亚麻粗纱煮漂工艺研究

亚麻粗纱优化煮漂工艺如下:(1)在100℃时,用3.5g/lNaOH碱煮30分钟;(2)在80℃时,在pH值为4.5,经30分钟完成亚漂;(3)在90℃时,pH为9的条件下处理20分钟完成氧漂;经煮漂的纱其纤维素含量提高了10.38%,果胶质、木质素、脂蜡等含量下降到了较好的水平,白度达到69.68%,大幅度改善了亚麻的纺织性能和服用性能。     

Surface plasmon resonance evaluation of various aminoglycoside-RNA hairpin interactions reveals low degree of selectivity

Aminoglycoside antibiotics, which are able to selectively bind to RNA, are considered to be an important lead in RNA-targeting drug discovery. In this study, surface plasmon resonance (SPR) was employed to explore the interaction of aminoglycosides with known tobramycin-binding RNA hairpins (aptamers) and an unrelated RNA hairpin. It was established that aminoglycosides have multiple interactions with RNA hairpins. Unexpectedly, the different hairpins showed comparable affinity for a set of related aminoglycosides. The observed absence of selectivity presents an extra hurdle in the discovery of novel aminoglycosides as specific drugs that target defined RNA hairpins.     

Interaction of CETP inhibitory peptide and lipoprotein substrates in cholesteryl ester transfer assay: relationship between association properties and inhibitory activities

In a previous study, CETP inhibitory peptide (3 kDa) was isolated from hog plasma. The peptide, synthesized chemically according to the amino acid sequence of the 3-kDa peptide (designated P₂₈), showed CETP inhibitory activity both in vitro and in vivo [Cho et al. (1998) Biochim. Biophys. Acta 1391, 133–144]. We report herein further unique features of P₂₈ when it was associated with the cholesteryl ester (CE)-donor and-acceptor lipoproteins. Lipoprotein substrates with P₂₈ present in both HDL (as a CE-donor) and LDL (as a CE-acceptor) served as poor substrates, with CE-transfer activity decreased up to 60% compared to normal substrates without P₂₈. P₂₈ was found to be located in HDL fractions of hog plasma and showed the same electromobility as that visualized by PAGE on 7% polyacrylamide gel under nondenaturing conditions. Addition of apolipoprotein A-1 (apoA-1) or apoB antibody to a normal CE-transfer mixture did not alter CE-transfer activity. However, addition of apoA-1 or −B antibody to a CETP-inhibition mixture decreased the inhibitory activity of P₂₈ by ca. 20%. Western blot analysis revealed that P₂₈ was associated only with human and hog HDL among several lipoproteins purified from human, hog, and rabbit. CFTP-inhibition assays with various lipoprotein substrates revealed that P₂₈ exhibited substrate-specific inhibitory activity. The inhibitory activity of P₂₈ was highly dependent on the type of lipoprotein substrate (whether CE-donor or-acceptor); P₂₈ inhibited CE transfer from HDL to LDL, but it did not inhibit CE transfer from HDL to HDL.     

非均相催化湿式氧化活性红2BF的研究

以Fe/AC为催化剂、O2为氧化剂的非均相催化氧化体系处理偶氮染料活性红2BF,考察了反应温度、氧分压、废水pH、催化剂投加量等因素对降解效果的影响。结果表明,染料初始质量浓度为400 mg/L时,在温度150℃、氧分压0.5 MPa、pH=3、反应时间60 min、催化剂投加量为4 g/L的最佳条件下,活性红2BF色度几乎完全去除,TOC去除率达94.21%。     

T202铁钼催化剂升温硫化

干法脱硫中铁钼催化剂将有机硫转化成H2S,再经氧化锰和氧化锌脱硫槽吸收H2S,每次升温硫化时间3—4d。 1理化指标和反应机理 T202型催化剂外观为棕褐色,圆柱体以γ-Al2O3为载体,载有Fe、Mo,堆密度0．7-0．9kg／L。主要成份MoO3：7．5％-10．5％、FeO：2．0％-3．0％。工业使用条件,温度：350-420℃,压力：1．6-4．0MPa,空速：1000h^-1,径向抗压碎力均值≥147N／cm^2,有机硫转化率≥96％。升温硫化机理是将氧化态的铁钼,转变为具有活性的硫化物。     

草酸改进铁/铜微电解体系降解活性艳蓝KN-R

在铸铁上负载铜的铁/铜催化微电解体系中加入草酸后,质量浓度为100 mg/L活性艳蓝KN-R溶液迅速脱色,化学需氧量明显降低,改善了微电解体系对废水处理时间长、化学需氧量去除效果低等缺点.实验结果表明:在pH为3.28(加入草酸后)、草酸投加量为5 mg/L、催化剂投加量为10 g/L的条件下,对质量浓度为100 mg...     

新工科背景下基于OBE的混合教学模式探索——以软件工程为例

基于OBE的混合教学模式以成果为导向,以学生为中心,以培养目标为核心的教学设计理念,符合新工科背景下培养大量应用型创新创业人才的需求。本文以提升学生自主学习能力和实践应用能力为目标,基于OBE反向教学设计理念实施软件工程混合式教学,将线上自主学习和线下翻转教学和案例驱动实践教学有机结合,充分调动学生的积极性和主动性。     

可见光级铝合金反射镜一体化设计与分析

高精度的反射镜对于航空航天载荷具有重要的意义。随着单点金刚石车削加工技术(SPDT)和抛光技术的发展,铝合金反射镜以快速低成本制造等优点用于可见光级的应用中。为了降低系统装调的自由度,设计了一种一体化的反射镜结构,并针对126mm口径主三反射镜进行有限元建模仿真,通过对反射镜自重分析、模态分析和加工离心力分析。得出设计的主三反射镜具有较高的动态刚度,多种工况下反射镜的镜面形变化均低于1/40λ(λ=632.8nm),可应用于可见光系统中,为金属反射镜的集成设计和制造提供一定的参考。     

工艺参数对直流磁控溅射法制备氧化铝薄膜的试验研究北大核心

采用直流磁控溅射法在载玻片和不锈钢基底上制备某设计要求的氧化铝薄膜,首先采用单因素法分别分析溅射功率、氧气流量、工作压强、负偏压及本底真空度等制备参数对薄膜沉积速率的影响;在此基础上设计正交试验,研究优化范围内溅射功率、氧气流量、工作压强对沉积速率的影响,并进行极差与方差分析。结果表明,在一定工艺参数范围内,随着溅射功率的增加,薄膜的沉积速率不断增大;氧气流量增加时薄膜的沉积速率不断下降;随着工作压强的增大,薄膜的沉积速率先增大后减小,在1.0 Pa时达到最大速率;加载的负偏压增加时,薄膜的沉积速率不断降低;本底真空度提高时薄膜的沉积速率不断增大;通过使用XRD衍射仪对制备的薄膜进行物相检测,研究结果表明,常温下不同氧气流量制备的氧化铝薄膜均为非晶态;获取了制备所需薄膜的较优的制备工艺。