From "macro" to "micro" manipulation: models and experiments

This paper addresses various problems related to manipulation in the micro domain, a field which is increasingly important for research and application. Grasping and manipulating parts with size ranging between a few micrometers and about 1 millimeter (defined in this paper as "micro parts") are required for an increasing number of applications: the assembly of micro systems and micro machines; and the operation in tiny and unpredictable environments, such as for inspection and interventions in pipes and for micro surgery. The aim of this work is to find out similarities and differences between traditional manipulation and micro manipulation, by investigating which requirements are still valid and which must be redefined when the object size scales down. The similarities between the two application domains "macro" and "micro" are pointed out along with the differences, and both are taken into account for the evaluation of different grasping typologies. Dedicated models for the adhesion forces arising at the micro level are presented, preliminarily tested, and discussed.     

Efficient and accurate approach for powder compaction problems

 In this paper, a new approach for powder cold compaction simulations is presented. A density-dependent plastic model within the framework of finite strain multiplicative hyperelastoplasticity is used to describe the highly nonlinear material behaviour; the Coulomb dry friction model is used to capture friction effects at die-powder contact; and an Arbitrary Lagrangian–Eulerian (ALE) formulation is used to avoid the (usual) excessive distortion of Lagrangian meshes caused by large mass fluxes. Several representative examples, involving structured and unstructured meshes are simulated. The results obtained agree with the experimental data and other numerical results reported in the literature. It is shown that, contrary to other Lagrangian and adaptive h-remeshing approaches recently reported for this type of problems, the present approach verifies the mass conservation principle with very low relative errors (less than 1% in all ALE examples and exactly in the pure Lagrangian examples). Moreover, thanks to the use of an ALE formulation and in contrast with other simulations, the presented density distributions do not present spurious oscillations. Received: 20 March 2002 / Accepted: 15 October 2002 The partial financial support of the Ministerio de Ciencia y Tecnología (grant number DPI 2001-2204) is gratefully acknowledged.     

Efficient design of oversampled NPR GDFT filterbanks

We propose a flexible, efficient design technique for the prototype filter of an oversampled near perfect reconstruction (NPR) generalized discrete Fourier transform (GDFT) filterbank. Such filterbanks have several desirable properties for subband processing systems that are sensitive to aliasing, such as subband adaptive filters. The design criteria for the prototype filter are explicit bounds (derived herein) on the aliased components in the subbands and the output, the distortion induced by the filterbank, and the imaged subband errors in the output. It is shown that the design of an optimal prototype filter can be transformed into a convex optimization problem, which can be efficiently solved. The proposed design technique provides an efficient and effective tool for exploring many of the inherent tradeoffs in the design of the prototype filter, including the tradeoff between aliasing in the subbands and the distortion induced by the filterbank. We calculate several examples of these tradeoffs and demonstrate that the proposed method can generate filters with significantly better performance than filters obtained using current design methods.     

Catalytic dehydrogenation of ethylbenzene with carbon dioxide: promotional effect of antimony in supported vanadium–antimony oxide catalyst

Alumina-supported vanadium oxide, VO_x/Al₂O₃, and binary vanadium–antimony oxides, VSbO_x/Al₂O₃, have been tested in the ethylbenzene dehydrogenation with carbon dioxide and characterized by S_BET, X-ray diffraction, X-ray photoelectron spectroscopy, hydrogen temperature-programmed reduction and CO₂ pulse methods. VSbO_x/Al₂O₃ exhibited enhanced catalytic activity and especially on-stream stability compared to VO_x/Al₂O₃ catalyst. Incorporation of antimony into VO_x/Al₂O₃ increased dispersion of active VO_x species, enhanced redox properties of the systems and formed a new mixed vanadium–antimony oxide phase in the most catalytically efficient V_0.43Sb_0.57O_x/Al₂O₃ system.     

An alternative blind feedforward symbol timing estimator using two samples per symbol

Recently, S.J. Lee proposed a blind feedforward symbol timing estimator that exhibits low computational complexity and requires only two samples per symbol (see IEEE Commun. Lett., vol.6, p.205-7, 2002). We analyze Lee's estimator rigorously by exploiting efficiently the cyclostationary statistics present in the received oversampled signal; its asymptotic (large sample) bias and mean-square error (MSE) are derived in closed-form expression. A new blind feedforward timing estimator that requires only two samples per symbol and presents the same computational complexity as Lee's estimator is proposed. It is shown that the proposed new estimator is asymptotically unbiased and exhibits smaller MSE than Lee's estimator. Computer simulations are presented to illustrate the performance of the proposed new estimator with respect to Lee's estimator and existing conventional estimators.     

Formation of C49-TiSi2 in flash memories: a nucleation controlled phenomenon?

The formation of Ti silicides has been examined in flash memories with 0.25 μm linewidth by X-ray diffraction, scanning electron microscopy, and transmission electron microscopy. It has been observed that, after the first rapid thermal process and the selective metal etch, there is no silicide on the source and on a majority of drain contacts while C49-TiSi₂ is found on the gate. A pre-amorphisation implant increases drastically the formation of C49-TiSi₂ in the drain zone while modifications of annealing conditions have little impact. These results indicate that the formation of C49-TiSi₂ is most likely controlled by nucleation and that this nucleation is sensitive to both the width and the length of the reaction zone. The formation of a Ti rich silicide may play an important role in this nucleation by decreasing the driving force for the formation of C49-TiSi₂. Curiously enough, the formation of C49-TiSi₂ appears thus as a major concern for the salicide process in flash memories.     

Distance spectrum analysis of space-time trellis-coded Modulations in quasi-static Rayleigh-fading channels

In this correspondence, we propose an algorithm for computing the distance spectrum of a space-time trellis code achieving maximal diversity gain in quasi-static fading channels. We further present a state reduction technique for trellis codes that can reduce the complexity of the distance spectrum computation. We provide numerical results supporting the empirical evidence that a truncated union bound obtained from the distance spectrum provides an accurate characterization of the relative performance ordering of different space-time trellis codes and, therefore, it offers a tool for better space-time trellis code design.     

Structure determination of CaMgGeO4

The crystal structure of CaMgGeO₄ is described. CaMgGeO₄, M_r = 200.9, orthorhombic, Pnam, A = 11.285(5) Å, B = 5.016(2) Å, C = 6.435(2) Å, V = 364.36 ų, Dx = 3.664 Mg/m³.λ(MoK_a = 0.71069 Å, F(000) = 384, room temperature, final R = 0.045 for 1752 observed reflections. The structure is isomorphous with CaMgSiO₄ (monticellite).     

Evaluation of solid-desiccant-based evaporative cooling cycles for typical hot and humid climates

This paper presents an evaluation of various solid desiccant cycles for air conditioning in hot and humid climates. Psychometric evaluation of potential cycles for 16 typical Indian cities has been carried out with the objective of achieving standard comfort conditions in the room. Computer simulation is based on constant effectiveness of heat exchangers and evaporative coolers and actual performance data of a commercially available desiccant wheel dehumidifier. The influence of various outdoor conditions, the effectiveness of heat exchangers/evaporative coolers on the cooling coefficient of performance and volumetric air flowrate per unit cooling capacity have been investigated. It is found that amongst ventilation, recirculation and Dunkle cycles, the Dunkle cycle is better for a wide range of outdoor conditions. However, cycles using wet surface heat exchangers give even higher performance.