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21.
Preparation and Use of a Boron Nitride Precursor as Binder for the Densification of Boron Nitride 总被引:1,自引:0,他引:1
A precursor of boron nitride was prepared through the partial condensation of 2,4,6-trichloroborazine and bis-(trimethylsilyl)acetylene. This reaction was conducted at 100°C and is catalyzed by AlCl3 . The condensation product pyrolyzed at 800°C, producing trimethylsilyl chloride as a volatile product and a boron nitride rich residue containing 54 wt% of the initial weight. Mixtures of the precursor and commercial boron nitride were made and hot-pressed at 800°C and 27.6 MPa. A maximum density of 1.84 g/cm3 is reached at a loading corresponding to the deposition of 13 wt% residue derived from the precursor. Examination by analytical electron microscopy, including X-ray energy dispersive spectroscopy and electron energy loss spectroscopy analyses, revealed the location of material derived from the precursor in BN-binder composites through the presence of residual aluminum, silicon, and carbon. Crystallization of boron nitride from the precursor appears to have taken place, as deduced from the morphology of the phases observed and association with residual elements present in the binder. 相似文献
22.
Forty-five harvests corresponding to the two predominating domestic species of amaranth in Mexico were studied. The proximate analysis revealed some statistically significant differences throughout three years of observation. The Ca, P and Fe content did not vary greatly in 15 samples. No chemical differences were either manifested in the Mercado and Aztec types of A. hypochondriacus, nor in the Mexican type of A. cruentus. The latter exhibits a higher grain yield and a shorter life cycle; however, its baking quality is apparently inferior to that of the Mercado type of A. hypochondriacus. The heat treatment of the seeds (toasting, popping and cooking) affected protein and lysine contents as does in cereals and leguminous seeds although toasting in particular improves its sensory characteristics without altering digestibility and PER. Popping only improves PER. Heating at 90 or 170 degrees C for three to five minutes, at the usual seed's moisture rate of 6 to 15%, does not affect protein content and does so only slightly in the case of the fatty acids content. Amylographic and farinographic values of the starchy fractions indicate similarities to C. quinoa and differences with respect to wheat. In the case of "amaranth milk", viscosity and gelatinization temperature produced satisfactory values. The extension of amaranth cultivation in the country is hereby suggested in view of the seed's nutritional quality, and considering the behavior of whole amaranth flour and its fractions. 相似文献
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The promise of biomolecular computers is their ability to interact with naturally occurring biomolecules, enabling in the future the development of context-dependent programmable drugs. Here we show a context-sensing mechanism of a biomolecular automaton that can simultaneously sense different types of molecules, allowing future integration of biomedical knowledge on a broad range of molecular disease symptoms in the decision of a biomolecular computer to release a drug molecule. 相似文献
25.
Stevenson KA Muralidharan G Maya L Wells JC Barhen J Thundat T 《Journal of nanoscience and nanotechnology》2002,2(3-4):397-404
Functionalized gold nanoparticles have been covalently bound to internal, modified sites on double-stranded DNA. Gold nanoparticles coated with mercaptosuccinic acid or thioctic acid were bound to amino-modified thymine bases on double-stranded DNA. Visible absorption spectra, gel electrophoresis, and atomic force microscopy were used to analyze the products. Thiol groups were added to one end of the gold/nanoparticle product, which was then attached to a gold surface. This method has the potential to allow controlled placement of particles with subnanometer precision and to allow attachment of the product to fixed contacts for nanodevice fabrication. 相似文献
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Iwao Matsuya Ryota Tomishi Maya Sato Kiyoshi Kanekawa Yoshihiro Nitta Motoichi Takahashi Satoru Miura Yasutsugu Suzuki Tomohiko Hatada Ryuta Katamura Takashi Tanii Shuichi Shoji Akira Nishitani Iwao Ohdomari 《IEEJ Transactions on Electrical and Electronic Engineering》2011,6(3):266-272
We have developed a novel sensor that enables us to measure the relative story displacement of a building structure in real time. This lateral displacement sensor (LDS) is composed of a light‐emitting diode (LED) array, which is fixed on the ceiling, and a position‐sensitive detector (PSD) unit, which is placed on the floor. We optimized the LDS to achieve high accuracy in lateral displacement measurement. The accuracy was evaluated to be 60 µm by conducting shaking table tests. Two LDSs were implemented in an actual building equipped with an active variable stiffness (AVS) system, and the building was vibrated with seismic waveforms by an exciter placed on the rooftop. The seismic displacement of the second floor relative to the first floor was measured using the LDS. Furthermore, the inclination angle of the second floor could be measured using the LDS during the seismic vibration. Using the AVS system, we realized the residual displacement of the second floor without inducing damage to the building, and succeeded in real‐time residual displacement measurement for the first time. These results indicate that the LDS is useful for the health diagnosis of a building structure. © 2011 Institute of Electrical Engineers of Japan. Published by John Wiley & Sons, Inc. 相似文献
28.
