Nucleation and growth of nickel by electrodeposition under galvanostatic conditions

The first stages of nickel electrodeposition on amorphous carbon and polycrystalline silver substrates have been studied under galvanostatic conditions. An island growth mode is observed on the two types of substrate. For equivalent conditions the cluster density is higher on silver substrates than on carbon substrates. Dissolution of some nickel clusters is observed a short time after the onset of electrolysis on carbon substrates. This is confirmed by the evolution of the current efficiency and the evolution of the metal surface cluster density as a function of the quantity of electricity.     

溶剂对溶胶-凝胶法制备LaMnFe2Al9O19催化剂的影响

摘要 用溶胶凝胶法制备六铝酸盐催化剂LaMnFe2Al9O19，通过BET、XPS、XRD等技术，对催化剂的结构和性质进行了研究，主要考察了在制备过程中不同的醇做溶剂对催化剂结构及其甲烷催化燃烧活性的影响。结果表明：不同醇做溶剂所制备的催化剂LaMnFe2Al9O19 在1200℃焙烧后都可以形成完整的六铝酸盐晶型，且具有较高高温稳定性。同时对于催化剂的的催化性能也有较大的影响，用异丙醇做溶剂所得催化剂的催化活性最高，并保持了较大的比表面积。     

税务发票改革的前哨战--访上海市北印刷厂

税收是国家的命脉.现行税收征管工作中存在着买卖和使用假发票,非法倒卖发票,虚开发票金额,消费者不索取发票等难以解决的顽症.为了加强税收征管,北京等地于今年8月推行新版税务发票,即"刮开式有奖发票".使用新版税务发票后,京城部分地区餐饮娱乐业的同期税收增长6倍!     

Al-Cu-Fe系初生准晶相凝固过程的电子显微分析

采用包括金相（OM），粉末X射线衍射（XRD），扫描电子显微镜（SEM）观察和透射电子显微（TEM）分析等方法，研究了铸态Al592.Cu36.8Fe3.0Si1.0合金（700℃保温2．5h后水淬）的显微组织及相组成。发现铸锭中存在4种相：准晶I相，τ3相（或φ相），θ－Al2Cu相和η－AlCu相，凝固过程可描述为：初生晶是准晶Ⅰ相；在保温过程中发生包晶或共晶反应（L＋i→τ3(或φ）或L→τ3（或φ）＋i)形成的τ3相（或φ相），呈微畴结构；而剩余液体水淬形成θ－Al2Cu相和η－AlCu 相。     

岩石工程力学特性参数测定装置设计

岩石工程力学特性参数测定装置实现了对试验载荷的恒速率加载 ,可对压模的吃深和试验载荷进行连续记录 ,记录的数据可实时显示及处理 ,且动态显示试验岩石的特性曲线 (试验载荷—轴向应变 )。该装置体积小、可移动性强 ,且能一机多用。文章详细阐述该装置机械结构、电路和系统软件的设计等     

影响超声测厚精度的因素浅析

超声测厚是一种简单易行、应用广泛的无损检测手段。但是 ,由于炼油系统的测厚对象大部分是曲率半径较小的管道 ,且经常需要带温测量 ,所以要保证超声测厚的数据精度并非易事。下文在总结实验室试验结果的基础上 ,提出一些保证测厚精度的措施 ,供各位专家参考。1　超声测厚原理及影响因素分析　　超声测厚是利用探头晶片发出的超声波脉冲在工件中传播时遇到异种介质界面就会产生反射这一原理进行的。仪器显示的测厚数据是超声波在被测物体中的声速与该声波在物体界面区内的往返时间乘积的一半。具体测量中 ,经常采用机械或化学方法清除被测…     

Transient Green’s Tensor for a Layered Solid Half-Space With Different Interface Conditions

Pulsed ultrasonic techniques can be and have been used to examine the interface conditions of a bonded structure. To provide a theoretical basis for such testing techniques we model the structure as a layer on top of a half-space, both of different elastic properties, with various interface bonding conditions. The exact dynamic Green’s tensor for such a structure is explicitly derived from the three-dimensional equations of motion. The final solution is a series. Each term of the series corresponds to a successive arrival of a “generalized ray” and each is a definite line integral along a fixed path which can be easily computed numerically. Willis’ method is used in the derivation. A new scheme of automatic generation of the arrivals and ray paths using combinatorial analysis, along with the summation of the corresponding products of reflection coefficients is presented. A FORTRAN code is developed for computation of the Green’s tensor when both the source and the detector are located on the top surface. The Green’s tensor is then used to simulate displacements due to pulsed ultrasonic point sources of known time waveform. Results show that the interface bonding conditions have a great influence on the transient displacements. For example, when the interface bonding conditions vary, some of the first few head waves and regular reflected rays change polarities and amplitudes. This phenomenon can be used to infer the quality of the interface bond of materials in ultrasonic nondestructive evaluation. In addition the results are useful in the study of acoustic microscopy probes, coatings, and geo-exploration.     

CAD8903机芯的视频音频转换电路设计

本文概要介绍了CAD 8903机芯采用国产集成电路CD7680,CD74211,DG4053实现音频、视频切换功能的电路,并对CD7680中音频信号处理电路的特殊用法进行了说明。     

广义米理论及其在粒度分析中的应用

有形波束的散射问题在粒度分析测量仪器的研究中有着特殊重要的意义，本文介绍了处理均匀球形粒子对有形波束散射的广义米理论，并应用该理论研究了双柱形激光波束粒子测量系统的散射问题，与未理论和几何光学相比，其结果与实验吻合很好。