ma Paul W. Brown Sridhar Komarneni 《Journal of the American Ceramic Society》1996,79(6):1707-1710
Tobermorites were synthesized from oxides and from fly ashes under mild hydrothermal conditions. The bulk compositions of the ash-based formulations were adjusted to give the same [Ca]/[Si + Al] ratio as for the oxides. Selective Cs and Sr exchange with these tobermorites was measured. Compared to those prepared from the oxides and from class C fly ash, the tobermorites obtained from class F fly ash exhibited superior Cs and Sr selective properties. This is apparently a result of more extensive Al incorporation with class F fly ash. For example, tobermorite synthesized from class F fly ash exhibited a cesium K d (mL/g) of 3826 while those prepared from oxides and from class C fly ash showed K d values of 1112 and 796, respectively, under the same conditions. These results suggest that fly ash waste materials can be converted into tobermorite, which can serve as a resource in the separation, immobilization, and disposal of radioactive species such as Cs and Sr. 相似文献
953.
ABSTRACTTo prepare H2-permeable palladium composite membranes, a novel carbon-doped microporous TiO2 intermediate layer was introduced to modify the surface of macroporous Al2O3 substrates. The Pd/TiO2–C/Al2O3 membrane was prepared via electroless plating, and thereafter, carbon residue in the intermediate layer was removed by calcination in air, yielding a Pd/TiO2/Al2O3 membrane. Experimental results indicate that the carbon residue shrinks the pore size of the intermediate layer and facilitates a decrease of membrane defects. Additionally, carbon removal induces a higher effective membrane area at the permeate side, which enhances hydrogen permeability. Furthermore, the apparent activation energy (EA) and stability of the as-prepared Pd/TiO2/Al2O3 membrane were investigated. 相似文献
954.
企业的信息安全威胁及应对措施 总被引:2,自引:0,他引:2
目前信息安全已成为企业的一个主要风险,在信息安全受到越来越多的威胁时,完整的企业信息安全解决方案应该分为几个层次,并且与安全管理相结合,建立一个动态的信息安全防范系统。 相似文献
955.
介绍了微机监控系统在辽化芳烃空压站的应用,系统采用集散式控制系统,以方正微机为上位管理机,以西门子公司的S7—300型PLC为下位控制机,实现自动化控制和管理。 相似文献
956.
957.
在核磁共振检查前需要进行无磁化确认,针对核磁共振检查所处的环境背景磁场复杂、干扰较多,系统出现误报警高、探测失效等问题,设计了基于磁通门传感器的铁磁探测系统。系统使用二次谐波法测量磁场信号,设计模拟电路进行信号相敏检测。通过积分反馈提高闭环系统的线性度和抗干扰性,探头工作在稳定的状态。采用卡尔曼滤波对背景磁场和磁异信号进行处理,提高信号信噪比,同时设计能量检测器对磁异信号进行检测。试验测试结果表明,系统在核磁共振室外复杂磁场环境可以减少设备工作时的误报警,有效探测出铁磁性物质。 相似文献
958.
脂肪族形状记忆聚氨酯的合成及表征 总被引:2,自引:0,他引:2
以脂肪族异氰酸酯HDI为硬段原料合成了脂肪族的形状记忆聚氨酯,通过调节硬段含量研究了硬段结构对形状记忆性能的影响.DSC、DMA等分析结果表明,硬段含量的增加使软段结晶的不完善程度增大,并使硬段的结晶趋于完善,而软段结晶的完善程度决定了维持暂时形状的能力,所以形变固定率随着硬段增加而下降.同时IR结果证明,HDI形成的硬段间的氢键作用更强,从而得到了比芳香族形状记忆聚氨酯更高的形变回复率. 相似文献
959.
Sit-Foon?Cheng Yuen-May?ChooEmail author Ah-Ngan?Ma Cheng-Hock?Chuah 《Journal of the American Oil Chemists' Society》2005,82(11):791-795
Rapid synthesis of high-purity MAG from refined, bleached, and deodorized palm stearin (RBDPS) via chemical glycerolysis in the presence of pyridine was developed to obviate the conventional molecular distillation in the
production of pure MAG. The optimal reaction for the sodium methoxide-catalyzed glycerolyis of RBDPS was recorded at 110°C
using a 3 wt% catalyst concentration based on the weight of RBDPS, with an RBDPS/glycerol ratio of 1∶2 and an RBDPS/pyridine
ratio of 1∶4. High yields of over 99% were achieved rapidly in 15 min, and increases in DAG and FFA were observed after a
prolonged reaction time. 相似文献
960.
Ti‐based Ziegler–Natta catalysts supported on MgCl2 doped with AlCl3 were prepared by the reaction of MgCl2/AlCl3–ethanol adduct with TiCl4. No AlCl3 crystallites were found in the AlCl3‐doped catalysts by WAXD analysis, suggesting that AlCl3/MgCl2 solid solution was formed. The effect of doping on the catalyst performance in ethylene polymerization was investigated. The results showed that the catalysts based on AlCl3‐doped MgCl2 support exhibited a slightly higher activity than did the MgCl2‐supported catalyst and the molecular weight distribution (MWD) of polyethylene (PE) markedly increased (from 10.8 to 47.9) with the increase of AlCl3 content in catalysts. The changes in catalyst's active center distribution were studied based on nonlinear fitting of the polymer GPC curves by multiple Flory functions. It was found that increase of types of active centers by introducing AlCl3 into the support should be responsible for the broadening of MWD of PE. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 1768–1772, 2006 相似文献