Fault estimation and tolerant control for discrete‐time switched systems with sojourn probabilities 下载免费PDF全文
Rathinasamy Sakthivel Maya Joby Srimanta Santra Yong Ren 《International Journal of Adaptive Control and Signal Processing》2017,31(12):1808-1824
This paper addresses the issue of fault estimation and accommodation for a discrete‐time switched system with actuator faults. Here, we assume that the sojourn probabilities are known a priori. By using the reduced‐order observer method, the sojourn probability approach, and the Lyapunov technique, a fault estimation algorithm is obtained for the considered system. The main objective of this work is to design a dynamic output feedback fault‐tolerant controller based on the obtained fault estimation information such that the closed‐loop discrete‐time switched system with available sojourn probabilities is robustly mean‐square stable and satisfies a prescribed mixed and passivity disturbance attenuation level in the presence of actuator faults. More precisely, a dynamic output feedback fault‐tolerant controller is established in terms of linear matrix inequalities. Finally, numerical examples are provided to illustrate the usefulness and effectiveness of the proposed design technique. 相似文献
29.
Maya B. Gokhale Janice M. Stone Edson Gomersall 《The Journal of VLSI Signal Processing》2000,24(2-3):165-180
Hybrid architectures combining conventional processors with configurable logic resources enable efficient coordination of control with datapath computation. With integration of the two components on a single device, housekeeping tasks and, optionally, loop control and data-dependent branching, can be handled by the conventional processor, while regular datapath computation occurs on the configurable hardware. This paper describes a novel approach to programming such hybrid devices that gives the programmer control over mapping of data and computation between conventional processor and configurable logic. With a simple set of pragma and intrinsic function directives, the NAPA C language provides for manual control over perhaps the most important aspect of programming such hybrid devices. Alternatively, as experience is gained about tradeoffs between the two computational resources, mapping directives may eventually be generated by an external tool. The paper further describes a research prototype compiler that targets the hybrid processor model, with a concrete implementation for the National Semiconductor NAPA1000 chip. The NAPA C compiler parses the mapping directives, performs semantic analysis, and co-synthesizes a conventional processor executable combined with a configuration bit stream for the configurable logic. Two major compiler phases, the synthesis of pipelined loops and the datapath synthesis, are described in detail. 相似文献
30.
Marcelle Nardelli Baptista Ricardo Valcarcel Vandré Maya Fernando Canto 《Water Resources Management》2014,28(13):4781-4793
The primary goal of this study is to identify floodplains that are in large river basins and could potentially undergo renaturalization of their hydrologic functions. The study area is the Paraíba do Sul River Basin (55,400 km2), which is located in southeastern Brazil. The field work included the application of geoprocessing techniques (ArcGIS 10 and ENVI 4.7) for the delineation and individualization of the floodplain, and the following characteristics were surveyed: area, perimeter, circularity index and urbanization index. Discriminant and cluster analyses (SPSS 15) were performed, and 77 floodplains were found that exhibited a wide variation in area (0.13 to 1,540 km2) and perimeter (1.8 to 4,200 km), low circularity indices (<0.52), and a low average urbanization index (18.9 %). The floodplains were grouped according to how well the renaturalization of their hydrologic functions could be managed and categorized as follows: a) low management potential (9 units); b) medium management potential (15 units); and c) high management potential (52 units). The discriminant analysis correctly classified 100 % of the cases, which indicates that the model has a high predictive ability and can accurately classify the management potential of floodplains. 相似文献