Crystallization of glass in fireclay refractories; part III: Detailed study on the mullite crystal size in the ‘synthetic’ glass

Poor-grade fireclay products contain substantial amount of glass. A glass of similar composition was synthesized, nucleated and heat-treated for crystallization of mullite. The size and size-distribution of mullite crystals, the rate of change of size and the aspect ratio of the crystals were investigated in relation to the nucleating agents and temperature.     

Transition metal joints for steam generators—An overview

The transition metal joint (TMJ) between an austenitic stainless steel and a chromium-molybdenum (Cr-Mo) ferritic steel used widely in steam generators of power plants has for a long time presented problems relating to premature failures in service. The direct (bimetallic) TMJ presently in use is designed for a service life of about 200,000 h; but such TMJs with iron-base weld metals have been failing in service within about one-third of their design lifetime, while their counterparts with nickel-base weld metals fail within about one-half of their design lifetime. The causes for such premature service failures of these TMJs are discussed in detail, leading to the development of improved TMJs. One of the improved TMJs with a trimetallic configuration of austenitic stainless steel/Alloy 800/Cr-Mo ferritic steel is discussed in detail, covering its development, characterisation and evaluation. Accelerated performance tests in the laboratory have indicated a four-fold improvement in the service life of the TMJ with this trimetallic configuration compared to the bimetallic configuration. The metallurgical details of these studies are also discussed in this paper.     

Minimal inhibition concentrations of selected antibiotics for strains of Staphylococcus aureus

Minimal inhibition concentrations (MIC) of gentamycin (Ge), neomycin (Neo), rifampicin (Rif), ampicillin (Amp), lincomycin (Lin), erythromycin (Ery), and streptomycin (STM) were determined by the agar dilution technique using 46, 130, 131, 125, 140, 139 and 142 strains of Staphylococcus aureus, respectively. The strains, selected from the collection of the authors' laboratory, were isolated from mammary gland secretions of cows affected with clinical or subclinical mastitis. The following ranges of MIC (micrograms/ml) were assessed for the antibiotics under study: Ge 0.125-0.50, Neo 0.06-0.50, Rif 0.0039-0.030, Amp 0.015-1.00, Lin 0.25-1.00, Ery 0.06-0.25, STM 0.50-64.0. Modal MIC (micrograms/ml) were as follows; Ery 0.125 (86%), Lin 0.5 (71.4%), Rif 0.007 (68.7%), Ge 0.25 (56.5%), STM 1.00 (54.2%), Neo 0.25 (53.8%), Amp 0.06 (41.6%). The order of efficiency expressed in MIC 90 (micrograms/ml) was as follows: Rif (0.015), Ery (0.125), Ge (0.25), Neo (0.25), Amp (0.5), STM (4.0).     

Analysis of aperture blockage in reflector antennas by usingobstacle-located blockage currents

An improved method is presented to account for blockage effects in the analysis of reflector antennas. Commonly this is done by introducing shadows on the reflector surface according to the location of the obstacles when performing the physical optics integration. By using physical optics blockage currents located at the blocking obstacle instead of at the main reflector surface, the effect of the different locations in the axial direction is accurately accounted for. This can easily be included by a single phase factor in existing computer programs based on physical optics integration     

New wire interface for graded 3-D TLM

A new 3-D graded TLM model for thin radiating wires is presented. The model differs from previous TLM models because the wire is modelled at the interfaces between cells, rather than through the centre of the node. The connection between the TLM symmetrical condensed-node link lines and the line forms a 'wire interface'. The scattering algorithm for the interface and simulation results are given.<>     

Organized media for fluorescence analysis of complex samples: comparison of bile salt and conventional detergent micelles in coal liquids.

Accurate quantitative determinations are often difficult to obtain from fluorescence analysis of complex samples due to sample matrix effects and intermolecular interactions between solutes. Organized media can be used to minimize these unwanted processes without physical separation or extraction of the analytes from the sample matrix by isolating the analyte molecules in a uniform microenvironment within the sample. The advantages of bile salt micellar media over conventional detergent micelles are demonstrated for analysis of coal liquids. The bile salt media is shown to increase the sensitivity and dynamic range of fluorescence measurements relative to simple ethanolic solutions, without promoting gound-state and excited-state interactions that occur in the detergent micellar media.     

Energy method of longevity calculation under an irregular loading. Report 2. Longevity under programmed block loading

A method of calculating longevity to macrocrack development under a programmed loading in the form of a block repeated many times to failure is proposed. Relationships are derived for calculation of longevity under blocks with stepwise variation in stress amplitude, and also blocks assigned by the probability-distribution density of the stress amplitudes and tables of the differential frequency of repetition of peak and average stresses. Consideration of variation in the material's endurance limit under an irregular cyclic loading is demonstrated. It is shown that a specific type of relationships can be derived for the material under investigation with allowance for its kinetic cyclic-strain diagrams. An example of the longevity calculation, which is compared with experimental data for the block loading of steel 40Kh specimens, is cited.Translated from Problemy Prochnosti, No. 8, pp. 3–11, August, 1995.     

The influence of cathodic hydrogen charging on the mechanical behaviour of Al-4Zn-1Mg alloy

The effect of cathodic charging on the mechanical behaviour of Al-4Zn-1Mg alloy was studied. Hardening of the Al-4Zn-1Mg alloy surface, due to the hydrogen absorption, was observed. The ultimate tensile stress of the charged aluminium alloy was noted to be a non-linear function of the charging current density. The cathodically charged aluminium alloy exhibited brittle transgranular fracture at the surface layer, whereas ductile intergranular fracture was observed at the deeper layers of the same alloy.     

Analysis of the effect of shrinkage on macrosegregation in alloy solidification

Numerical calculations based on a continuum model are used to examine the effects of solidification shrinkage on the redistribution of solute in a Pb-19.2 pct Sn mixture which is convectively cooled at a sidewall. For each of three different cooling rates, separate calculations are performed for shrinkage and buoyancy-induced flows, as well as for the combined influence of shrinkage and buoyancy effects. The calculations reveal that flow and macrosegregation patterns are more strongly influenced by buoyancy effects over a wide range of solidification rates. Although extremely large solidification rates yield small regions near the chilled wall in which shrinkage-induced flows control the redis-tribution of solute, the overall effect on macrosegregation is small relative to that associated with buoyancy. Scaling analysis of the governing equations produces reference shrinkage and buoyancy velocities which can be used to extend the current numerical results to other binary systems.