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The powder synchrotron X-ray diffraction pattern of a mixed sodium–silver–Y zeolite, Ag56−xNaxSi136Al56O384 x≈19, saturated with pyridine, has been analysed by the Rietveld method to reveal positions for the adsorbed molecules. Cations are distributed over three sites, SII, constrained to 100% occupancy, with 17.2(1) and 14.8(1) Ag(1) and Na(1) ions per unit cell, respectively, SI′ with 18.3(1) Ag(2) ions per cell, and SI with 1.8(1) Ag(3) ions per cell. The refinement suggests that approximately 7.5 pyridine molecules are adsorbed per supercage, located in two sites within the cavities of the zeolite. Pyridine(1) is in the 12-ring window connecting supercages. Three molecules project through each window and approach the SII cations in a supercage, with an average Ag(1)–N distance of 3.17(2) Å. An SII cation can be linked to three pyridine(1) molecules from three separate windows. These sites are full with 5.98(2) molecules per supercage. Pyridine(2) is found in the supercage, oriented with its π electron density towards the SII cations, with its centre at 2.87(2) Å from Ag(1). The average occupancy was fixed at 1.5 molecules per supercage, corresponding to 20% of the pyridine content. A local ordering scheme can be postulated, whereby alternate supercages are filled by pyridine(1) and pyridine(2) molecules, efficiently filling the channels of the zeolite. 相似文献
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Andrea D. Adamczak Adam A. Spriggs Danielle M. Fitch Walid Awad Charles A. Wilkie Jaime C. Grunlan 《应用聚合物科学杂志》2010,115(4):2254-2261
High‐temperature polymers are being used for a broad range of applications, such as composite matrices for structural applications (e.g., high speed aircraft). Polyimides are a special class of polymers that meet the thermal and oxidative stability requirements for high temperature composite aerospace applications. A weight loss study was performed on a fluorinated polyimide resin and its carbon fiber composite in an effort to determine its thermal stability and degradation mechanisms. Experiments were conducted using a preheated oven and thermogravimetric analysis to obtain the weight loss. Regardless of the method used, the resin and composite exhibited excellent thermal stability (less than 1% weight loss) below 430°C, regardless of 2–20 min of exposure. After 20 min of exposure at 510°C, the composite remained relatively stable with only 5.3% weight loss using the oven technique, whereas the neat polyimide sustained 12.6%. When degradation occurred, it was found to be the result of thermolysis and oxidation (to a lesser extent). © 2009 Wiley Periodicals, Inc. J Appl Polym Sci, 2010 相似文献
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<正>本期重点:1使用仿制图章工具2转换黑白影调和调整反差3调整画面影调与色彩4调整高光与增加细节5使用蒙版工具强化色彩和反差6调整构图与使用可选颜色7使用自由变换与调节曲线一张优秀的照片如何脱颖而出?是什么让它显得与众不同?如果你需要建议让自己的照片变得出色,我们的专家很乐意在此提供 相似文献
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Daytime sleep tendency was assessed in 10 drug-free patients with narcolepsy-cataplexy and 10 normals matched for age and gender. Following nocturnal polysomnography, the alpha attenuation test (AAT) and the multiple sleep latency test (MSLT) were administered during five sessions occurring at 2-hour intervals beginning at 0900 and 1000 hours, respectively. For the AAT, participants were polysomnographically recorded for 8 minutes while seated in an illuminated room with their eyes alternately opened and closed. Power spectral analyses of electroencephalograph (EEG) activity at 02-A1 (10 second epochs) were calculated using fast Fourier transformations (FFT) within the alpha frequency range (8-12 Hz) to obtain ratios of mean eyes-closed to mean eyes-open alpha power (i.e. the alpha attenuation coefficient, AAC). The narcoleptics were sleepier than the normals as indicated by a significantly smaller mean AAC and a significantly shorter mean latency to stage 1 on the MSLT. These findings suggest that the AAT may provide a quick and practical objective assessment of the excessive daytime sleepiness (EDS) associated with narcolepsy. 相似文献