高流速双室床节水效果评价

高流速双室床(HDCB)是我国自主开发的一项水处理新技术。陕西某热电厂1年多的运行结果表明,其自用水率仅为3.2%,远低于反渗透(33%)及其他离子交换技术(10%)。HDCB自用水率低是由其结构及运行特性决定的,它具有周期制水量大,再生步骤少,再生过程用水量少,大反洗(清洗)次数少等特性,是目前化学水处理技术中节水效果最好的一种技术。     

提高品种钢质量推动精益化管理

介绍了湘钢以82B为代表的品种钢质量控制方面的作法与经验,以及以其为切入点,全面推行产品质量的精益化管理模式.     

Rapid and Sensitive Liquid Chromatography-Tandem Mass Spectrometry for Quantification of Glycyrrhetic Acid in Human Plasma

A simple, rapid and sensitive liquid chromatography-tandem mass spectrometry(LC-MS/MS) for the determination of glycyrrhetic acid in human plasma with ginsenoside Rh2 as internal standard was developed and validated. The plasma samples were prepared via liquid-liquid extraction with ethyl acetate. Chromatographic separation was accomplished on a Venusil MP-C18(50 mm×2.1 mm, 5μm i.d.) column at 25℃. The mobile phase consisted of acetonitrile/5 mmol·L-1 ammonium acetate(10:90, volume ratio) at a flow rate of 0.4 mL/min. Negative electrospray ionization was utilized as the ionization source. Glycyrrhetic acid and internal standard were determined via the mutiple reaction monitoring of precursor→production ion transitions at m/z 469→425, 409 and m/z 621→161,respectively. Each sample was chromatographed within 2.5 min. The lower limit of uantification was 0.50 ng/mL for 200 μL of plasma sample and the linear range was from 0.50 ng/mL to 800 ng/mL. The intra-and inter-day precisions were less than 8.76% in terms of relative standard deviation(RSD), and the accuracy was within a range of -3.25%-1.32% in terms of relative error(RE). The method was successfully applied to the pharmacokinetic studies of glycyrrhetic acid in healthy male Chinese volunteers after a single oral administration of 75 mg of glycyrrhizin.     

我国有机食品的现状及发展趋势

介绍了有机食品的特点及对人与自然和谐发展的作用,并概述了我国有机食品的发展现状及趋势.     

锚杆锚索联合支护在大断面巷道中的应用

分析了沈阳煤业集团西马煤矿北二区的地质条件,根据生产实际对北二区回风上山掘进工作面的支护选择锚杆锚索联合支护方式,确保了大断面巷道支护的安全。     

K52合金及其涂层的涂盐热腐蚀行为

研究了合金及其涂层的热腐蚀行为,测定了它们的氧化动力学曲线。用扫描电镜和电子探针观察了合金及涂层腐蚀后的表面形貌和横截面显微组织。结果表明:溅射K52纳米晶涂层在含有NaCl的盐中腐蚀10 h,氧化膜就大面积剥落,涂层遭受很大的破坏。而铸态合金腐蚀50 h后,产生已基本连续的内氧化铝层,这层氧化铝对阻止O、S和Cl的进入起到一定的作用,提高了合金的抗氯盐腐蚀。     

井工采区煤、矸分运系统集中优化布置

为适应高产、高效矿井建设和矿井水平延伸需要,文章介绍了采区煤仓与溜矸仓布置的基本原则与实际,实现设计优化。     

焦作矿区煤层瓦斯合理预抽期的研究

主要介绍了合理预抽期确定模型在焦作矿区的应用。为了减少瓦斯突出的危险性,合理地确定预抽期是瓦斯抽放的关键因素之一。     

中空海胆状结构的碳包覆Fe2O3用作锂离子电池的高性能负极材料

Fe2O3由于成本低廉,储量丰富和理论比容量高(1007 mA hg^-1)等特点,在锂离子电池负极材料的应用中极具发展前景.然而一些问题仍然存在,如:充放电过程中比容量的迅速衰减,不可逆的体积膨胀以及较短的循环寿命等.这些问题严重制约了Fe2O3在锂离子电池中的实际应用.为了突破这些局限,本文以金属-有机骨架(MOF...     

Influences of harmonic cavities on single-bunch instabilities in electron storage rings

Harmonic cavities (HCs) are widely used in electron storage rings, mainly to increase the Touschek lifetime by lengthening bunches. HCs have become critical com...