Soft Wearable Systems for Colorimetric and Electrochemical Analysis of Biofluids

Wearable monitoring systems provide valuable insights about the state of wellness, performance, and progression of diseases. Although conventional wearable systems have been effective in measuring a few key biophysical markers, they offer limited insights into biochemical activity and are otherwise cumbersome in ambulatory modes of use, relying on wired connections, mechanical straps, and bulky electronics. Recent advances in skin‐interfaced microfluidics, stretchable/flexible electronics, and mechanics have created new wearable systems with capabilities in real‐time, noninvasive analysis of sweat biochemistry in combination with biophysical metrics. Here, the latest technologies in multifunctional sweat sensing systems are presented with a focus on novel microfluidic designs, fully‐integrated wireless electrochemical sensors, and hybrid biochemical/biophysical sensing capabilities, creating real‐time physiological insights.     

A fast-locking low-jitter digitally-enhanced DLL dynamically controlled for loop-gain and stability

Conventional structure of delay locked loops (DLLs) is modified to achieve better jitter and smaller lock time. In the proposed structure, analog charge pump is eliminated, to remove the problems of leakage current on output capacitance, and is replaced by combination of a digital accumulator (ACC) and a digital-to-analog converter. A programmable ACC is also proposed, to dynamically control the loop gain and lock time. When the loop enters to lock region at the first time, a lock detector block disables ACC and equivalent digital code is stored on a latch array. So, a fixed control voltage controls delay elements and the systematic jitter, due to periodic discharge of control voltage. RMS jitter of less than 33.5 and 1.6 ps are achieved at 20 and 625 MHz operating frequencies, respectively, when the supply is subject to 110 mV random noise and also 40 mV periodic noise, related to generated clock signals. Lock time is reduced from 38 to 2 µs at 20 MHz, and also from 900 to 45 ns at 600 MHz, when the proposed dynamic control mechanism is applied on the loop. Total power consumption for the main core of DLL is 7.85 mW at 1.8 V supply in 0.18 µm CMOS process.     

Feasibility of automating military''s environmental operations

This paper focuses on analyses of the feasibility of telerobotic and autonomous systems in hazardous environments. The hazardous environments are divided into three missions: area clearance, removal of unexploded ordnance, and hazardous waste removal. This paper identifies the factors impacting military's missions on various operating systems. Then, a decision support system based on fuzzy logic is developed for studying these factors to determine the feasibility of automating military's environmental restoration operations. The last part of the paper provides a set of recommendations for technology policy development.     

Effect of processing parameters and glycerin addition on the properties of Al foams

Aluminum foam has been produced by sintering and dissolution processes using NaCl powders as a space holder. In this research, glycerin is used as a novel lubricant along with acetone. The effects of the processing parameters including compacting pressure, sintering temperatures (620, 640 and 650 °C), size, and volume fraction of the space holder, on the physical and mechanical properties of the produced foams have been investigated. Due to segregation of the Al and NaCl powders at high compaction pressures, spalling of Al foams was observed. Meanwhile, adding small amounts of acetone and glycerin to the mixture ensures homogeneity and prevents segregation of dissimilar powders at varying pressure. Moreover, the addition of glycerin provides an improved homogenous stress distribution within the produced foams during mechanical testing, which in turn halts crack propagation. Meanwhile, an alternative technique to remove NaCl particles during the dissolution stage has been proposed. The results showed that high quality foams were successfully produced under a compaction pressure range of 250–265 MPa and sintering temperature of 650 °C.     

Analyzing the fractal feature of nickel thin films surfaces modified by low energy nitrogen ion

Fractal concepts are used to explore how different energies (10, 20 and 50 keV) and fluence of 5 × 10¹⁷ N⁺ cm^?2 affect the morphology of nickel thin film. The nickel thin film with thickness of 100 nm is prepared by electron beam evaporation technique at room temperature on stainless steel (AISI 316) substrates. The nanoscale three‐dimensional (3‐D) surface micro‐morphologies are investigated by atomic force microscopy (AFM). Interface width is used to describe the surface height fluctuations. The autocorrelation function with height‐height correlation function give the quantitative data about the morphology of surface. The value of roughness exponent and fractal dimension is computed by height‐height correlation function. Fractal measure is an important analysis which provides fundamental insights into the texture characteristics and a direct way of testing their functional role.     

Polyphenol-Induced Adhesive Liquid Metal Inks for Substrate-Independent Direct Pen Writing

Surface patterning of liquid metals (LMs) is a key processing step for LM-based functional systems. Current patterning methods are substrate specific and largely suffer from undesired imperfections—restricting their widespread applications. Inspired by the universal catechol adhesion chemistry observed in nature, LM inks stabilized by the assembly of a naturally abundant polyphenol, tannic acid, has been developed. The intrinsic adhesive properties of tannic acid containing multiple catechol/gallol groups, allow the inks to be applied to a variety of substrates ranging from flexible to rigid, metallic to plastics and flat to curved, even using a ballpoint pen. This method can be further extended from hand-written texts to complex conductive patterns using an automated setup. In addition, capacitive touch and hazardous heavy metal ion sensors have been patterned, leveraging from the synergistic combination of polyphenols and LMs. Overall, this strategy provides a unique platform to manipulate LMs from hand-written pattern to complex designs onto the substrate of choice, that has remained challenging to achieve otherwise.     

Behaviors of capacitive and Pirani vacuum gauges

Knowing the exact pressure of the process has a great impact on the validity of the results, product quality, energy efficiency, and in some processes, on the security of work with the system. Hence, the calibration of the barometers and the accuracy of the readings should be taken seriously. Choosing the appropriate time interval for re-calibration is done according to the extent and conditions of use, uncertainty, and the inaccuracy allowed in measurement, constructive suggestion, and some other things. Failure to pay attention to the importance of periodic calibration in vacuum gauges leads to some irreparable losses in the research project and the vacuum generator system. In this study, using McLeod's barometer, the deviation of capacitive and Pirani vacuum gauges is investigated at different time intervals in the middle vacuum range, and it is determined that the vacuum gauge faces a serious deviation from the actual calibrated amount for upper and lower ranges of middle vacuum in the same working pressure range over time.