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51.
Surface mechanical and tribological properties of a copolymer based on benzoyl-1,4-phenylene and 1,3-phenylene were evaluated using nanoprobe investigation techniques and compared to the properties obtained at the macroscale. These copolymers are commonly referred to as self-reinforced polymers (SRPs) because of their intrinsic high strength and modulus without addition of a reinforcing agent. Specimens were prepared by spin casting, solvent casting, and compression molding. Surface mechanical properties and film thickness were measured by nanoindentation and scratching techniques. Friction properties were found using lateral force microscopy (LFM), and surface topography was imaged by tapping mode atomic force microscopy (AFM). Macroscale friction testing revealed a kinetic coefficient of friction of 0.08 for SRP, approaching that of Teflon. Similarly low relative friction coefficients were obtained in nanoprobe measurements. Nanoindentation of SRP, polycarbonate (PC), and polyetherimide (PEI) demonstrated superior surface hardness and modulus of SRP copolymer thin films. 相似文献
52.
(4‐Ethylphenyl)‐3,5‐ditertiarybutyl‐4‐hydroxybenzylamine, 1‐phenyl‐4‐(3,5‐ditertiarybutyl‐4‐hydroxybenzyl)piperazine, and 1‐(3,5‐ditertiarybutyl‐4‐hydroxybenzyl)piperidine were synthesized and characterized, and their performance in polypropylene copolymer (PPCP) was tested by multiple extrusions in a Brabender plasticorder. The thermooxidative stability of PPCP was assessed by the measurement of oxidative induction time at 200 ± 1°C, and the thermal stability was assessed by observation of the change in the melt flow rate. A comparative study of the synthesized antioxidants with the commercially available antioxidant 2,6‐ditertiarybutyl‐4‐methylphenol was made. The presence of phenolic and amino groups influenced the performance of the antioxidants. The performance of the antioxidants influenced the thermal stability of the PPCP. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 91: 1097–1103, 2004 相似文献
53.
54.
Joseph Sam Armijo Piyush Kar Manoranjan Misra 《Nuclear Engineering and Design》2006,236(24):2589-2598
The reference waste package design and operating mode to be used in the Yucca Mountain Repository is reviewed. An alternate (second generation) operating concept and waste package design is proposed to reduce the risk of localized corrosion of waste packages and to reduce repository costs. The second generation waste package design and storage concept is proposed for implementation after the initial licensing and operation of the reference repository design. Implementation of the second generation concept at Yucca Mountain would follow regulatory processes analogous to those used successfully to extend the design life and uprate the power of commercial light water nuclear reactors in the United States. The second generation concept utilizes the benefits of hot dry storage to minimize the potential for localized corrosion of the waste package by liquid electrolytes. The second generation concept permits major reductions in repository costs by increasing the number of fuel assemblies stored in each waste package, by eliminating the need for titanium drip shields and by fabricating the outer container from corrosion resistant low alloy carbon steel. 相似文献
55.
Jignasu P. Mehta Prashant N. Bhatt Sudhindra N. Misra 《中国稀土学报(英文版)》2006,24(6):648-652
Pr( Ⅲ ) and Nd( Ⅲ ) can be utilized as absorption spectroscopic probes to investigate the interaction of biomolecules like Lysozyme (HEW) with Ca( Ⅱ ) in-vitro ; the most abundant metal ion in the human body system. The spectroscopic techniques involving comparative absorption, absorption difference, and quantitative intensity analysis using 4f-4f transitions are utilized for changes in the inner sphere coordination pattern of Pr( Ⅲ ) and Nd(Ⅲ ) in solution as well as in solid state. The present study deals with an important biomolecule in human metabolism, that is, Lysozyme (HEW). The absorption er-Condon the probab spectral parameters such as the oscillator strength (P), the Judd-Ofelt (Tλ) intensity parameters, and the Slatinter electronic parameters are calculated using chi square methods. The obtained results are used to determine le geometry of the complex in the solution, the nature of the bond between Pr(Ⅲ)/Nd(Ⅲ) with lysozyme, and the inner sphere coordination environment of f-f transitions. The results obtained from various experimental conditions are utilized to investigate the coordination changes in the Pr(Ⅲ)/Nd(Ⅲ) complexes caused by different coordinating sites of lysozyme, normalized bite, denticity, the solvent nature, the coordination number, the nature of bond and other parameters to mimic the interaction of the Ca( Ⅱ ) ion with such biomolecule. 相似文献
56.
For large well-connected reliability networks, it has been observed that the delta and star transformations are sometimes unable to tackle the complexity of the network. The quadrilateral-star transformation may be helpful in initiating network reduction under these circumstances. Probability conditions for approximate equivalence of quadrilateral and star networks have been derived. Using these conditions, six different sets of transformation equations have been obtained and compared from the point of view of accuracy. 相似文献
57.
The Landsat multispectral scanner data have been analyzed with a view toward crop identification and inventory. The notion of spectral-temporal trajectory as crop signature, introduced in an earlier paper, has been further developed leading to a formulation of the problem similar to one of recognition of hand-written characters. A simple classification rule based on angular features of the trajectory is discussed and classification results are given for Landsat images from several sites. 相似文献
58.
Mathematical statistics are used to design electronic systems in which the effects of the initial variations of the system parameters and the drift of these parameters on the system performance criteria are a minimum. This is accomplished by minimizing the initial variances of the system performance criteria with respect to the initial mean values of the system parameters while constraining the means of these parameters to their required values. In addition, the drift rates of the system parameters are selected in such a manner as to prevent the drift of the mean values of the system performance criteria while reducing the tendencies of the variances of these criteria to increase with time. These techniques were successfully applied to a number of electronic systems, including systems with both active and passive elements, thus illustrating the usefulness of mathematical statistics in the design of mass produced electronic systems. 相似文献
59.
In this paper, we propose two information-theoretic techniques for efficiently trading off the location update and paging costs associated with mobility management in wireless cellular networks. Previous approaches always attempt to accurately convey a mobile's movement sequence and hence cannot reduce the signaling cost below the entropy bound. Our proposed techniques, however, exploit the rate distortion theory to arbitrarily reduce the update cost at the expense of an increase in the corresponding paging overhead. To this end, we describe two location tracking algorithms based on spatial quantization and temporal quantization, which first quantize the movement sequence into a smaller set of codewords and then report a compressed representation of the codeword sequence. Although the spatial quantization algorithm clusters individual cells into registration areas, the more powerful temporal quantization algorithm groups sets of consecutive movement patterns. The quantizers themselves are adaptive and periodically reconfigure to accommodate changes in the mobile's movement pattern. Simulation study with synthetic and real movement traces for both single-system and multisystem cellular networks demonstrate that the proposed algorithms can reduce the mobile's update frequency to 3-4 updates/day with reasonable paging cost, low computational complexity, storage overhead, and codebook updates. 相似文献
60.
S. K. Sasamal R. C. Panigrahy Sangeeta Misra 《International journal of remote sensing》2013,34(17):3853-3858
Asterionella glacialis Castracane, a diatom species of marine phytoplankton, bloomed in the coastal waters of the northwestern Bay of Bengal during 24 March to 4 April 2004. This species dominated by 99% in cell concentration on 26 March 2004. During the bloom period, phytoplankton population density increased by three orders of magnitude, while the chlorophyll a concentration increased by 70 to 80 times relative to the pre‐bloom situation. The blooming was associated with coastal upwelling and influenced water quality. Corresponding to the blooming period, satellite sensor‐derived products of sea surface temperature (SST) and chlorophyll a data were analysed to understand the coverage and dynamics of phytoplankton in the area. 相似文献