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91.
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M. Petrova Z. Noncheva Ts. Dobrev St. Rashkov N. Kounchev D. Petrov St. Vlaev V. Mihnev S. Zarev L. Georgieva D. Buttinelli 《Hydrometallurgy》1996,40(3):293-318
The influence of the mode of obtaining and plastic treatment of binary PbAg and PbCa, and ternary PbAgCa alloys (used as anodes in Zn electro-extraction from sulphate electrolytes) on their electrochemical behaviour and corrosion resistance is studied.It has been established that the rolled PbAg alloys possess a higher corrosion resistance and lower anodic polarization compared to the cast lead-silver ones due to the structural fineness and homogeneity of the plastic deformed anodes. The plastic deformation of the ternary alloys with calcium content of 0.06% causes Pb3Ca precipitation in the solid solution. The hot-rolled alloys form an solid solution of Pb3Ca with fine-grained structure, deformed through the rolling direction. The cold-rolled alloys possess clearly expressed oriented structures also through the rolling direction.Cast and plastically deformed PbCa anodes possess better electrochemical and corrosion characteristics than pure Pb but a considerably higher anodic polarization and lower corrosion resistance than PbAg alloys. Both PbCa systems, with a calcium content of 0.08 and 0.11 % are very appropriate for the preparation of ternary PbAgCa alloys. These alloys (PbAg 0.5 %-Ca 0.11 %) possess better electrochemical and corrosion characteristics than binary PbCa ones. Only ternary rolled alloys have equal corrosion and electrochemical properties to those of the alloy PbAg (0.75%–1.0%) used in practice. 相似文献
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O. A. Kaibyshev N. G. Zaripov L. V. Petrova O. Yu. Efimov 《Journal of Engineering Physics and Thermophysics》1993,65(5):1138-1142
The superplastic ductility of oxide and nonoxide SHS ceramics is considered. It is established that with certain temperature-rate dependences these ceramic materials manifest features typical of superplastic flow. It is shown that the ceramics undergo some specific microstructural changes under strain conditions.Institute of Problems of Metal Superductility, Russian Academy of Sciences, Ufa. Translated from Inzhenerno-Fizicheskii Zhurnal, Vol. 65, No. 5, pp. 617–622, November, 1993. 相似文献
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St. Rashkov Y. Stefanov Z. Noncheva M. Petrova Ts. Dobrev N. Kunchev D. Petrov St. Vlaev V. Mihnev S. Zarev L. Georgieva D. Buttinelli 《Hydrometallurgy》1996,40(3):319-334
The electrochemical oxidation processes and phase formation on binary PbAg and PbCa, and ternary PbAgCa alloys during anodic treatment of the electrodes for conditions in a sulphuric acid electrolyte were investigated.The electrochemical behaviour of lead and its alloys was studied by the cyclic voltammetry method (CVA). X-ray and SEM were used for the phase composition and surface structure analysis. It was established that only the ternary plastically treated PbAg 0.5%-Ca 0.11% alloys reveal similarities to the industrially applied PbAg 1 % anodes. It may be assumed in the case of ternary alloys that the catalytic layer is composed of a dense non-conductive MnO2 layer of crystals serving as basic sites for oxygen evolution. 相似文献